Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain Inspection

By testing the parameters of graphite digestion instrument, the effects of graphite digestion method and microwave digestion method on the determination of total arsenic in rice were analyzed and compared.The results showed that the RSD of rice standard sample digested by graphite digestion method...

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Main Authors: HU Xue-chun, REN Ling-yun, WANG Li-juan, JIN Zeng-wei, WU Zhen-zhen, ZHAO Ying, WANG Rui-jie
Format: Article
Language:English
Published: Academy of National Food and Strategic Reserves Administration 2021-01-01
Series:Liang you shipin ke-ji
Subjects:
Online Access:http://lyspkj.ijournal.cn/lyspkj/article/abstract/20210123?st=article_issue
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author HU Xue-chun
REN Ling-yun
WANG Li-juan
JIN Zeng-wei
WU Zhen-zhen
ZHAO Ying
WANG Rui-jie
author_facet HU Xue-chun
REN Ling-yun
WANG Li-juan
JIN Zeng-wei
WU Zhen-zhen
ZHAO Ying
WANG Rui-jie
author_sort HU Xue-chun
collection DOAJ
description By testing the parameters of graphite digestion instrument, the effects of graphite digestion method and microwave digestion method on the determination of total arsenic in rice were analyzed and compared.The results showed that the RSD of rice standard sample digested by graphite digestion method was 5.25%~6.86%, and the relative error between the test result and the standard value was 5.66%~7.55%. The RSD of rice standard sample digested by microwave digestion method was 8.67%~12.26%, and the relative error was 17.96%~21.7%. The accuracy and precision of graphite digestion method are higher than that of microwave digestion method.
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spelling doaj.art-2de682219d7a4adbbf555cc4bc9ccaaa2023-06-07T06:15:24ZengAcademy of National Food and Strategic Reserves AdministrationLiang you shipin ke-ji1007-75612021-01-0129116817210.16210/j.cnki.1007-7561.2021.01.022Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain InspectionHU Xue-chun0REN Ling-yun1WANG Li-juan2JIN Zeng-wei3WU Zhen-zhen4ZHAO Ying5 WANG Rui-jie6Shandong Grain and Oil Testing Center, Jinan, Shandong 250100, ChinaShandong Grain and Oil Testing Center, Jinan, Shandong 250100, ChinaShanxi Grain Quality Monitoring Center, Taiyuan, Shanxi 030024, ChinaShandong Grain and Oil Testing Center, Jinan, Shandong 250100, ChinaShandong Grain and Oil Testing Center, Jinan, Shandong 250100, ChinaShandong Grain and Oil Testing Center, Jinan, Shandong 250100, ChinaShandong Grain and Oil Testing Center, Jinan, Shandong 250100, China By testing the parameters of graphite digestion instrument, the effects of graphite digestion method and microwave digestion method on the determination of total arsenic in rice were analyzed and compared.The results showed that the RSD of rice standard sample digested by graphite digestion method was 5.25%~6.86%, and the relative error between the test result and the standard value was 5.66%~7.55%. The RSD of rice standard sample digested by microwave digestion method was 8.67%~12.26%, and the relative error was 17.96%~21.7%. The accuracy and precision of graphite digestion method are higher than that of microwave digestion method.http://lyspkj.ijournal.cn/lyspkj/article/abstract/20210123?st=article_issuedigestgraphite digestionmicrowave digestiongrainriceinspecttotal arsenic
spellingShingle HU Xue-chun
REN Ling-yun
WANG Li-juan
JIN Zeng-wei
WU Zhen-zhen
ZHAO Ying
WANG Rui-jie
Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain Inspection
Liang you shipin ke-ji
digest
graphite digestion
microwave digestion
grain
rice
inspect
total arsenic
title Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain Inspection
title_full Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain Inspection
title_fullStr Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain Inspection
title_full_unstemmed Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain Inspection
title_short Application of Automatic Graphite Digestion Method in Inspection of Total Arsenic in Grain Inspection
title_sort application of automatic graphite digestion method in inspection of total arsenic in grain inspection
topic digest
graphite digestion
microwave digestion
grain
rice
inspect
total arsenic
url http://lyspkj.ijournal.cn/lyspkj/article/abstract/20210123?st=article_issue
work_keys_str_mv AT huxuechun applicationofautomaticgraphitedigestionmethodininspectionoftotalarsenicingraininspection
AT renlingyun applicationofautomaticgraphitedigestionmethodininspectionoftotalarsenicingraininspection
AT wanglijuan applicationofautomaticgraphitedigestionmethodininspectionoftotalarsenicingraininspection
AT jinzengwei applicationofautomaticgraphitedigestionmethodininspectionoftotalarsenicingraininspection
AT wuzhenzhen applicationofautomaticgraphitedigestionmethodininspectionoftotalarsenicingraininspection
AT zhaoying applicationofautomaticgraphitedigestionmethodininspectionoftotalarsenicingraininspection
AT wangruijie applicationofautomaticgraphitedigestionmethodininspectionoftotalarsenicingraininspection