Selected Rheological Properties of RS3/4 Type Resistant Starch
This study was aimed at determining the effect of acetylation degree and crosslinking of retrograded starch with adipic acid on selected rheological properties of prepared pastes and gels. The esterification of retrograded starch allowed obtaining preparations with various degrees of substitution wi...
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Institute of Animal Reproduction and Food Research
2017-12-01
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Series: | Polish Journal of Food and Nutrition Sciences |
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Online Access: | http://www.degruyter.com/view/j/pjfns.2017.67.issue-4/pjfns-2016-0033/pjfns-2016-0033.xml?format=INT |
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author | Kapelko-Żeberska Małgorzata Zięba Tomasz Spychaj Radosław Gryszkin Artur |
author_facet | Kapelko-Żeberska Małgorzata Zięba Tomasz Spychaj Radosław Gryszkin Artur |
author_sort | Kapelko-Żeberska Małgorzata |
collection | DOAJ |
description | This study was aimed at determining the effect of acetylation degree and crosslinking of retrograded starch with adipic acid on selected rheological properties of prepared pastes and gels. The esterification of retrograded starch allowed obtaining preparations with various degrees of substitution with residues of acetic (0.7–11.2 g/100 g) and adipic acids (0.1–0.3 g/100 g). Acetylation and crosslinking caused a decrease in amylose content of the preparations (3–21 g/100 g). Solubility of the preparations in water, in a wide range of variability, was increasing along with an increasing degree of acetylation and with a decreasing degree of crosslinking (19–100 g/100 g). Values of most of the rheological coefficients determined based on the flow curves of the prepared pastes and mechanical spectra of gels (3.5<K<31.5 Pa×sn, 4.2<τ0C<70 Pa, 0.26<tg α<0.57) were increasing in a wide range along with increasing crosslinking of starch. Changes in the rheological properties upon the effect of double modification were not the sum of changes proceeding as a result of single modifications. Instead, interaction of both factors was observed. The conducted modifications enable modelling the properties of produced preparations. |
first_indexed | 2024-12-19T23:31:47Z |
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id | doaj.art-2bf77a5f6ca84e6f9ed3e090b024ccae |
institution | Directory Open Access Journal |
issn | 2083-6007 |
language | English |
last_indexed | 2024-12-19T23:31:47Z |
publishDate | 2017-12-01 |
publisher | Institute of Animal Reproduction and Food Research |
record_format | Article |
series | Polish Journal of Food and Nutrition Sciences |
spelling | doaj.art-2bf77a5f6ca84e6f9ed3e090b024ccae2022-12-21T20:01:43ZengInstitute of Animal Reproduction and Food ResearchPolish Journal of Food and Nutrition Sciences2083-60072017-12-0167429330010.1515/pjfns-2016-0033pjfns-2016-0033Selected Rheological Properties of RS3/4 Type Resistant StarchKapelko-Żeberska Małgorzata0Zięba Tomasz1Spychaj Radosław2Gryszkin Artur3The Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThe Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThe Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThe Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThis study was aimed at determining the effect of acetylation degree and crosslinking of retrograded starch with adipic acid on selected rheological properties of prepared pastes and gels. The esterification of retrograded starch allowed obtaining preparations with various degrees of substitution with residues of acetic (0.7–11.2 g/100 g) and adipic acids (0.1–0.3 g/100 g). Acetylation and crosslinking caused a decrease in amylose content of the preparations (3–21 g/100 g). Solubility of the preparations in water, in a wide range of variability, was increasing along with an increasing degree of acetylation and with a decreasing degree of crosslinking (19–100 g/100 g). Values of most of the rheological coefficients determined based on the flow curves of the prepared pastes and mechanical spectra of gels (3.5<K<31.5 Pa×sn, 4.2<τ0C<70 Pa, 0.26<tg α<0.57) were increasing in a wide range along with increasing crosslinking of starch. Changes in the rheological properties upon the effect of double modification were not the sum of changes proceeding as a result of single modifications. Instead, interaction of both factors was observed. The conducted modifications enable modelling the properties of produced preparations.http://www.degruyter.com/view/j/pjfns.2017.67.issue-4/pjfns-2016-0033/pjfns-2016-0033.xml?format=INTretrograded potato starchacetylated distarch adipaterheological properties |
spellingShingle | Kapelko-Żeberska Małgorzata Zięba Tomasz Spychaj Radosław Gryszkin Artur Selected Rheological Properties of RS3/4 Type Resistant Starch Polish Journal of Food and Nutrition Sciences retrograded potato starch acetylated distarch adipate rheological properties |
title | Selected Rheological Properties of RS3/4 Type Resistant Starch |
title_full | Selected Rheological Properties of RS3/4 Type Resistant Starch |
title_fullStr | Selected Rheological Properties of RS3/4 Type Resistant Starch |
title_full_unstemmed | Selected Rheological Properties of RS3/4 Type Resistant Starch |
title_short | Selected Rheological Properties of RS3/4 Type Resistant Starch |
title_sort | selected rheological properties of rs3 4 type resistant starch |
topic | retrograded potato starch acetylated distarch adipate rheological properties |
url | http://www.degruyter.com/view/j/pjfns.2017.67.issue-4/pjfns-2016-0033/pjfns-2016-0033.xml?format=INT |
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