Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm Deformation

Evolution of microstructure and hardness in quenched ultrahigh carbon steel Fe-0.85Mo-0.6Si-1.4C by warm compression on a Bähr plastometer-dilatometer at 775 °C and at 0.001 to 1 s<sup>−1</sup> strain rate range is reported. The material was prepared via powder metallurgy: cold pressing...

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Main Authors: Piotr Nikiel, Stefan Szczepanik, Grzegorz Korpała
Format: Article
Language:English
Published: MDPI AG 2021-02-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/11/2/328
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author Piotr Nikiel
Stefan Szczepanik
Grzegorz Korpała
author_facet Piotr Nikiel
Stefan Szczepanik
Grzegorz Korpała
author_sort Piotr Nikiel
collection DOAJ
description Evolution of microstructure and hardness in quenched ultrahigh carbon steel Fe-0.85Mo-0.6Si-1.4C by warm compression on a Bähr plastometer-dilatometer at 775 °C and at 0.001 to 1 s<sup>−1</sup> strain rate range is reported. The material was prepared via powder metallurgy: cold pressing and liquid phase sintering. Independent of strain rate, the initial martenstic microstructure was transformed to ferrite and spheroidized cementite. Strain rate had an effect on size and shape of spheroidized Fe<sub>3</sub>C precipitates: the higher the strain rate, the smaller the precipitates. Morphology of the spheroidized carbides influenced hardness, with the highest hardness, 362 HV10, for strain rate 1 s<sup>−1</sup> and the lowest, 295 HV10, for the lowest strain rate 0.001 s<sup>−1</sup>. Resultant microstructure and ambient temperature mechanical properties were comparable to those of the material that had undergone a fully spheroidizing treatment with increased time and energy consumption, indicating that it can be dispensed with in industrial processing. All our results are consistent with the Hall–Petch relation developed for spheroidized steels.
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spelling doaj.art-2af19596735e4bc1bd36879617bdef792023-12-11T17:01:04ZengMDPI AGMetals2075-47012021-02-0111232810.3390/met11020328Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm DeformationPiotr Nikiel0Stefan Szczepanik1Grzegorz Korpała2Faculty of Metals Engineering and Industrial Computer Science, AGH University of Science and Technology, Av. Mickiewicza 30, 30-059 Kraków, PolandFaculty of Metals Engineering and Industrial Computer Science, AGH University of Science and Technology, Av. Mickiewicza 30, 30-059 Kraków, PolandInstitut für Metallformung, Technische Universität Bergakademie Freiberg, Bernhard-Von-Cotta Str. 4, 09-599 Freiberg, GermanyEvolution of microstructure and hardness in quenched ultrahigh carbon steel Fe-0.85Mo-0.6Si-1.4C by warm compression on a Bähr plastometer-dilatometer at 775 °C and at 0.001 to 1 s<sup>−1</sup> strain rate range is reported. The material was prepared via powder metallurgy: cold pressing and liquid phase sintering. Independent of strain rate, the initial martenstic microstructure was transformed to ferrite and spheroidized cementite. Strain rate had an effect on size and shape of spheroidized Fe<sub>3</sub>C precipitates: the higher the strain rate, the smaller the precipitates. Morphology of the spheroidized carbides influenced hardness, with the highest hardness, 362 HV10, for strain rate 1 s<sup>−1</sup> and the lowest, 295 HV10, for the lowest strain rate 0.001 s<sup>−1</sup>. Resultant microstructure and ambient temperature mechanical properties were comparable to those of the material that had undergone a fully spheroidizing treatment with increased time and energy consumption, indicating that it can be dispensed with in industrial processing. All our results are consistent with the Hall–Petch relation developed for spheroidized steels.https://www.mdpi.com/2075-4701/11/2/328ultrahigh carbon sintered steelwarm workingaccelerated spheroidizationmicrostructurehardness
spellingShingle Piotr Nikiel
Stefan Szczepanik
Grzegorz Korpała
Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm Deformation
Metals
ultrahigh carbon sintered steel
warm working
accelerated spheroidization
microstructure
hardness
title Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm Deformation
title_full Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm Deformation
title_fullStr Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm Deformation
title_full_unstemmed Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm Deformation
title_short Accelerated Spheroidization of Cementite in Sintered Ultrahigh Carbon Steel by Warm Deformation
title_sort accelerated spheroidization of cementite in sintered ultrahigh carbon steel by warm deformation
topic ultrahigh carbon sintered steel
warm working
accelerated spheroidization
microstructure
hardness
url https://www.mdpi.com/2075-4701/11/2/328
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AT stefanszczepanik acceleratedspheroidizationofcementiteinsinteredultrahighcarbonsteelbywarmdeformation
AT grzegorzkorpała acceleratedspheroidizationofcementiteinsinteredultrahighcarbonsteelbywarmdeformation