Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue Dye

Various ZnO nanomaterials such as nanorods, nanoparticles, and nanosheets were synthesized using <i>Salvadora persica</i> leaf extract via the sol–gel method. The prepared nanomaterials possess a large number of nanocavities. The synthesized nanomaterials were characterized using X-ray d...

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Main Authors: Fahad A. Alharthi, Abdulaziz Ali Alghamdi, Asma A. Alothman, Zainab M. Almarhoon, Munairah F. Alsulaiman, Nabil Al-Zaqri
Format: Article
Language:English
Published: MDPI AG 2020-05-01
Series:Crystals
Subjects:
Online Access:https://www.mdpi.com/2073-4352/10/6/441
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author Fahad A. Alharthi
Abdulaziz Ali Alghamdi
Asma A. Alothman
Zainab M. Almarhoon
Munairah F. Alsulaiman
Nabil Al-Zaqri
author_facet Fahad A. Alharthi
Abdulaziz Ali Alghamdi
Asma A. Alothman
Zainab M. Almarhoon
Munairah F. Alsulaiman
Nabil Al-Zaqri
author_sort Fahad A. Alharthi
collection DOAJ
description Various ZnO nanomaterials such as nanorods, nanoparticles, and nanosheets were synthesized using <i>Salvadora persica</i> leaf extract via the sol–gel method. The prepared nanomaterials possess a large number of nanocavities. The synthesized nanomaterials were characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), UV-visible diffuse reflectance studies (UV-DRS), scanning electron microscopy (SEM), and high resolution transmission electron microscopy (HT-TEM), and these nanomaterials were used to test photocatalytic applications for the degradation of highly hazardous methylene blue dye. The degradation efficiency was higher for materials with nanorods and nanosheets with nanocavities; this was due to the presence of the nanocavities, which made the catalyst more sensitive to light absorption. This method offers a green synthesis of different nanomaterials in bulk quantity at low cost.
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spelling doaj.art-2d63a54885444dc59ab827c4f3602e9d2023-11-20T02:19:22ZengMDPI AGCrystals2073-43522020-05-0110644110.3390/cryst10060441Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue DyeFahad A. Alharthi0Abdulaziz Ali Alghamdi1Asma A. Alothman2Zainab M. Almarhoon3Munairah F. Alsulaiman4Nabil Al-Zaqri5Department of Chemistry, College of Science, King Saud University, P.O. Box 2445, Riyadh 11451, Saudi ArabiaDepartment of Chemistry, College of Science, King Saud University, P.O. Box 2445, Riyadh 11451, Saudi ArabiaDepartment of Chemistry, College of Science, King Saud University, P.O. Box 2445, Riyadh 11451, Saudi ArabiaDepartment of Chemistry, College of Science, King Saud University, P.O. Box 2445, Riyadh 11451, Saudi ArabiaDepartment of Chemistry, College of Science, King Saud University, P.O. Box 2445, Riyadh 11451, Saudi ArabiaDepartment of Chemistry, College of Science, King Saud University, P.O. Box 2445, Riyadh 11451, Saudi ArabiaVarious ZnO nanomaterials such as nanorods, nanoparticles, and nanosheets were synthesized using <i>Salvadora persica</i> leaf extract via the sol–gel method. The prepared nanomaterials possess a large number of nanocavities. The synthesized nanomaterials were characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), UV-visible diffuse reflectance studies (UV-DRS), scanning electron microscopy (SEM), and high resolution transmission electron microscopy (HT-TEM), and these nanomaterials were used to test photocatalytic applications for the degradation of highly hazardous methylene blue dye. The degradation efficiency was higher for materials with nanorods and nanosheets with nanocavities; this was due to the presence of the nanocavities, which made the catalyst more sensitive to light absorption. This method offers a green synthesis of different nanomaterials in bulk quantity at low cost.https://www.mdpi.com/2073-4352/10/6/441green synthesissol–gel methodnanorodsnanosheetsnanoparticlesphotocatalytic
spellingShingle Fahad A. Alharthi
Abdulaziz Ali Alghamdi
Asma A. Alothman
Zainab M. Almarhoon
Munairah F. Alsulaiman
Nabil Al-Zaqri
Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue Dye
Crystals
green synthesis
sol–gel method
nanorods
nanosheets
nanoparticles
photocatalytic
title Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue Dye
title_full Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue Dye
title_fullStr Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue Dye
title_full_unstemmed Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue Dye
title_short Green Synthesis of ZnO Nanostructures Using Salvadora Persica Leaf Extract: Applications for Photocatalytic Degradation of Methylene Blue Dye
title_sort green synthesis of zno nanostructures using salvadora persica leaf extract applications for photocatalytic degradation of methylene blue dye
topic green synthesis
sol–gel method
nanorods
nanosheets
nanoparticles
photocatalytic
url https://www.mdpi.com/2073-4352/10/6/441
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