AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL

Extracts of black mulberry leaves present phytochemicals such as phenolic compounds and minerals. These substances have been studied because they show several health benefits. In this work we report the influence of drying temperature, infusion temperature and extraction time by means of factorial d...

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Main Authors: Kathlyn Schafranski, Matheus P. Postigo, Luciano Vitali, Gustavo A. Micke, Wagner E. Richter, Eduardo S. Chaves
Format: Article
Language:English
Published: Sociedade Brasileira de Química
Series:Química Nova
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422019004700736&lng=en&tlng=en
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author Kathlyn Schafranski
Matheus P. Postigo
Luciano Vitali
Gustavo A. Micke
Wagner E. Richter
Eduardo S. Chaves
author_facet Kathlyn Schafranski
Matheus P. Postigo
Luciano Vitali
Gustavo A. Micke
Wagner E. Richter
Eduardo S. Chaves
author_sort Kathlyn Schafranski
collection DOAJ
description Extracts of black mulberry leaves present phytochemicals such as phenolic compounds and minerals. These substances have been studied because they show several health benefits. In this work we report the influence of drying temperature, infusion temperature and extraction time by means of factorial design monitoring the total phenolic content (CFT) of aqueous extracts of leaves of Morus nigra L. The concentrations of CFT, flavonoids, flavonols and antioxidant activity of the extracts were determined by spectrophotometry. The identification and quantification of phenolic compounds were performed by LC-ESI-MS / MS. The determination of the mineral concentration in the black mulberry leaves was performed by ICP-MS. The Pareto and surface response graphs suggested that the most efficient extractions occurred for leaves drying at lower temperatures and using higher infusion temperatures, extraction time did not show significant influence. The extracts presented concentration of CFT from 16.96 ± 0.15 to 5.73 ± 0.33 mg GAE g-1. The analyzes by LC-ESI-MS / MS allowed to identify phenolic substances not yet reported in the literature to date. In addition 10 mineral elements were determined in the black mulberry leaves at mg kg-1 concentrations range.
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spelling doaj.art-2b8936440c3245f7930c5487dc291fb12022-12-22T02:05:06ZengSociedade Brasileira de QuímicaQuímica Nova1678-706442773674410.21577/0100-4042.20170389S0100-40422019004700736AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTALKathlyn SchafranskiMatheus P. PostigoLuciano VitaliGustavo A. MickeWagner E. RichterEduardo S. ChavesExtracts of black mulberry leaves present phytochemicals such as phenolic compounds and minerals. These substances have been studied because they show several health benefits. In this work we report the influence of drying temperature, infusion temperature and extraction time by means of factorial design monitoring the total phenolic content (CFT) of aqueous extracts of leaves of Morus nigra L. The concentrations of CFT, flavonoids, flavonols and antioxidant activity of the extracts were determined by spectrophotometry. The identification and quantification of phenolic compounds were performed by LC-ESI-MS / MS. The determination of the mineral concentration in the black mulberry leaves was performed by ICP-MS. The Pareto and surface response graphs suggested that the most efficient extractions occurred for leaves drying at lower temperatures and using higher infusion temperatures, extraction time did not show significant influence. The extracts presented concentration of CFT from 16.96 ± 0.15 to 5.73 ± 0.33 mg GAE g-1. The analyzes by LC-ESI-MS / MS allowed to identify phenolic substances not yet reported in the literature to date. In addition 10 mineral elements were determined in the black mulberry leaves at mg kg-1 concentrations range.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422019004700736&lng=en&tlng=enphenolic compoundsMorus nigrafactorial design
spellingShingle Kathlyn Schafranski
Matheus P. Postigo
Luciano Vitali
Gustavo A. Micke
Wagner E. Richter
Eduardo S. Chaves
AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL
Química Nova
phenolic compounds
Morus nigra
factorial design
title AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL
title_full AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL
title_fullStr AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL
title_full_unstemmed AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL
title_short AVALIAÇÃO DE COMPOSTOS BIOATIVOS E ATIVIDADE ANTIOXIDANTE DE EXTRATOS DE FOLHAS DE AMOREIRA PRETA (Morus nigra L.) UTILIZANDO PLANEJAMENTO EXPERIMENTAL
title_sort avaliacao de compostos bioativos e atividade antioxidante de extratos de folhas de amoreira preta morus nigra l utilizando planejamento experimental
topic phenolic compounds
Morus nigra
factorial design
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422019004700736&lng=en&tlng=en
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