Selected Rheological Properties of RS3/4 Type Resistant Starch

This study was aimed at determining the effect of acetylation degree and crosslinking of retrograded starch with adipic acid on selected rheological properties of prepared pastes and gels. The esterification of retrograded starch allowed obtaining preparations with various degrees of substitution wi...

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Main Authors: Kapelko-Żeberska Małgorzata, Zięba Tomasz, Spychaj Radosław, Gryszkin Artur
Format: Article
Language:English
Published: Institute of Animal Reproduction and Food Research 2017-12-01
Series:Polish Journal of Food and Nutrition Sciences
Subjects:
Online Access:http://www.degruyter.com/view/j/pjfns.2017.67.issue-4/pjfns-2016-0033/pjfns-2016-0033.xml?format=INT
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author Kapelko-Żeberska Małgorzata
Zięba Tomasz
Spychaj Radosław
Gryszkin Artur
author_facet Kapelko-Żeberska Małgorzata
Zięba Tomasz
Spychaj Radosław
Gryszkin Artur
author_sort Kapelko-Żeberska Małgorzata
collection DOAJ
description This study was aimed at determining the effect of acetylation degree and crosslinking of retrograded starch with adipic acid on selected rheological properties of prepared pastes and gels. The esterification of retrograded starch allowed obtaining preparations with various degrees of substitution with residues of acetic (0.7–11.2 g/100 g) and adipic acids (0.1–0.3 g/100 g). Acetylation and crosslinking caused a decrease in amylose content of the preparations (3–21 g/100 g). Solubility of the preparations in water, in a wide range of variability, was increasing along with an increasing degree of acetylation and with a decreasing degree of crosslinking (19–100 g/100 g). Values of most of the rheological coefficients determined based on the flow curves of the prepared pastes and mechanical spectra of gels (3.5<K<31.5 Pa×sn, 4.2<τ0C<70 Pa, 0.26<tg α<0.57) were increasing in a wide range along with increasing crosslinking of starch. Changes in the rheological properties upon the effect of double modification were not the sum of changes proceeding as a result of single modifications. Instead, interaction of both factors was observed. The conducted modifications enable modelling the properties of produced preparations.
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spelling doaj.art-2bf77a5f6ca84e6f9ed3e090b024ccae2022-12-21T20:01:43ZengInstitute of Animal Reproduction and Food ResearchPolish Journal of Food and Nutrition Sciences2083-60072017-12-0167429330010.1515/pjfns-2016-0033pjfns-2016-0033Selected Rheological Properties of RS3/4 Type Resistant StarchKapelko-Żeberska Małgorzata0Zięba Tomasz1Spychaj Radosław2Gryszkin Artur3The Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThe Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThe Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThe Faculty of Food Science, Wroclaw University of Environmental and Life Science, Chełmońskiego 37/41, 51–630 Wroclaw, PolandThis study was aimed at determining the effect of acetylation degree and crosslinking of retrograded starch with adipic acid on selected rheological properties of prepared pastes and gels. The esterification of retrograded starch allowed obtaining preparations with various degrees of substitution with residues of acetic (0.7–11.2 g/100 g) and adipic acids (0.1–0.3 g/100 g). Acetylation and crosslinking caused a decrease in amylose content of the preparations (3–21 g/100 g). Solubility of the preparations in water, in a wide range of variability, was increasing along with an increasing degree of acetylation and with a decreasing degree of crosslinking (19–100 g/100 g). Values of most of the rheological coefficients determined based on the flow curves of the prepared pastes and mechanical spectra of gels (3.5<K<31.5 Pa×sn, 4.2<τ0C<70 Pa, 0.26<tg α<0.57) were increasing in a wide range along with increasing crosslinking of starch. Changes in the rheological properties upon the effect of double modification were not the sum of changes proceeding as a result of single modifications. Instead, interaction of both factors was observed. The conducted modifications enable modelling the properties of produced preparations.http://www.degruyter.com/view/j/pjfns.2017.67.issue-4/pjfns-2016-0033/pjfns-2016-0033.xml?format=INTretrograded potato starchacetylated distarch adipaterheological properties
spellingShingle Kapelko-Żeberska Małgorzata
Zięba Tomasz
Spychaj Radosław
Gryszkin Artur
Selected Rheological Properties of RS3/4 Type Resistant Starch
Polish Journal of Food and Nutrition Sciences
retrograded potato starch
acetylated distarch adipate
rheological properties
title Selected Rheological Properties of RS3/4 Type Resistant Starch
title_full Selected Rheological Properties of RS3/4 Type Resistant Starch
title_fullStr Selected Rheological Properties of RS3/4 Type Resistant Starch
title_full_unstemmed Selected Rheological Properties of RS3/4 Type Resistant Starch
title_short Selected Rheological Properties of RS3/4 Type Resistant Starch
title_sort selected rheological properties of rs3 4 type resistant starch
topic retrograded potato starch
acetylated distarch adipate
rheological properties
url http://www.degruyter.com/view/j/pjfns.2017.67.issue-4/pjfns-2016-0033/pjfns-2016-0033.xml?format=INT
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AT spychajradosław selectedrheologicalpropertiesofrs34typeresistantstarch
AT gryszkinartur selectedrheologicalpropertiesofrs34typeresistantstarch