CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT
The Cyclic Voltammetric (CV) technique is one of the Ag/AgCl fabrication processes. In electrochemical processes using this CV technique, the microstructure of the surface of a substrate or electrode can affect the scan rate. Thus, this study aims to identify the scan rate effect of the Cl-ion senso...
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| Format: | Article |
| Language: | English |
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Universitas Mercu Buana
2021-08-01
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| Series: | Jurnal Ilmiah SINERGI |
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| Online Access: | https://publikasi.mercubuana.ac.id/index.php/sinergi/article/view/10498 |
| _version_ | 1797712319273238528 |
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| author | Mas'ud Asadullah Sagir Alva Ali Rinaldi Rita Sundari |
| author_facet | Mas'ud Asadullah Sagir Alva Ali Rinaldi Rita Sundari |
| author_sort | Mas'ud Asadullah |
| collection | DOAJ |
| description | The Cyclic Voltammetric (CV) technique is one of the Ag/AgCl fabrication processes. In electrochemical processes using this CV technique, the microstructure of the surface of a substrate or electrode can affect the scan rate. Thus, this study aims to identify the scan rate effect of the Cl-ion sensor fabrication process using the CV technique on the performance of the Cl-ion sensor. First, the CV process was carried out in one cycle to grow the AgCl layer on the Ag surface. Then, this process was carried out at varied scan rates of 20, 40, 60, 80, and 100 mV/s. After completing the Ag/AgCl fabrication process, it was followed by the characterization process, selectivity coefficient test, lifetime test, and validation test to compare the test results of the Cl SPE Ag/AgCl ion sensor with Ag/AgCl commercial. The results showed that the optimum Cl-ion sensor response was obtained at the scan rate of 60 mV/s. Then, based on the validation test, the Cl-ion in the two samples did not show significant differences. Therefore, it indicates that the SPE Ag/AgCl ion sensor has the same performance as the Ag/AgCl commercial. |
| first_indexed | 2024-03-12T07:19:59Z |
| format | Article |
| id | doaj.art-2a2b3b1168214a0e9f66fc5cd34484fd |
| institution | Directory Open Access Journal |
| issn | 1410-2331 2460-1217 |
| language | English |
| last_indexed | 2024-03-12T07:19:59Z |
| publishDate | 2021-08-01 |
| publisher | Universitas Mercu Buana |
| record_format | Article |
| series | Jurnal Ilmiah SINERGI |
| spelling | doaj.art-2a2b3b1168214a0e9f66fc5cd34484fd2023-09-02T22:32:44ZengUniversitas Mercu BuanaJurnal Ilmiah SINERGI1410-23312460-12172021-08-0125335136010.22441/sinergi.2021.3.0124404CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECTMas'ud Asadullah0Sagir Alva1Ali Rinaldi2Rita Sundari3Department of Mechanical Engineering, Faculty of Engineering, Universitas Mercu BuanaDepartment of Mechanical Engineering, Faculty of Engineering, Universitas Mercu BuanaDepartment of Physical Chemistry Division, King Fahd University of Petroleum & MineralsDepartment of Mechanical Engineering, Faculty of Engineering, Universitas Mercu BuanaThe Cyclic Voltammetric (CV) technique is one of the Ag/AgCl fabrication processes. In electrochemical processes using this CV technique, the microstructure of the surface of a substrate or electrode can affect the scan rate. Thus, this study aims to identify the scan rate effect of the Cl-ion sensor fabrication process using the CV technique on the performance of the Cl-ion sensor. First, the CV process was carried out in one cycle to grow the AgCl layer on the Ag surface. Then, this process was carried out at varied scan rates of 20, 40, 60, 80, and 100 mV/s. After completing the Ag/AgCl fabrication process, it was followed by the characterization process, selectivity coefficient test, lifetime test, and validation test to compare the test results of the Cl SPE Ag/AgCl ion sensor with Ag/AgCl commercial. The results showed that the optimum Cl-ion sensor response was obtained at the scan rate of 60 mV/s. Then, based on the validation test, the Cl-ion in the two samples did not show significant differences. Therefore, it indicates that the SPE Ag/AgCl ion sensor has the same performance as the Ag/AgCl commercial.https://publikasi.mercubuana.ac.id/index.php/sinergi/article/view/10498ag/agclchloride ioncyclic voltammetry (cv)ion-selective electrode (ise)screen-printed electrode (spe)scan rate |
| spellingShingle | Mas'ud Asadullah Sagir Alva Ali Rinaldi Rita Sundari CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT Jurnal Ilmiah SINERGI ag/agcl chloride ion cyclic voltammetry (cv) ion-selective electrode (ise) screen-printed electrode (spe) scan rate |
| title | CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT |
| title_full | CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT |
| title_fullStr | CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT |
| title_full_unstemmed | CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT |
| title_short | CHLORIDE SENSOR FABRICATION BASED ON SPE Ag/AgCl THROUGH CYCLIC VOLTAMMETRIC TECHNIQUE: SCAN RATE EFFECT |
| title_sort | chloride sensor fabrication based on spe ag agcl through cyclic voltammetric technique scan rate effect |
| topic | ag/agcl chloride ion cyclic voltammetry (cv) ion-selective electrode (ise) screen-printed electrode (spe) scan rate |
| url | https://publikasi.mercubuana.ac.id/index.php/sinergi/article/view/10498 |
| work_keys_str_mv | AT masudasadullah chloridesensorfabricationbasedonspeagagclthroughcyclicvoltammetrictechniquescanrateeffect AT sagiralva chloridesensorfabricationbasedonspeagagclthroughcyclicvoltammetrictechniquescanrateeffect AT alirinaldi chloridesensorfabricationbasedonspeagagclthroughcyclicvoltammetrictechniquescanrateeffect AT ritasundari chloridesensorfabricationbasedonspeagagclthroughcyclicvoltammetrictechniquescanrateeffect |