High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressing

Two compositions of ZrB2-based ceramic composites containing Si3N4, Al2O3 and Y2O3 have been hot-pressed at different temperatures between 1673 and 1773 K for 60 min in vacuum. The densification behavior of the composites was examined during the sintering process. The microstructures of the composit...

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Main Author: Shuqi Guo and Yutaka Kagawa
Format: Article
Language:English
Published: Taylor & Francis Group 2012-01-01
Series:Science and Technology of Advanced Materials
Online Access:http://dx.doi.org/10.1088/1468-6996/13/4/045007
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author Shuqi Guo and Yutaka Kagawa
author_facet Shuqi Guo and Yutaka Kagawa
author_sort Shuqi Guo and Yutaka Kagawa
collection DOAJ
description Two compositions of ZrB2-based ceramic composites containing Si3N4, Al2O3 and Y2O3 have been hot-pressed at different temperatures between 1673 and 1773 K for 60 min in vacuum. The densification behavior of the composites was examined during the sintering process. The microstructures of the composites were characterized by scanning electron microscopy, and the crystalline phases were identified by x-ray diffraction. The effects of Al2O3 and Y2O3 additives on the densification behavior and flexural strength were assessed. A relative density of ~95% was obtained after sintering at 1723 K or higher temperatures. The microstructures of the composites consisted of (Zr,Y)B2, α-Si3N4 and Y3(Al,Si)5O12 phases. The room-temperature flexural strength increased with the amount of additives and approached 1 GPa.
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spelling doaj.art-2a4824e029444c9fa5772288db3cdba72022-12-21T18:12:03ZengTaylor & Francis GroupScience and Technology of Advanced Materials1468-69961878-55142012-01-01134045007High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressingShuqi Guo and Yutaka KagawaTwo compositions of ZrB2-based ceramic composites containing Si3N4, Al2O3 and Y2O3 have been hot-pressed at different temperatures between 1673 and 1773 K for 60 min in vacuum. The densification behavior of the composites was examined during the sintering process. The microstructures of the composites were characterized by scanning electron microscopy, and the crystalline phases were identified by x-ray diffraction. The effects of Al2O3 and Y2O3 additives on the densification behavior and flexural strength were assessed. A relative density of ~95% was obtained after sintering at 1723 K or higher temperatures. The microstructures of the composites consisted of (Zr,Y)B2, α-Si3N4 and Y3(Al,Si)5O12 phases. The room-temperature flexural strength increased with the amount of additives and approached 1 GPa.http://dx.doi.org/10.1088/1468-6996/13/4/045007
spellingShingle Shuqi Guo and Yutaka Kagawa
High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressing
Science and Technology of Advanced Materials
title High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressing
title_full High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressing
title_fullStr High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressing
title_full_unstemmed High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressing
title_short High-strength zirconium diboride-based ceramic composites consolidated by low-temperature hot pressing
title_sort high strength zirconium diboride based ceramic composites consolidated by low temperature hot pressing
url http://dx.doi.org/10.1088/1468-6996/13/4/045007
work_keys_str_mv AT shuqiguoandyutakakagawa highstrengthzirconiumdiboridebasedceramiccompositesconsolidatedbylowtemperaturehotpressing