5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
In the title molecule, C23H25FN4O7, the dihedral angle between the indole skeleton (r.m.s. deviation = 0.022 Å) and the triazole moiety is 74.67 (7)°. The molecules pack in a three-dimensional network in the crystal, being linked by C—H...O and N—H...O hydrogen bonds.
| Main Authors: | , , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2017-05-01
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| Series: | IUCrData |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314617007398 |
| _version_ | 1818858583550328832 |
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| author | Fatima-Zahrae Qachchachi Joel T. Mague Youssef Kandri Rodi Amal Haoudi El Mestafa El Hadrami El Mokhtar Essassi |
| author_facet | Fatima-Zahrae Qachchachi Joel T. Mague Youssef Kandri Rodi Amal Haoudi El Mestafa El Hadrami El Mokhtar Essassi |
| author_sort | Fatima-Zahrae Qachchachi |
| collection | DOAJ |
| description | In the title molecule, C23H25FN4O7, the dihedral angle between the indole skeleton (r.m.s. deviation = 0.022 Å) and the triazole moiety is 74.67 (7)°. The molecules pack in a three-dimensional network in the crystal, being linked by C—H...O and N—H...O hydrogen bonds. |
| first_indexed | 2024-12-19T08:58:36Z |
| format | Article |
| id | doaj.art-283f16056d774f2fa5a7ffc810225009 |
| institution | Directory Open Access Journal |
| issn | 2414-3146 |
| language | English |
| last_indexed | 2024-12-19T08:58:36Z |
| publishDate | 2017-05-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | IUCrData |
| spelling | doaj.art-283f16056d774f2fa5a7ffc8102250092022-12-21T20:28:32ZengInternational Union of CrystallographyIUCrData2414-31462017-05-0125x17073910.1107/S2414314617007398hb41455-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dioneFatima-Zahrae Qachchachi0Joel T. Mague1Youssef Kandri Rodi2Amal Haoudi3El Mestafa El Hadrami4El Mokhtar Essassi5Laboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoDepartment of Chemistry, Tulane University, New Orleans, LA 70118, USALaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Hétérocyclique URAC 21, Pôle de Compétence Pharmacochimie, Av. Ibn Battouta, BP 1014, Faculté des Sciences, Université Mohammed V, Rabat, MoroccoIn the title molecule, C23H25FN4O7, the dihedral angle between the indole skeleton (r.m.s. deviation = 0.022 Å) and the triazole moiety is 74.67 (7)°. The molecules pack in a three-dimensional network in the crystal, being linked by C—H...O and N—H...O hydrogen bonds.http://scripts.iucr.org/cgi-bin/paper?S2414314617007398crystal structuretriazoleisatinhydrogen bond |
| spellingShingle | Fatima-Zahrae Qachchachi Joel T. Mague Youssef Kandri Rodi Amal Haoudi El Mestafa El Hadrami El Mokhtar Essassi 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione IUCrData crystal structure triazole isatin hydrogen bond |
| title | 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione |
| title_full | 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione |
| title_fullStr | 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione |
| title_full_unstemmed | 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione |
| title_short | 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione |
| title_sort | 5 fluoro 1 1 1s 2r 6r 8s 9r 4 4 11 11 tetramethyl 3 5 7 10 12 pentaoxatricyclo 7 3 0 02 6 dodecan 8 yl methyl 1h 1 2 3 triazol 4 yl methyl 2 3 dihydro 1h indole 2 3 dione |
| topic | crystal structure triazole isatin hydrogen bond |
| url | http://scripts.iucr.org/cgi-bin/paper?S2414314617007398 |
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