A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass
Lemon grass is an inexpensive raw material that can be used to produce natural silica. A method using hydrochloric acid (HCl) leaching followed by thermal combustion at 600 °C was developed to produce purified silica from lemon grass. Acid leaching temperatures of 33, 50, 80, and 110 °C were used. T...
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North Carolina State University
2015-12-01
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Series: | BioResources |
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Online Access: | http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_1_1270_Nur_Firdaus_Simple_Method_Production_Pure%20Crystalline_Silica |
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author | Mohamed Yusof Nur Firdaus Hakimah Osman Hank S. C. Metselaar A. Rahman Rozyanty |
author_facet | Mohamed Yusof Nur Firdaus Hakimah Osman Hank S. C. Metselaar A. Rahman Rozyanty |
author_sort | Mohamed Yusof Nur Firdaus |
collection | DOAJ |
description | Lemon grass is an inexpensive raw material that can be used to produce natural silica. A method using hydrochloric acid (HCl) leaching followed by thermal combustion at 600 °C was developed to produce purified silica from lemon grass. Acid leaching temperatures of 33, 50, 80, and 110 °C were used. The silica content of the lemon grass ash was characterized using X-ray fluorescence (XRF), X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) analysis. The shape and texture of the lemon grass ash were studied using SEM. The highest silica content (98.59%) was produced by lemon grass that had been treated at the highest leaching temperature (110 °C). Other elements that were found in the lemon grass ash were magnesium, calcium, potassium, and chlorine. XRD analysis showed that the crystallinity of the silica in treated lemon grass ash increased with increasing leaching temperature. The FTIR analysis confirmed the presence of siloxane and silanol bonds in lemon grass that was calcined at different leaching temperatures. |
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institution | Directory Open Access Journal |
issn | 1930-2126 1930-2126 |
language | English |
last_indexed | 2024-04-12T04:25:21Z |
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spelling | doaj.art-281bd48bb48041b790dcc7b67783c3032022-12-22T03:48:06ZengNorth Carolina State UniversityBioResources1930-21261930-21262015-12-011111270127910.15376/biores.11.1.1270-1279A Simple Method for the Production of Pure Crystalline Silica from Lemon GrassMohamed Yusof Nur Firdaus0Hakimah Osman1Hank S. C. Metselaar2A. Rahman Rozyanty3Universiti Malaysia Perlis; MalaysiaUniversiti Malaysia Perlis; MalaysiaUniversity of Malaya; MalaysiaUniversiti Malaysia Perlis; MalaysiaLemon grass is an inexpensive raw material that can be used to produce natural silica. A method using hydrochloric acid (HCl) leaching followed by thermal combustion at 600 °C was developed to produce purified silica from lemon grass. Acid leaching temperatures of 33, 50, 80, and 110 °C were used. The silica content of the lemon grass ash was characterized using X-ray fluorescence (XRF), X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) analysis. The shape and texture of the lemon grass ash were studied using SEM. The highest silica content (98.59%) was produced by lemon grass that had been treated at the highest leaching temperature (110 °C). Other elements that were found in the lemon grass ash were magnesium, calcium, potassium, and chlorine. XRD analysis showed that the crystallinity of the silica in treated lemon grass ash increased with increasing leaching temperature. The FTIR analysis confirmed the presence of siloxane and silanol bonds in lemon grass that was calcined at different leaching temperatures.http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_1_1270_Nur_Firdaus_Simple_Method_Production_Pure%20Crystalline_SilicaSilicaInorganic compoundsAcid leaching treatmentCrystallinity |
spellingShingle | Mohamed Yusof Nur Firdaus Hakimah Osman Hank S. C. Metselaar A. Rahman Rozyanty A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass BioResources Silica Inorganic compounds Acid leaching treatment Crystallinity |
title | A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass |
title_full | A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass |
title_fullStr | A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass |
title_full_unstemmed | A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass |
title_short | A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass |
title_sort | simple method for the production of pure crystalline silica from lemon grass |
topic | Silica Inorganic compounds Acid leaching treatment Crystallinity |
url | http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_1_1270_Nur_Firdaus_Simple_Method_Production_Pure%20Crystalline_Silica |
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