Morphology Characterization of Electrospun Polystyrene Membranes

The polymeric solution concentration is one of the most critical factors in forming of fibers in electrospinning technology. In this study, various polymeric concentrations of thermoplastic polystyrene are used. At the same time, keeping the other electrospinning process operating parameters (such a...

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Main Authors: Ahmed Oleiwi, Akram Jabur, Qusay Alsalhy, Suriani Abu Bakar
Format: Article
Language:English
Published: University of Technology, Baghdad 2024-02-01
Series:Journal of Applied Sciences and Nanotechnology
Subjects:
Online Access:https://jasn.uotechnology.edu.iq/article_24087_3b84820d8038bf94869ddd27d6735218.pdf
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author Ahmed Oleiwi
Akram Jabur
Qusay Alsalhy
Suriani Abu Bakar
author_facet Ahmed Oleiwi
Akram Jabur
Qusay Alsalhy
Suriani Abu Bakar
author_sort Ahmed Oleiwi
collection DOAJ
description The polymeric solution concentration is one of the most critical factors in forming of fibers in electrospinning technology. In this study, various polymeric concentrations of thermoplastic polystyrene are used. At the same time, keeping the other electrospinning process operating parameters (such as flow rate, voltage, capillary to collector distance), solution parameters (such as solution conductivity and molecular weight), and environmental conditions (such as temperature and humidity) constant. Field emission scanning electron microscopy was used to investigate the morphological changes that took place on the surface of the fibres and determine the typical fibre diameter. It was found that as the concentration of polystyrene increased from 15% to 30%, the average pore size increased from (0.5µm and 0.44µm) to (2.7µm and 2.6µm). The FT-IR demonstrated the main chemical bonds in polystyrene membranes and the change in peak intensity caused by increasing the polymeric concentration. According to contact angle measurements, which examine the change in hydrophobic properties, the hydrophobicity of membranes decreases as the water contact angle falls from 135 to 116 with increasing the polymeric concentration from 15% to 30%.
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spelling doaj.art-2f6da3bfcb2643f4844646c79a64110f2024-03-14T04:11:38ZengUniversity of Technology, BaghdadJournal of Applied Sciences and Nanotechnology2788-68672024-02-01411810.53293/jasn.2023.7010.122524087Morphology Characterization of Electrospun Polystyrene MembranesAhmed Oleiwi0Akram Jabur1Qusay Alsalhy2Suriani Abu Bakar3College of Engineering / Wasit University – IraqDepartment of Materials Engineering – University of Technology – IraqDepartment of Chemical Engineering – University of Technology – IraqNanotechnology Research Centre, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris – MalaysiaThe polymeric solution concentration is one of the most critical factors in forming of fibers in electrospinning technology. In this study, various polymeric concentrations of thermoplastic polystyrene are used. At the same time, keeping the other electrospinning process operating parameters (such as flow rate, voltage, capillary to collector distance), solution parameters (such as solution conductivity and molecular weight), and environmental conditions (such as temperature and humidity) constant. Field emission scanning electron microscopy was used to investigate the morphological changes that took place on the surface of the fibres and determine the typical fibre diameter. It was found that as the concentration of polystyrene increased from 15% to 30%, the average pore size increased from (0.5µm and 0.44µm) to (2.7µm and 2.6µm). The FT-IR demonstrated the main chemical bonds in polystyrene membranes and the change in peak intensity caused by increasing the polymeric concentration. According to contact angle measurements, which examine the change in hydrophobic properties, the hydrophobicity of membranes decreases as the water contact angle falls from 135 to 116 with increasing the polymeric concentration from 15% to 30%.https://jasn.uotechnology.edu.iq/article_24087_3b84820d8038bf94869ddd27d6735218.pdfelectrospinning techniquenano-fibers membranesfe-sem
spellingShingle Ahmed Oleiwi
Akram Jabur
Qusay Alsalhy
Suriani Abu Bakar
Morphology Characterization of Electrospun Polystyrene Membranes
Journal of Applied Sciences and Nanotechnology
electrospinning technique
nano-fibers membranes
fe-sem
title Morphology Characterization of Electrospun Polystyrene Membranes
title_full Morphology Characterization of Electrospun Polystyrene Membranes
title_fullStr Morphology Characterization of Electrospun Polystyrene Membranes
title_full_unstemmed Morphology Characterization of Electrospun Polystyrene Membranes
title_short Morphology Characterization of Electrospun Polystyrene Membranes
title_sort morphology characterization of electrospun polystyrene membranes
topic electrospinning technique
nano-fibers membranes
fe-sem
url https://jasn.uotechnology.edu.iq/article_24087_3b84820d8038bf94869ddd27d6735218.pdf
work_keys_str_mv AT ahmedoleiwi morphologycharacterizationofelectrospunpolystyrenemembranes
AT akramjabur morphologycharacterizationofelectrospunpolystyrenemembranes
AT qusayalsalhy morphologycharacterizationofelectrospunpolystyrenemembranes
AT surianiabubakar morphologycharacterizationofelectrospunpolystyrenemembranes