Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron Garnet

In this study, the synthesis and magnetic properties of the rare-earth iron garnets Sm<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, Pr<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, and Er<sub>3</sub>Fe<sub>5</sub>...

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Main Authors: Natalia Tsidaeva, Ahsarbek Nakusov, Spartak Khaimanov, Wei Wang
Format: Article
Language:English
Published: MDPI AG 2021-04-01
Series:Nanomaterials
Subjects:
Online Access:https://www.mdpi.com/2079-4991/11/4/972
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author Natalia Tsidaeva
Ahsarbek Nakusov
Spartak Khaimanov
Wei Wang
author_facet Natalia Tsidaeva
Ahsarbek Nakusov
Spartak Khaimanov
Wei Wang
author_sort Natalia Tsidaeva
collection DOAJ
description In this study, the synthesis and magnetic properties of the rare-earth iron garnets Sm<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, Pr<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, and Er<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub> (in the form of powders and thin films) are reported. According to the composition, shape, and size of particles, the optimal precipitant for the synthesis of Sm<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, Pr<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, and Er<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub> films is an aqueous solution. The parameters for the synthesis of powders and films of the rare-earth iron garnets with micro- and nano-particles have been investigated and selected. The magnetic properties of these materials were studied; field dependencies of the magnetic moment (hysteresis loops) of nanostructured powders of iron garnets of samarium, praseodymium, and erbium in the range of +20 kOe to −20 kOe were obtained. The structural features of the Al<sub>2</sub>O<sub>3</sub> substrate on which the films were formed are also shown.
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spelling doaj.art-2cb82932e2274442a437fe414397a6b82023-11-21T14:57:43ZengMDPI AGNanomaterials2079-49912021-04-0111497210.3390/nano11040972Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron GarnetNatalia Tsidaeva0Ahsarbek Nakusov1Spartak Khaimanov2Wei Wang3Scientific Center “Magnetic Nanostructures”, North Caucasus Mining and Metallurgical Institute, State Technological University, 44, Nikolaeva str., 362021 Vladikavkaz, RussiaScientific Center “Magnetic Nanostructures”, North Caucasus Mining and Metallurgical Institute, State Technological University, 44, Nikolaeva str., 362021 Vladikavkaz, RussiaScientific Center “Magnetic Nanostructures”, North Caucasus Mining and Metallurgical Institute, State Technological University, 44, Nikolaeva str., 362021 Vladikavkaz, RussiaDepartment of Physics and Electronics, School of Mathematics and Physics, Beijing University of Chemical Technology, Beijing 100029, ChinaIn this study, the synthesis and magnetic properties of the rare-earth iron garnets Sm<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, Pr<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, and Er<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub> (in the form of powders and thin films) are reported. According to the composition, shape, and size of particles, the optimal precipitant for the synthesis of Sm<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, Pr<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub>, and Er<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub> films is an aqueous solution. The parameters for the synthesis of powders and films of the rare-earth iron garnets with micro- and nano-particles have been investigated and selected. The magnetic properties of these materials were studied; field dependencies of the magnetic moment (hysteresis loops) of nanostructured powders of iron garnets of samarium, praseodymium, and erbium in the range of +20 kOe to −20 kOe were obtained. The structural features of the Al<sub>2</sub>O<sub>3</sub> substrate on which the films were formed are also shown.https://www.mdpi.com/2079-4991/11/4/972rare-earth iron garnetsmicro/nanostructured powders and filmsX-ray diffraction analysisatomic force microscopyRaman spectroscopysurface topology
spellingShingle Natalia Tsidaeva
Ahsarbek Nakusov
Spartak Khaimanov
Wei Wang
Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron Garnet
Nanomaterials
rare-earth iron garnets
micro/nanostructured powders and films
X-ray diffraction analysis
atomic force microscopy
Raman spectroscopy
surface topology
title Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron Garnet
title_full Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron Garnet
title_fullStr Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron Garnet
title_full_unstemmed Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron Garnet
title_short Hydrothermal Synthesis of Various Magnetic Properties of Controlled Micro/Nanostructured Powders and Films of Rare-Earth Iron Garnet
title_sort hydrothermal synthesis of various magnetic properties of controlled micro nanostructured powders and films of rare earth iron garnet
topic rare-earth iron garnets
micro/nanostructured powders and films
X-ray diffraction analysis
atomic force microscopy
Raman spectroscopy
surface topology
url https://www.mdpi.com/2079-4991/11/4/972
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