4-(4-Pyridyl)pyridinium perchlorate methanol solvate
In the cation of the title hydrated molecular salt, C10H9N2+·ClO4−·CH3OH, the dihedral angle formed by the pyridine rings is 28.82 (15)°. The crystal structure is stabilized by intermolecular N—H...O and O&#8212...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2010-05-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810012985 |
| _version_ | 1818791663147941888 |
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| author | Yu-Hua Gao De-Ming Wu |
| author_facet | Yu-Hua Gao De-Ming Wu |
| author_sort | Yu-Hua Gao |
| collection | DOAJ |
| description | In the cation of the title hydrated molecular salt, C10H9N2+·ClO4−·CH3OH, the dihedral angle formed by the pyridine rings is 28.82 (15)°. The crystal structure is stabilized by intermolecular N—H...O and O—H...N hydrogen bonds and π–π stacking interactions, with centroid-to-centroid distances of 3.5913 (7) and 3.6526 (7) Å. Three O atoms of the perchlorate anion are disordered over two positions with refined occupancy factors of 0.649 (7):0.351 (7). |
| first_indexed | 2024-12-18T15:14:56Z |
| format | Article |
| id | doaj.art-2e23b52ee1484de18cb15736a871722c |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-18T15:14:56Z |
| publishDate | 2010-05-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-2e23b52ee1484de18cb15736a871722c2022-12-21T21:03:33ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-05-01665o1068o106810.1107/S16005368100129854-(4-Pyridyl)pyridinium perchlorate methanol solvateYu-Hua GaoDe-Ming WuIn the cation of the title hydrated molecular salt, C10H9N2+·ClO4−·CH3OH, the dihedral angle formed by the pyridine rings is 28.82 (15)°. The crystal structure is stabilized by intermolecular N—H...O and O—H...N hydrogen bonds and π–π stacking interactions, with centroid-to-centroid distances of 3.5913 (7) and 3.6526 (7) Å. Three O atoms of the perchlorate anion are disordered over two positions with refined occupancy factors of 0.649 (7):0.351 (7).http://scripts.iucr.org/cgi-bin/paper?S1600536810012985 |
| spellingShingle | Yu-Hua Gao De-Ming Wu 4-(4-Pyridyl)pyridinium perchlorate methanol solvate Acta Crystallographica Section E |
| title | 4-(4-Pyridyl)pyridinium perchlorate methanol solvate |
| title_full | 4-(4-Pyridyl)pyridinium perchlorate methanol solvate |
| title_fullStr | 4-(4-Pyridyl)pyridinium perchlorate methanol solvate |
| title_full_unstemmed | 4-(4-Pyridyl)pyridinium perchlorate methanol solvate |
| title_short | 4-(4-Pyridyl)pyridinium perchlorate methanol solvate |
| title_sort | 4 4 pyridyl pyridinium perchlorate methanol solvate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810012985 |
| work_keys_str_mv | AT yuhuagao 44pyridylpyridiniumperchloratemethanolsolvate AT demingwu 44pyridylpyridiniumperchloratemethanolsolvate |