The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition
The research aims to determine the influence of aniline concentration and deposition time on the characteristics of polyaniline prepared using potentiostatic and galvanostatic electrodeposition methods. FTIR characterization data shows the typical peak of polyaniline in the form of the presence of a...
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Format: | Article |
Language: | English |
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The Center for Science Innovation
2022-02-01
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Series: | Chemistry and Materials |
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Online Access: | https://piscience.org/index.php/cma/article/view/20 |
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author | Mega Sutrisno Maria Paristiowati Nailah Fauziyyah |
author_facet | Mega Sutrisno Maria Paristiowati Nailah Fauziyyah |
author_sort | Mega Sutrisno |
collection | DOAJ |
description | The research aims to determine the influence of aniline concentration and deposition time on the characteristics of polyaniline prepared using potentiostatic and galvanostatic electrodeposition methods. FTIR characterization data shows the typical peak of polyaniline in the form of the presence of a quinoid functional group at a wavenumber of 1596.16 cm-1. The typical diffraction pattern of polyaniline using XRD was detected at peaks of 2θ 21.1007o and 23.5995o. Polyaniline formed using SEM has a surface morphology that grows in a stacked and irregular manner and has a high conductance value so that it can be used as a substrate in Fe/Ni electrodeposition. The results of the Fe/Ni electrodeposition process when viewed using SEM cause the polyaniline surface morphology to be covered by a Fe/Ni alloy by having an elemental composition from the EDS test data, are iron (Fe) 68.15% and nickel (Ni) 24.83%. Fe/Ni levels from AAS data attached to PANI(pot)-Fe/Ni are 1.1912 ppm and 0.8288 ppm; in PANI(gal)-Fe/Ni are 1.2219 ppm and 0.8392 ppm. |
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issn | 2828-271X 2828-2310 |
language | English |
last_indexed | 2024-03-12T23:05:27Z |
publishDate | 2022-02-01 |
publisher | The Center for Science Innovation |
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series | Chemistry and Materials |
spelling | doaj.art-285019fb9039493ca5669532333b29ce2023-07-19T02:26:46ZengThe Center for Science InnovationChemistry and Materials2828-271X2828-23102022-02-0111121720The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni ElectrodepositionMega Sutrisno0Maria Paristiowati1Nailah Fauziyyah2The Centre for Science InnovationUniversitas Negeri JakartaUniversitas Negeri JakartaThe research aims to determine the influence of aniline concentration and deposition time on the characteristics of polyaniline prepared using potentiostatic and galvanostatic electrodeposition methods. FTIR characterization data shows the typical peak of polyaniline in the form of the presence of a quinoid functional group at a wavenumber of 1596.16 cm-1. The typical diffraction pattern of polyaniline using XRD was detected at peaks of 2θ 21.1007o and 23.5995o. Polyaniline formed using SEM has a surface morphology that grows in a stacked and irregular manner and has a high conductance value so that it can be used as a substrate in Fe/Ni electrodeposition. The results of the Fe/Ni electrodeposition process when viewed using SEM cause the polyaniline surface morphology to be covered by a Fe/Ni alloy by having an elemental composition from the EDS test data, are iron (Fe) 68.15% and nickel (Ni) 24.83%. Fe/Ni levels from AAS data attached to PANI(pot)-Fe/Ni are 1.1912 ppm and 0.8288 ppm; in PANI(gal)-Fe/Ni are 1.2219 ppm and 0.8392 ppm.https://piscience.org/index.php/cma/article/view/20electrodepositionfe/nigalvanostaticpolyanilinepotensiostatic |
spellingShingle | Mega Sutrisno Maria Paristiowati Nailah Fauziyyah The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition Chemistry and Materials electrodeposition fe/ni galvanostatic polyaniline potensiostatic |
title | The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition |
title_full | The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition |
title_fullStr | The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition |
title_full_unstemmed | The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition |
title_short | The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition |
title_sort | effects of aniline concentration and deposition time on polyaniline conductance as substrate in fe ni electrodeposition |
topic | electrodeposition fe/ni galvanostatic polyaniline potensiostatic |
url | https://piscience.org/index.php/cma/article/view/20 |
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