Hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions

Monodispersed tetragonal barium titanate (BaTiO3) nanopowders were synthesized by a convenient hydrothermal route at a low temperature of 200°C in only 24 h. The key point of this method is to promote the generation of ultrafine titanium hydroxide precipitation precursors with the help of absolute e...

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Main Authors: Meng Huaxing, Chen Zhiwu, Lu Zhenya, Wang Xin, Fu Xiaoyi
Format: Article
Language:English
Published: University of Novi Sad 2021-06-01
Series:Processing and Application of Ceramics
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/1820-6131/2021/1820-61312102179M.pdf
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author Meng Huaxing
Chen Zhiwu
Lu Zhenya
Wang Xin
Fu Xiaoyi
author_facet Meng Huaxing
Chen Zhiwu
Lu Zhenya
Wang Xin
Fu Xiaoyi
author_sort Meng Huaxing
collection DOAJ
description Monodispersed tetragonal barium titanate (BaTiO3) nanopowders were synthesized by a convenient hydrothermal route at a low temperature of 200°C in only 24 h. The key point of this method is to promote the generation of ultrafine titanium hydroxide precipitation precursors with the help of absolute ethyl alcohol and ammonia solution during the hydrolysis of Ti(OC4H9)4. The results of X-ray diffraction and Raman spectra show that the as-prepared BaTiO3 nanopowders possess tetragonal-dominant structure. The synthesized tetragonal BaTiO3 nanopowders exhibit relatively uniform size and good dispersity, with the average particle size of 96.1 nm and a tetragonality of 1.0073, which enable broad application prospects in the field of multilayer ceramic capacitors.
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spelling doaj.art-2cae07f18b924469becc400ea2353d992022-12-21T20:00:59ZengUniversity of Novi SadProcessing and Application of Ceramics1820-61312406-10342021-06-0115217918310.2298/PAC2102179MHydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditionsMeng Huaxing0Chen Zhiwu1Lu Zhenya2Wang Xin3Fu Xiaoyi4School of Materials Science and Engineering, South China University of Technology, Guangzhou, ChinaSchool of Materials Science and Engineering, South China University of Technology, Guangzhou, ChinaSchool of Materials Science and Engineering, South China University of Technology, Guangzhou, ChinaSchool of Materials Science and Engineering, South China University of Technology, Guangzhou, ChinaSchool of Materials Science and Engineering, South China University of Technology, Guangzhou, ChinaMonodispersed tetragonal barium titanate (BaTiO3) nanopowders were synthesized by a convenient hydrothermal route at a low temperature of 200°C in only 24 h. The key point of this method is to promote the generation of ultrafine titanium hydroxide precipitation precursors with the help of absolute ethyl alcohol and ammonia solution during the hydrolysis of Ti(OC4H9)4. The results of X-ray diffraction and Raman spectra show that the as-prepared BaTiO3 nanopowders possess tetragonal-dominant structure. The synthesized tetragonal BaTiO3 nanopowders exhibit relatively uniform size and good dispersity, with the average particle size of 96.1 nm and a tetragonality of 1.0073, which enable broad application prospects in the field of multilayer ceramic capacitors.http://www.doiserbia.nb.rs/img/doi/1820-6131/2021/1820-61312102179M.pdftetragonal batio3nanoparticleshydrothermal synthesis
spellingShingle Meng Huaxing
Chen Zhiwu
Lu Zhenya
Wang Xin
Fu Xiaoyi
Hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions
Processing and Application of Ceramics
tetragonal batio3
nanoparticles
hydrothermal synthesis
title Hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions
title_full Hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions
title_fullStr Hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions
title_full_unstemmed Hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions
title_short Hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions
title_sort hydrothermal synthesis of tetragonal barium titanate nanopowders under moderate conditions
topic tetragonal batio3
nanoparticles
hydrothermal synthesis
url http://www.doiserbia.nb.rs/img/doi/1820-6131/2021/1820-61312102179M.pdf
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AT chenzhiwu hydrothermalsynthesisoftetragonalbariumtitanatenanopowdersundermoderateconditions
AT luzhenya hydrothermalsynthesisoftetragonalbariumtitanatenanopowdersundermoderateconditions
AT wangxin hydrothermalsynthesisoftetragonalbariumtitanatenanopowdersundermoderateconditions
AT fuxiaoyi hydrothermalsynthesisoftetragonalbariumtitanatenanopowdersundermoderateconditions