Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent

Abstract The objective of this work was to evaluate the efficacy of ethyl acetate as a solvent in the extraction of macauba kernel oil (MKO) using ultrasonic-assisted extraction (UAE). It was shown that more MKO oil could be extracted with the use of larger amounts of solvent, higher temperatures a...

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Main Authors: Ana Claudia Santos da Rosa, Natália Stevanato, Isabela Iwassa, Vitor Augusto dos Santos Garcia, Camila da Silva
Format: Article
Language:English
Published: Instituto de Tecnologia de Alimentos (ITAL) 2019-04-01
Series:Brazilian Journal of Food Technology
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1981-67232019000100410&lng=en&tlng=en
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author Ana Claudia Santos da Rosa
Natália Stevanato
Isabela Iwassa
Vitor Augusto dos Santos Garcia
Camila da Silva
author_facet Ana Claudia Santos da Rosa
Natália Stevanato
Isabela Iwassa
Vitor Augusto dos Santos Garcia
Camila da Silva
author_sort Ana Claudia Santos da Rosa
collection DOAJ
description Abstract The objective of this work was to evaluate the efficacy of ethyl acetate as a solvent in the extraction of macauba kernel oil (MKO) using ultrasonic-assisted extraction (UAE). It was shown that more MKO oil could be extracted with the use of larger amounts of solvent, higher temperatures and longer extraction times. Thus the maximum oil yield (40.61%) was obtained by UAE at 60 °C for 45 min, using a solvent to kernel ratio of 12 (mL g-1), obtaining a higher yield than that obtained with n-hexane under the same experimental conditions. UAE was favorable for this oil extraction (p < 0.05), presenting a yield close to that reported for classical extraction but with a shorter extraction time and smaller solvent volume. Lauric acid corresponded to ~44% of the MKO composition. The oils presented low free fatty acid contents (<0.80% wt), and the phytosterols, campesterol and β-sitosterol, were identified in the MKO with higher levels in the oil obtained by UAE.
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spelling doaj.art-2f435ec570c54ec699c3684da5c691462022-12-22T03:20:37ZengInstituto de Tecnologia de Alimentos (ITAL)Brazilian Journal of Food Technology1981-67232019-04-0122010.1590/1981-6723.19518S1981-67232019000100410Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solventAna Claudia Santos da RosaNatália StevanatoIsabela IwassaVitor Augusto dos Santos GarciaCamila da SilvaAbstract The objective of this work was to evaluate the efficacy of ethyl acetate as a solvent in the extraction of macauba kernel oil (MKO) using ultrasonic-assisted extraction (UAE). It was shown that more MKO oil could be extracted with the use of larger amounts of solvent, higher temperatures and longer extraction times. Thus the maximum oil yield (40.61%) was obtained by UAE at 60 °C for 45 min, using a solvent to kernel ratio of 12 (mL g-1), obtaining a higher yield than that obtained with n-hexane under the same experimental conditions. UAE was favorable for this oil extraction (p < 0.05), presenting a yield close to that reported for classical extraction but with a shorter extraction time and smaller solvent volume. Lauric acid corresponded to ~44% of the MKO composition. The oils presented low free fatty acid contents (<0.80% wt), and the phytosterols, campesterol and β-sitosterol, were identified in the MKO with higher levels in the oil obtained by UAE.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1981-67232019000100410&lng=en&tlng=enEthyl acetateUltrasoundMacauba kernelSolventFatty acidsClassic extraction
spellingShingle Ana Claudia Santos da Rosa
Natália Stevanato
Isabela Iwassa
Vitor Augusto dos Santos Garcia
Camila da Silva
Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent
Brazilian Journal of Food Technology
Ethyl acetate
Ultrasound
Macauba kernel
Solvent
Fatty acids
Classic extraction
title Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent
title_full Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent
title_fullStr Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent
title_full_unstemmed Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent
title_short Obtaining oil from macauba kernels by ultrasound-assisted extraction using ethyl acetate as the solvent
title_sort obtaining oil from macauba kernels by ultrasound assisted extraction using ethyl acetate as the solvent
topic Ethyl acetate
Ultrasound
Macauba kernel
Solvent
Fatty acids
Classic extraction
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1981-67232019000100410&lng=en&tlng=en
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