A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass

Lemon grass is an inexpensive raw material that can be used to produce natural silica. A method using hydrochloric acid (HCl) leaching followed by thermal combustion at 600 °C was developed to produce purified silica from lemon grass. Acid leaching temperatures of 33, 50, 80, and 110 °C were used. T...

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Main Authors: Mohamed Yusof Nur Firdaus, Hakimah Osman, Hank S. C. Metselaar, A. Rahman Rozyanty
Format: Article
Language:English
Published: North Carolina State University 2015-12-01
Series:BioResources
Subjects:
Online Access:http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_1_1270_Nur_Firdaus_Simple_Method_Production_Pure%20Crystalline_Silica
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author Mohamed Yusof Nur Firdaus
Hakimah Osman
Hank S. C. Metselaar
A. Rahman Rozyanty
author_facet Mohamed Yusof Nur Firdaus
Hakimah Osman
Hank S. C. Metselaar
A. Rahman Rozyanty
author_sort Mohamed Yusof Nur Firdaus
collection DOAJ
description Lemon grass is an inexpensive raw material that can be used to produce natural silica. A method using hydrochloric acid (HCl) leaching followed by thermal combustion at 600 °C was developed to produce purified silica from lemon grass. Acid leaching temperatures of 33, 50, 80, and 110 °C were used. The silica content of the lemon grass ash was characterized using X-ray fluorescence (XRF), X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) analysis. The shape and texture of the lemon grass ash were studied using SEM. The highest silica content (98.59%) was produced by lemon grass that had been treated at the highest leaching temperature (110 °C). Other elements that were found in the lemon grass ash were magnesium, calcium, potassium, and chlorine. XRD analysis showed that the crystallinity of the silica in treated lemon grass ash increased with increasing leaching temperature. The FTIR analysis confirmed the presence of siloxane and silanol bonds in lemon grass that was calcined at different leaching temperatures.
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spelling doaj.art-281bd48bb48041b790dcc7b67783c3032022-12-22T03:48:06ZengNorth Carolina State UniversityBioResources1930-21261930-21262015-12-011111270127910.15376/biores.11.1.1270-1279A Simple Method for the Production of Pure Crystalline Silica from Lemon GrassMohamed Yusof Nur Firdaus0Hakimah Osman1Hank S. C. Metselaar2A. Rahman Rozyanty3Universiti Malaysia Perlis; MalaysiaUniversiti Malaysia Perlis; MalaysiaUniversity of Malaya; MalaysiaUniversiti Malaysia Perlis; MalaysiaLemon grass is an inexpensive raw material that can be used to produce natural silica. A method using hydrochloric acid (HCl) leaching followed by thermal combustion at 600 °C was developed to produce purified silica from lemon grass. Acid leaching temperatures of 33, 50, 80, and 110 °C were used. The silica content of the lemon grass ash was characterized using X-ray fluorescence (XRF), X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) analysis. The shape and texture of the lemon grass ash were studied using SEM. The highest silica content (98.59%) was produced by lemon grass that had been treated at the highest leaching temperature (110 °C). Other elements that were found in the lemon grass ash were magnesium, calcium, potassium, and chlorine. XRD analysis showed that the crystallinity of the silica in treated lemon grass ash increased with increasing leaching temperature. The FTIR analysis confirmed the presence of siloxane and silanol bonds in lemon grass that was calcined at different leaching temperatures.http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_1_1270_Nur_Firdaus_Simple_Method_Production_Pure%20Crystalline_SilicaSilicaInorganic compoundsAcid leaching treatmentCrystallinity
spellingShingle Mohamed Yusof Nur Firdaus
Hakimah Osman
Hank S. C. Metselaar
A. Rahman Rozyanty
A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass
BioResources
Silica
Inorganic compounds
Acid leaching treatment
Crystallinity
title A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass
title_full A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass
title_fullStr A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass
title_full_unstemmed A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass
title_short A Simple Method for the Production of Pure Crystalline Silica from Lemon Grass
title_sort simple method for the production of pure crystalline silica from lemon grass
topic Silica
Inorganic compounds
Acid leaching treatment
Crystallinity
url http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_1_1270_Nur_Firdaus_Simple_Method_Production_Pure%20Crystalline_Silica
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