Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing Techniques

This study investigated the surface properties of optical sensor layers prepared using sol-gel technology and their response to dissolved NH<sub>3</sub>. A glass substrate was used to fabricate the optical sensor layers. The sol-gel solution was applied to the glass substrate using three...

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Main Authors: Nena Dimitrušev, Polonca Nedeljko, A. F. P. Allwin Mabes Raj, Aleksandra Lobnik
Format: Article
Language:English
Published: MDPI AG 2023-02-01
Series:Chemosensors
Subjects:
Online Access:https://www.mdpi.com/2227-9040/11/2/136
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author Nena Dimitrušev
Polonca Nedeljko
A. F. P. Allwin Mabes Raj
Aleksandra Lobnik
author_facet Nena Dimitrušev
Polonca Nedeljko
A. F. P. Allwin Mabes Raj
Aleksandra Lobnik
author_sort Nena Dimitrušev
collection DOAJ
description This study investigated the surface properties of optical sensor layers prepared using sol-gel technology and their response to dissolved NH<sub>3</sub>. A glass substrate was used to fabricate the optical sensor layers. The sol-gel solution was applied to the glass substrate using three different techniques: spin coating (SC), inkjet printing (IP), and spray coating (SP). In this work, we have attempted to investigate the effects of the different techniques for producing the sensor layers and to determine their response in the presence of ammonia. The surface properties (surface free energy—SFE and surface chemical composition—XPS) and spectral properties (response to ammonia and real-time response) of the prepared optical sensor layers were characterised. The results show that the sensor layers prepared by different techniques have similar SFE and XPS values, but different responses to dissolved NH<sub>3</sub> solution and different responses in real-time measurements (exposure to fresh fish). Sensor layers prepared with a spray coating (SP) are the most responsive, the most sensitive, and have a higher response over time and the biggest colour change compared to SC and IP sensor layers.
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spelling doaj.art-2a3965c937b0471797ad2eab9e1863a02023-11-16T19:46:47ZengMDPI AGChemosensors2227-90402023-02-0111213610.3390/chemosensors11020136Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing TechniquesNena Dimitrušev0Polonca Nedeljko1A. F. P. Allwin Mabes Raj2Aleksandra Lobnik3Messer Slovenija, Jugova ulica 20, 2342 Ruše, SloveniaInstitute for Environmental Protection and Sensors, Beloruska 7, 2000 Maribor, SloveniaInstitute for Environmental Protection and Sensors, Beloruska 7, 2000 Maribor, SloveniaInstitute for Environmental Protection and Sensors, Beloruska 7, 2000 Maribor, SloveniaThis study investigated the surface properties of optical sensor layers prepared using sol-gel technology and their response to dissolved NH<sub>3</sub>. A glass substrate was used to fabricate the optical sensor layers. The sol-gel solution was applied to the glass substrate using three different techniques: spin coating (SC), inkjet printing (IP), and spray coating (SP). In this work, we have attempted to investigate the effects of the different techniques for producing the sensor layers and to determine their response in the presence of ammonia. The surface properties (surface free energy—SFE and surface chemical composition—XPS) and spectral properties (response to ammonia and real-time response) of the prepared optical sensor layers were characterised. The results show that the sensor layers prepared by different techniques have similar SFE and XPS values, but different responses to dissolved NH<sub>3</sub> solution and different responses in real-time measurements (exposure to fresh fish). Sensor layers prepared with a spray coating (SP) are the most responsive, the most sensitive, and have a higher response over time and the biggest colour change compared to SC and IP sensor layers.https://www.mdpi.com/2227-9040/11/2/136optical sensor layers preparationspin coatingspray coatinginkjet printingSFEXPS
spellingShingle Nena Dimitrušev
Polonca Nedeljko
A. F. P. Allwin Mabes Raj
Aleksandra Lobnik
Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing Techniques
Chemosensors
optical sensor layers preparation
spin coating
spray coating
inkjet printing
SFE
XPS
title Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing Techniques
title_full Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing Techniques
title_fullStr Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing Techniques
title_full_unstemmed Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing Techniques
title_short Comparison of Surface and Spectral Properties of Optical Sensor Layers Prepared by Spin/Spray Coating and Printing Techniques
title_sort comparison of surface and spectral properties of optical sensor layers prepared by spin spray coating and printing techniques
topic optical sensor layers preparation
spin coating
spray coating
inkjet printing
SFE
XPS
url https://www.mdpi.com/2227-9040/11/2/136
work_keys_str_mv AT nenadimitrusev comparisonofsurfaceandspectralpropertiesofopticalsensorlayerspreparedbyspinspraycoatingandprintingtechniques
AT poloncanedeljko comparisonofsurfaceandspectralpropertiesofopticalsensorlayerspreparedbyspinspraycoatingandprintingtechniques
AT afpallwinmabesraj comparisonofsurfaceandspectralpropertiesofopticalsensorlayerspreparedbyspinspraycoatingandprintingtechniques
AT aleksandralobnik comparisonofsurfaceandspectralpropertiesofopticalsensorlayerspreparedbyspinspraycoatingandprintingtechniques