Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine System

Sediment is a useful environmental compartment in the evaluation and monitoring of microplastics (i.e., plastic particles between 1 ​μm and 5 ​mm in length) in aquatic environments, since 70% of plastic waste is deposited on the ocean floor, in riverbeds, and on the bottom of estuaries. The techniqu...

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Main Authors: Giovana Teixeira Gimiliani, Milene Fornari, Marcelo Miyada Redígolo, José Oscar Willian Vega Bustillos, Denis Moledo de Souza Abessa, Maria Aparecida Faustino Pires
Format: Article
Language:English
Published: Elsevier 2020-09-01
Series:Case Studies in Chemical and Environmental Engineering
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2666016420300189
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author Giovana Teixeira Gimiliani
Milene Fornari
Marcelo Miyada Redígolo
José Oscar Willian Vega Bustillos
Denis Moledo de Souza Abessa
Maria Aparecida Faustino Pires
author_facet Giovana Teixeira Gimiliani
Milene Fornari
Marcelo Miyada Redígolo
José Oscar Willian Vega Bustillos
Denis Moledo de Souza Abessa
Maria Aparecida Faustino Pires
author_sort Giovana Teixeira Gimiliani
collection DOAJ
description Sediment is a useful environmental compartment in the evaluation and monitoring of microplastics (i.e., plastic particles between 1 ​μm and 5 ​mm in length) in aquatic environments, since 70% of plastic waste is deposited on the ocean floor, in riverbeds, and on the bottom of estuaries. The techniques typically used to separate and quantify microplastics require extensive sample preparation and are often ineffective for estuarine sediment samples. In this study, we present a new method for separating and quantifying microplastics found in estuarine sediment samples. This procedure involves sediment collection, drying, sieving (2.0, 1.0, 0.5 and 0.25 ​mm mesh sizes), and stereomicroscopic examination of the samples retained in each sieve. The results were measured as microplastic abundance (particles g-1 of sediment). This method allows researchers to estimate total microplastic abundance and distribution at the sieve meshes tested, calculate thread/fiber and fragment proportions, and separate microplastic samples for subsequent Py-GC/MS analysis in order to identify their respective compositions. This method was found to be effective in precluding the need for solvents and reducing the amount of time required for sample preparation. For these reasons, this method is more cost-effective and generates less environmental impact than those currently available.
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spelling doaj.art-2c2bd3ab40224ddd98aac30bc9f65ca52022-12-21T20:21:51ZengElsevierCase Studies in Chemical and Environmental Engineering2666-01642020-09-012100020Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine SystemGiovana Teixeira Gimiliani0Milene Fornari1Marcelo Miyada Redígolo2José Oscar Willian Vega Bustillos3Denis Moledo de Souza Abessa4Maria Aparecida Faustino Pires5Nuclear and Energy Research Institute, São Paulo, Brazil; Corresponding author.São Paulo State University, São Vicente, BrazilNuclear and Energy Research Institute, São Paulo, BrazilNuclear and Energy Research Institute, São Paulo, BrazilSão Paulo State University, São Vicente, BrazilNuclear and Energy Research Institute, São Paulo, BrazilSediment is a useful environmental compartment in the evaluation and monitoring of microplastics (i.e., plastic particles between 1 ​μm and 5 ​mm in length) in aquatic environments, since 70% of plastic waste is deposited on the ocean floor, in riverbeds, and on the bottom of estuaries. The techniques typically used to separate and quantify microplastics require extensive sample preparation and are often ineffective for estuarine sediment samples. In this study, we present a new method for separating and quantifying microplastics found in estuarine sediment samples. This procedure involves sediment collection, drying, sieving (2.0, 1.0, 0.5 and 0.25 ​mm mesh sizes), and stereomicroscopic examination of the samples retained in each sieve. The results were measured as microplastic abundance (particles g-1 of sediment). This method allows researchers to estimate total microplastic abundance and distribution at the sieve meshes tested, calculate thread/fiber and fragment proportions, and separate microplastic samples for subsequent Py-GC/MS analysis in order to identify their respective compositions. This method was found to be effective in precluding the need for solvents and reducing the amount of time required for sample preparation. For these reasons, this method is more cost-effective and generates less environmental impact than those currently available.http://www.sciencedirect.com/science/article/pii/S2666016420300189MicroplasticsEstuarine sedimentSievingPy-GC/MS analysis
spellingShingle Giovana Teixeira Gimiliani
Milene Fornari
Marcelo Miyada Redígolo
José Oscar Willian Vega Bustillos
Denis Moledo de Souza Abessa
Maria Aparecida Faustino Pires
Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine System
Case Studies in Chemical and Environmental Engineering
Microplastics
Estuarine sediment
Sieving
Py-GC/MS analysis
title Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine System
title_full Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine System
title_fullStr Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine System
title_full_unstemmed Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine System
title_short Simple and cost-effective method for microplastic quantification in estuarine sediment: A case study of the Santos and São Vicente Estuarine System
title_sort simple and cost effective method for microplastic quantification in estuarine sediment a case study of the santos and sao vicente estuarine system
topic Microplastics
Estuarine sediment
Sieving
Py-GC/MS analysis
url http://www.sciencedirect.com/science/article/pii/S2666016420300189
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