The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition

The research aims to determine the influence of aniline concentration and deposition time on the characteristics of polyaniline prepared using potentiostatic and galvanostatic electrodeposition methods. FTIR characterization data shows the typical peak of polyaniline in the form of the presence of a...

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Main Authors: Mega Sutrisno, Maria Paristiowati, Nailah Fauziyyah
Format: Article
Language:English
Published: The Center for Science Innovation 2022-02-01
Series:Chemistry and Materials
Subjects:
Online Access:https://piscience.org/index.php/cma/article/view/20
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author Mega Sutrisno
Maria Paristiowati
Nailah Fauziyyah
author_facet Mega Sutrisno
Maria Paristiowati
Nailah Fauziyyah
author_sort Mega Sutrisno
collection DOAJ
description The research aims to determine the influence of aniline concentration and deposition time on the characteristics of polyaniline prepared using potentiostatic and galvanostatic electrodeposition methods. FTIR characterization data shows the typical peak of polyaniline in the form of the presence of a quinoid functional group at a wavenumber of 1596.16 cm-1. The typical diffraction pattern of polyaniline using XRD was detected at peaks of 2θ 21.1007o and 23.5995o. Polyaniline formed using SEM has a surface morphology that grows in a stacked and irregular manner and has a high conductance value so that it can be used as a substrate in Fe/Ni electrodeposition. The results of the Fe/Ni electrodeposition process when viewed using SEM cause the polyaniline surface morphology to be covered by a Fe/Ni alloy by having an elemental composition from the EDS test data, are iron (Fe) 68.15% and nickel (Ni) 24.83%. Fe/Ni levels from AAS data attached to PANI(pot)-Fe/Ni are 1.1912 ppm and 0.8288 ppm; in PANI(gal)-Fe/Ni are 1.2219 ppm and 0.8392 ppm.
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spelling doaj.art-285019fb9039493ca5669532333b29ce2023-07-19T02:26:46ZengThe Center for Science InnovationChemistry and Materials2828-271X2828-23102022-02-0111121720The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni ElectrodepositionMega Sutrisno0Maria Paristiowati1Nailah Fauziyyah2The Centre for Science InnovationUniversitas Negeri JakartaUniversitas Negeri JakartaThe research aims to determine the influence of aniline concentration and deposition time on the characteristics of polyaniline prepared using potentiostatic and galvanostatic electrodeposition methods. FTIR characterization data shows the typical peak of polyaniline in the form of the presence of a quinoid functional group at a wavenumber of 1596.16 cm-1. The typical diffraction pattern of polyaniline using XRD was detected at peaks of 2θ 21.1007o and 23.5995o. Polyaniline formed using SEM has a surface morphology that grows in a stacked and irregular manner and has a high conductance value so that it can be used as a substrate in Fe/Ni electrodeposition. The results of the Fe/Ni electrodeposition process when viewed using SEM cause the polyaniline surface morphology to be covered by a Fe/Ni alloy by having an elemental composition from the EDS test data, are iron (Fe) 68.15% and nickel (Ni) 24.83%. Fe/Ni levels from AAS data attached to PANI(pot)-Fe/Ni are 1.1912 ppm and 0.8288 ppm; in PANI(gal)-Fe/Ni are 1.2219 ppm and 0.8392 ppm.https://piscience.org/index.php/cma/article/view/20electrodepositionfe/nigalvanostaticpolyanilinepotensiostatic
spellingShingle Mega Sutrisno
Maria Paristiowati
Nailah Fauziyyah
The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition
Chemistry and Materials
electrodeposition
fe/ni
galvanostatic
polyaniline
potensiostatic
title The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition
title_full The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition
title_fullStr The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition
title_full_unstemmed The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition
title_short The Effects of Aniline Concentration and Deposition Time on Polyaniline Conductance as Substrate in Fe/Ni Electrodeposition
title_sort effects of aniline concentration and deposition time on polyaniline conductance as substrate in fe ni electrodeposition
topic electrodeposition
fe/ni
galvanostatic
polyaniline
potensiostatic
url https://piscience.org/index.php/cma/article/view/20
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