Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent
Abstract The objective of this work was to evaluate the efficacy of ethyl acetate as a solvent in the extraction of macauba kernel oil (MKO) using ultrasonic-assisted extraction (UAE). It was shown that more MKO oil could be extracted with the use of larger amounts of solvent, higher temperatures a...
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Format: | Article |
Language: | English |
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Instituto de Tecnologia de Alimentos (ITAL)
2019-04-01
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Series: | Brazilian Journal of Food Technology |
Subjects: | |
Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1981-67232019000100410&lng=en&tlng=en |
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author | Ana Claudia Santos da Rosa Natália Stevanato Isabela Iwassa Vitor Augusto dos Santos Garcia Camila da Silva |
author_facet | Ana Claudia Santos da Rosa Natália Stevanato Isabela Iwassa Vitor Augusto dos Santos Garcia Camila da Silva |
author_sort | Ana Claudia Santos da Rosa |
collection | DOAJ |
description | Abstract The objective of this work was to evaluate the efficacy of ethyl acetate as a solvent in the extraction of macauba kernel oil (MKO) using ultrasonic-assisted extraction (UAE). It was shown that more MKO oil could be extracted with the use of larger amounts of solvent, higher temperatures and longer extraction times. Thus the maximum oil yield (40.61%) was obtained by UAE at 60 °C for 45 min, using a solvent to kernel ratio of 12 (mL g-1), obtaining a higher yield than that obtained with n-hexane under the same experimental conditions. UAE was favorable for this oil extraction (p < 0.05), presenting a yield close to that reported for classical extraction but with a shorter extraction time and smaller solvent volume. Lauric acid corresponded to ~44% of the MKO composition. The oils presented low free fatty acid contents (<0.80% wt), and the phytosterols, campesterol and β-sitosterol, were identified in the MKO with higher levels in the oil obtained by UAE. |
first_indexed | 2024-04-12T18:46:06Z |
format | Article |
id | doaj.art-2f435ec570c54ec699c3684da5c69146 |
institution | Directory Open Access Journal |
issn | 1981-6723 |
language | English |
last_indexed | 2024-04-12T18:46:06Z |
publishDate | 2019-04-01 |
publisher | Instituto de Tecnologia de Alimentos (ITAL) |
record_format | Article |
series | Brazilian Journal of Food Technology |
spelling | doaj.art-2f435ec570c54ec699c3684da5c691462022-12-22T03:20:37ZengInstituto de Tecnologia de Alimentos (ITAL)Brazilian Journal of Food Technology1981-67232019-04-0122010.1590/1981-6723.19518S1981-67232019000100410Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solventAna Claudia Santos da RosaNatália StevanatoIsabela IwassaVitor Augusto dos Santos GarciaCamila da SilvaAbstract The objective of this work was to evaluate the efficacy of ethyl acetate as a solvent in the extraction of macauba kernel oil (MKO) using ultrasonic-assisted extraction (UAE). It was shown that more MKO oil could be extracted with the use of larger amounts of solvent, higher temperatures and longer extraction times. Thus the maximum oil yield (40.61%) was obtained by UAE at 60 °C for 45 min, using a solvent to kernel ratio of 12 (mL g-1), obtaining a higher yield than that obtained with n-hexane under the same experimental conditions. UAE was favorable for this oil extraction (p < 0.05), presenting a yield close to that reported for classical extraction but with a shorter extraction time and smaller solvent volume. Lauric acid corresponded to ~44% of the MKO composition. The oils presented low free fatty acid contents (<0.80% wt), and the phytosterols, campesterol and β-sitosterol, were identified in the MKO with higher levels in the oil obtained by UAE.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1981-67232019000100410&lng=en&tlng=enEthyl acetateUltrasoundMacauba kernelSolventFatty acidsClassic extraction |
spellingShingle | Ana Claudia Santos da Rosa Natália Stevanato Isabela Iwassa Vitor Augusto dos Santos Garcia Camila da Silva Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent Brazilian Journal of Food Technology Ethyl acetate Ultrasound Macauba kernel Solvent Fatty acids Classic extraction |
title | Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent |
title_full | Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent |
title_fullStr | Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent |
title_full_unstemmed | Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent |
title_short | Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent |
title_sort | obtaining oil from macauba kernels by ultrasound assisted extraction using ethyl acetate as the solvent |
topic | Ethyl acetate Ultrasound Macauba kernel Solvent Fatty acids Classic extraction |
url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1981-67232019000100410&lng=en&tlng=en |
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