Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass Production

The aim of this paper focuses on presenting a recent study that describes the fundamental steps needed to effectively scale-up from lab to mass production parts produced from Al powders reinforced with 0.5 wt% of industrial multiwalled carbon nanotubes (MWCNTs), with mechanical and electrical conduc...

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Main Authors: Roberto Hernández-Maya, Nicolás Antonio Ulloa-Castillo, Oscar Martínez-Romero, Emmanuel Segura-Cárdenas, Alex Elías-Zúñiga
Format: Article
Language:English
Published: MDPI AG 2021-12-01
Series:Nanomaterials
Subjects:
Online Access:https://www.mdpi.com/2079-4991/11/12/3372
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author Roberto Hernández-Maya
Nicolás Antonio Ulloa-Castillo
Oscar Martínez-Romero
Emmanuel Segura-Cárdenas
Alex Elías-Zúñiga
author_facet Roberto Hernández-Maya
Nicolás Antonio Ulloa-Castillo
Oscar Martínez-Romero
Emmanuel Segura-Cárdenas
Alex Elías-Zúñiga
author_sort Roberto Hernández-Maya
collection DOAJ
description The aim of this paper focuses on presenting a recent study that describes the fundamental steps needed to effectively scale-up from lab to mass production parts produced from Al powders reinforced with 0.5 wt% of industrial multiwalled carbon nanotubes (MWCNTs), with mechanical and electrical conductivity properties higher that those measured at the lab scale. The produced material samples were produced via a Spark Plasma Sintering (SPS) process using nanocomposite aluminum powders elaborated with a planetary ball-mill at the lab scale, and high-volume attrition milling equipment in combination with controlled atmosphere sinter hardening furnace equipment, which were used to consolidate the material at the industrial level. Surprisingly, the electrical conductivity and mechanical properties of the samples produced with the reinforced nanocomposite Al powders were made with mass production equipment and were similar or higher than those samples fabricated using metallic powders prepared with ball-mill lab equipment. Experimental measurements show that the hardness and the electrical conductivity properties of the samples fabricated with the mass production Al powders are 48% and 7.5% higher than those of the produced lab samples. This paper elucidates the steps that one needs to follow during the mass production process of reinforced aluminum powders to improve the physical properties of metallic samples consolidated via the SPS process.
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spelling doaj.art-2ce3de9e88a14276a0d91033f367b1ee2023-11-23T09:51:41ZengMDPI AGNanomaterials2079-49912021-12-011112337210.3390/nano11123372Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass ProductionRoberto Hernández-Maya0Nicolás Antonio Ulloa-Castillo1Oscar Martínez-Romero2Emmanuel Segura-Cárdenas3Alex Elías-Zúñiga4Siemens, Research and Development Department, Libramiento Arco Vial Poniente Km 4.2, Santa Catarina 66350, Nuevo León, MexicoTecnologico de Monterrey, Department of Mechanical Engineering and Advanced Materials, School of Engineering and Sciences, Av. Eugenio Garza Sada Sur 2501, Monterrey 64849, Nuevo León, MexicoTecnologico de Monterrey, Department of Mechanical Engineering and Advanced Materials, School of Engineering and Sciences, Av. Eugenio Garza Sada Sur 2501, Monterrey 64849, Nuevo León, MexicoTecnologico de Monterrey, Department of Mechanical Engineering and Advanced Materials, School of Engineering and Sciences, Av. Eugenio Garza Sada Sur 2501, Monterrey 64849, Nuevo León, MexicoTecnologico de Monterrey, Department of Mechanical Engineering and Advanced Materials, School of Engineering and Sciences, Av. Eugenio Garza Sada Sur 2501, Monterrey 64849, Nuevo León, MexicoThe aim of this paper focuses on presenting a recent study that describes the fundamental steps needed to effectively scale-up from lab to mass production parts produced from Al powders reinforced with 0.5 wt% of industrial multiwalled carbon nanotubes (MWCNTs), with mechanical and electrical conductivity properties higher that those measured at the lab scale. The produced material samples were produced via a Spark Plasma Sintering (SPS) process using nanocomposite aluminum powders elaborated with a planetary ball-mill at the lab scale, and high-volume attrition milling equipment in combination with controlled atmosphere sinter hardening furnace equipment, which were used to consolidate the material at the industrial level. Surprisingly, the electrical conductivity and mechanical properties of the samples produced with the reinforced nanocomposite Al powders were made with mass production equipment and were similar or higher than those samples fabricated using metallic powders prepared with ball-mill lab equipment. Experimental measurements show that the hardness and the electrical conductivity properties of the samples fabricated with the mass production Al powders are 48% and 7.5% higher than those of the produced lab samples. This paper elucidates the steps that one needs to follow during the mass production process of reinforced aluminum powders to improve the physical properties of metallic samples consolidated via the SPS process.https://www.mdpi.com/2079-4991/11/12/3372aluminum nanocomposite materialmulti-walled carbon nanotubes (MWCNTs)reinforced Al powdersfrom lab to mass productionscale up processindustrial implementation process
spellingShingle Roberto Hernández-Maya
Nicolás Antonio Ulloa-Castillo
Oscar Martínez-Romero
Emmanuel Segura-Cárdenas
Alex Elías-Zúñiga
Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass Production
Nanomaterials
aluminum nanocomposite material
multi-walled carbon nanotubes (MWCNTs)
reinforced Al powders
from lab to mass production
scale up process
industrial implementation process
title Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass Production
title_full Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass Production
title_fullStr Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass Production
title_full_unstemmed Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass Production
title_short Spark Plasma Sintering of Aluminum Nanocomposite Powders: Recent Strategy to Translate from Lab-Scale to Mass Production
title_sort spark plasma sintering of aluminum nanocomposite powders recent strategy to translate from lab scale to mass production
topic aluminum nanocomposite material
multi-walled carbon nanotubes (MWCNTs)
reinforced Al powders
from lab to mass production
scale up process
industrial implementation process
url https://www.mdpi.com/2079-4991/11/12/3372
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