METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATER
The article presents environmental assessment method and high performance liquid chromatography with solid phase extraction for detection of aldehydes in water. Presents a modernized method gives a number of significant advantages: considerably time procedure reduces sample preparation, compared wit...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
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Peoples’ Friendship University of Russia (RUDN University)
2016-12-01
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| Series: | RUDN Journal of Ecology and Life Safety |
| Subjects: | |
| Online Access: | https://journals.rudn.ru/ecology/article/viewFile/12908/12338 |
| _version_ | 1811343196940140544 |
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| author | P P Kochetkov E V Abramov V V Glebov |
| author_facet | P P Kochetkov E V Abramov V V Glebov |
| author_sort | P P Kochetkov |
| collection | DOAJ |
| description | The article presents environmental assessment method and high performance liquid chromatography with solid phase extraction for detection of aldehydes in water. Presents a modernized method gives a number of significant advantages: considerably time procedure reduces sample preparation, compared with traditional liquid extraction, easy to use and significantly reduces the amount of materials used and reagents in the determination of aldehydes in water. Separation of substances was achieved on reversed-phase C18 column chromatography using a mixture of deionized water and acetonitrile as the mobile phase. Determination of formaldehyde in water was performed at the absorption wavelength of 360 nm. Linearity was achieved in the concentration ranges from 1 to 200 mkg/dm3. Values of repeatability (RSD) presented the method was 15% and the total precision is 10% for control samples at all levels, including lower limit of quantification. |
| first_indexed | 2024-04-13T19:24:18Z |
| format | Article |
| id | doaj.art-2b62207954a8469eabb34446a663e0c5 |
| institution | Directory Open Access Journal |
| issn | 2313-2310 2408-8919 |
| language | English |
| last_indexed | 2024-04-13T19:24:18Z |
| publishDate | 2016-12-01 |
| publisher | Peoples’ Friendship University of Russia (RUDN University) |
| record_format | Article |
| series | RUDN Journal of Ecology and Life Safety |
| spelling | doaj.art-2b62207954a8469eabb34446a663e0c52022-12-22T02:33:24ZengPeoples’ Friendship University of Russia (RUDN University)RUDN Journal of Ecology and Life Safety2313-23102408-89192016-12-01029510312907METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATERP P Kochetkov0E V Abramov1V V Glebov2International Research Center of Health Protection of the Human, animals and environment (IRC «OZOS»)Federal State Budgetary Research Institute «K.I. Scriabin All-Russian Research Institute of Fundamental and Applied Parasitology of Animals and Plants»Peoples’ Friendship University of RussiaThe article presents environmental assessment method and high performance liquid chromatography with solid phase extraction for detection of aldehydes in water. Presents a modernized method gives a number of significant advantages: considerably time procedure reduces sample preparation, compared with traditional liquid extraction, easy to use and significantly reduces the amount of materials used and reagents in the determination of aldehydes in water. Separation of substances was achieved on reversed-phase C18 column chromatography using a mixture of deionized water and acetonitrile as the mobile phase. Determination of formaldehyde in water was performed at the absorption wavelength of 360 nm. Linearity was achieved in the concentration ranges from 1 to 200 mkg/dm3. Values of repeatability (RSD) presented the method was 15% and the total precision is 10% for control samples at all levels, including lower limit of quantification.https://journals.rudn.ru/ecology/article/viewFile/12908/12338environmental assessmenthigh performance liquid chromatographysolid phase extractionformaldehydewaterderivatizationenvironmentsample preparation |
| spellingShingle | P P Kochetkov E V Abramov V V Glebov METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATER RUDN Journal of Ecology and Life Safety environmental assessment high performance liquid chromatography solid phase extraction formaldehyde water derivatization environment sample preparation |
| title | METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATER |
| title_full | METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATER |
| title_fullStr | METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATER |
| title_full_unstemmed | METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATER |
| title_short | METHODS OF THE HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY ON IDENTIFICATION OF ALDEHYDES IN WATER |
| title_sort | methods of the highly effective liquid chromatography on identification of aldehydes in water |
| topic | environmental assessment high performance liquid chromatography solid phase extraction formaldehyde water derivatization environment sample preparation |
| url | https://journals.rudn.ru/ecology/article/viewFile/12908/12338 |
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