Synthesis and characterization of SnO2 thin films using metalorganic precursors

Tetrakis (dimethylamino) tin(IV) (TDMASn) is a metal organic precursor used for fabricating transparent conducting tin oxide (SnO2) thin films via atomic layer deposition process (ALD). This study reported for the first time, a spin coating fabrication process of transparent conducting SnO2 thin fil...

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Main Authors: Emeka Charles Nwanna, Patrick Ehi Imoisili, Tien-Chien Jen
Format: Article
Language:English
Published: Elsevier 2022-07-01
Series:Journal of King Saud University: Science
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S1018364722003044
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author Emeka Charles Nwanna
Patrick Ehi Imoisili
Tien-Chien Jen
author_facet Emeka Charles Nwanna
Patrick Ehi Imoisili
Tien-Chien Jen
author_sort Emeka Charles Nwanna
collection DOAJ
description Tetrakis (dimethylamino) tin(IV) (TDMASn) is a metal organic precursor used for fabricating transparent conducting tin oxide (SnO2) thin films via atomic layer deposition process (ALD). This study reported for the first time, a spin coating fabrication process of transparent conducting SnO2 thin films using TDMASn as the precursor for electrode materials of solar cells substrate. The samples were prepared using sol–gel spin-coating process and annealed at different temperatures to form metastable crystal structured SnO2 thin films. The manufactured thin films consequently underwent X-ray diffraction (XRD), scanning electron microscope (SEM), UV–vis spectroscopy, and resistivity analysis. The XRD analysis certified the films to be of polycrystalline structure, with the SEM results revealing variations in film thicknesses. The UV–vis analysis demonstrated a peak absorption band at 250 nm, while the highest transmittance of 83.2% in the visible range was noticed at the 550 °C sample.
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spelling doaj.art-2875fe7de8c14bd8a6be7ab966f426ab2022-12-22T02:34:09ZengElsevierJournal of King Saud University: Science1018-36472022-07-01345102123Synthesis and characterization of SnO2 thin films using metalorganic precursorsEmeka Charles Nwanna0Patrick Ehi Imoisili1Tien-Chien Jen2Department of Mechanical Engineering Science, Faculty of Engineering and the Built Environment, University of Johannesburg, Auckland 2006, Johannesburg, South AfricaDepartment of Mechanical Engineering Science, Faculty of Engineering and the Built Environment, University of Johannesburg, Auckland 2006, Johannesburg, South AfricaCorresponding author.; Department of Mechanical Engineering Science, Faculty of Engineering and the Built Environment, University of Johannesburg, Auckland 2006, Johannesburg, South AfricaTetrakis (dimethylamino) tin(IV) (TDMASn) is a metal organic precursor used for fabricating transparent conducting tin oxide (SnO2) thin films via atomic layer deposition process (ALD). This study reported for the first time, a spin coating fabrication process of transparent conducting SnO2 thin films using TDMASn as the precursor for electrode materials of solar cells substrate. The samples were prepared using sol–gel spin-coating process and annealed at different temperatures to form metastable crystal structured SnO2 thin films. The manufactured thin films consequently underwent X-ray diffraction (XRD), scanning electron microscope (SEM), UV–vis spectroscopy, and resistivity analysis. The XRD analysis certified the films to be of polycrystalline structure, with the SEM results revealing variations in film thicknesses. The UV–vis analysis demonstrated a peak absorption band at 250 nm, while the highest transmittance of 83.2% in the visible range was noticed at the 550 °C sample.http://www.sciencedirect.com/science/article/pii/S1018364722003044Tin oxideThin filmsSpin-coating
spellingShingle Emeka Charles Nwanna
Patrick Ehi Imoisili
Tien-Chien Jen
Synthesis and characterization of SnO2 thin films using metalorganic precursors
Journal of King Saud University: Science
Tin oxide
Thin films
Spin-coating
title Synthesis and characterization of SnO2 thin films using metalorganic precursors
title_full Synthesis and characterization of SnO2 thin films using metalorganic precursors
title_fullStr Synthesis and characterization of SnO2 thin films using metalorganic precursors
title_full_unstemmed Synthesis and characterization of SnO2 thin films using metalorganic precursors
title_short Synthesis and characterization of SnO2 thin films using metalorganic precursors
title_sort synthesis and characterization of sno2 thin films using metalorganic precursors
topic Tin oxide
Thin films
Spin-coating
url http://www.sciencedirect.com/science/article/pii/S1018364722003044
work_keys_str_mv AT emekacharlesnwanna synthesisandcharacterizationofsno2thinfilmsusingmetalorganicprecursors
AT patrickehiimoisili synthesisandcharacterizationofsno2thinfilmsusingmetalorganicprecursors
AT tienchienjen synthesisandcharacterizationofsno2thinfilmsusingmetalorganicprecursors