Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)

This study investigates methods for improving the heat resistance of polyvinyl alcohol/alkali lignin foam material (PLFM). Tetraethoxysilane (TEOS) was used as a precursor to prepare PLCFM by a sol-gel method. The PLCFM, prepared with different levels of TEOS, was characterized by Fourier Transform...

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Main Authors: Huachao Luo, Jing Lu, Shixue Ren, Guizhen Fang, Guiquan Jiang
Format: Article
Language:English
Published: North Carolina State University 2015-08-01
Series:BioResources
Subjects:
Online Access:http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_10_3_5961_Silica_Composite_Foam_Material
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author Huachao Luo
Jing Lu
Shixue Ren
Guizhen Fang
Guiquan Jiang
author_facet Huachao Luo
Jing Lu
Shixue Ren
Guizhen Fang
Guiquan Jiang
author_sort Huachao Luo
collection DOAJ
description This study investigates methods for improving the heat resistance of polyvinyl alcohol/alkali lignin foam material (PLFM). Tetraethoxysilane (TEOS) was used as a precursor to prepare PLCFM by a sol-gel method. The PLCFM, prepared with different levels of TEOS, was characterized by Fourier Transform Infrared spectrometry (FTIR), Differential Scanning Calorimetry (DSC), and Thermogravimetric Analysis (TGA). The results indicated that the addition of silica notably improved the heat resistance properties and the initial decomposition temperature of the foam and exhibited good biocompatibility with the polyvinyl alcohol (PVOH) and alkali lignin. The melting temperature of the PLCFM also increased significantly. It reached 268 °C when the silica content was 10%, which was 110 °C higher than that of PLFM. The mechanical properties were also improved to 27.42 MPa.
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spelling doaj.art-2d7cd56c48744b4cacb863908f15e9b02022-12-21T19:57:35ZengNorth Carolina State UniversityBioResources1930-21261930-21262015-08-011035961597310.15376/biores.10.3.5961-5973Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)Huachao Luo0Jing Lu1Shixue Ren2Guizhen Fang3Guiquan Jiang4Northeast Forestry University; ChinaNortheast Forestry University; ChinaNortheast Forestry University; ChinaNortheast Forestry University; ChinaBeihua University; ChinaThis study investigates methods for improving the heat resistance of polyvinyl alcohol/alkali lignin foam material (PLFM). Tetraethoxysilane (TEOS) was used as a precursor to prepare PLCFM by a sol-gel method. The PLCFM, prepared with different levels of TEOS, was characterized by Fourier Transform Infrared spectrometry (FTIR), Differential Scanning Calorimetry (DSC), and Thermogravimetric Analysis (TGA). The results indicated that the addition of silica notably improved the heat resistance properties and the initial decomposition temperature of the foam and exhibited good biocompatibility with the polyvinyl alcohol (PVOH) and alkali lignin. The melting temperature of the PLCFM also increased significantly. It reached 268 °C when the silica content was 10%, which was 110 °C higher than that of PLFM. The mechanical properties were also improved to 27.42 MPa.http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_10_3_5961_Silica_Composite_Foam_MaterialAlkali ligninPolyvinyl alcoholThermal propertiesSol-gel methodsFunctional composite
spellingShingle Huachao Luo
Jing Lu
Shixue Ren
Guizhen Fang
Guiquan Jiang
Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)
BioResources
Alkali lignin
Polyvinyl alcohol
Thermal properties
Sol-gel methods
Functional composite
title Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)
title_full Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)
title_fullStr Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)
title_full_unstemmed Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)
title_short Studies of Polyvinyl Alcohol/Alkali Lignin/Silica Composite Foam Material (PLCFM)
title_sort studies of polyvinyl alcohol alkali lignin silica composite foam material plcfm
topic Alkali lignin
Polyvinyl alcohol
Thermal properties
Sol-gel methods
Functional composite
url http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_10_3_5961_Silica_Composite_Foam_Material
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AT jinglu studiesofpolyvinylalcoholalkaliligninsilicacompositefoammaterialplcfm
AT shixueren studiesofpolyvinylalcoholalkaliligninsilicacompositefoammaterialplcfm
AT guizhenfang studiesofpolyvinylalcoholalkaliligninsilicacompositefoammaterialplcfm
AT guiquanjiang studiesofpolyvinylalcoholalkaliligninsilicacompositefoammaterialplcfm