Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测)
采用新型抑制器,对乙酸根、甲酸根、丙酮酸根、氟离子、山梨酸根、苯甲酸根、硝酸根、磷酸根、酒石酸根、硫酸根、草酸根、柠檬酸根在流速为1.5 ml/min,碳酸钠/碳酸氢钠梯度淋洗液分离,抑制电导检测得到理想的分离效果和较高的灵敏度.乙酸根、甲酸根、丙酮酸根、氯离子、山梨酸根、苯甲酸根、硝酸根、磷酸根、酒石酸根、硫酸根、草酸根、柠檬酸根检测限分别为0.45 μg/ml,0.27 μg/ml,0.60 μg/ml,0.42 μg/ml,0.72 μg/ml,2.16 μg/ml,3.66μg/ml,0.33 μg/ml,1.44 μg/ml,1.53 μg/ml,1.23 μg/ml,0.45 μg...
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Format: | Article |
Language: | zho |
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Zhejiang University Press
2003-03-01
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Series: | Zhejiang Daxue xuebao. Lixue ban |
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Online Access: | https://doi.org/zjup/1008-9497.2003.30.2.184-187 |
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author | ZHANGPei-min(张培敏) ZHUYan(朱岩) XUYu(徐育) |
author_facet | ZHANGPei-min(张培敏) ZHUYan(朱岩) XUYu(徐育) |
author_sort | ZHANGPei-min(张培敏) |
collection | DOAJ |
description | 采用新型抑制器,对乙酸根、甲酸根、丙酮酸根、氟离子、山梨酸根、苯甲酸根、硝酸根、磷酸根、酒石酸根、硫酸根、草酸根、柠檬酸根在流速为1.5 ml/min,碳酸钠/碳酸氢钠梯度淋洗液分离,抑制电导检测得到理想的分离效果和较高的灵敏度.乙酸根、甲酸根、丙酮酸根、氯离子、山梨酸根、苯甲酸根、硝酸根、磷酸根、酒石酸根、硫酸根、草酸根、柠檬酸根检测限分别为0.45 μg/ml,0.27 μg/ml,0.60 μg/ml,0.42 μg/ml,0.72 μg/ml,2.16 μg/ml,3.66μg/ml,0.33 μg/ml,1.44 μg/ml,1.53 μg/ml,1.23 μg/ml,0.45 μg/ml(S/N=3),具有良好的线性关系和重现性.对饮料样品进行测定,结果令人满意. |
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institution | Directory Open Access Journal |
issn | 1008-9497 |
language | zho |
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publishDate | 2003-03-01 |
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spelling | doaj.art-3050f4ba1bc04ef19a1d5ef961099bd92024-03-29T01:58:19ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972003-03-01302184187zjup/1008-9497.2003.30.2.184-187Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测)ZHANGPei-min(张培敏)0ZHUYan(朱岩)1XUYu(徐育)2Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)采用新型抑制器,对乙酸根、甲酸根、丙酮酸根、氟离子、山梨酸根、苯甲酸根、硝酸根、磷酸根、酒石酸根、硫酸根、草酸根、柠檬酸根在流速为1.5 ml/min,碳酸钠/碳酸氢钠梯度淋洗液分离,抑制电导检测得到理想的分离效果和较高的灵敏度.乙酸根、甲酸根、丙酮酸根、氯离子、山梨酸根、苯甲酸根、硝酸根、磷酸根、酒石酸根、硫酸根、草酸根、柠檬酸根检测限分别为0.45 μg/ml,0.27 μg/ml,0.60 μg/ml,0.42 μg/ml,0.72 μg/ml,2.16 μg/ml,3.66μg/ml,0.33 μg/ml,1.44 μg/ml,1.53 μg/ml,1.23 μg/ml,0.45 μg/ml(S/N=3),具有良好的线性关系和重现性.对饮料样品进行测定,结果令人满意.https://doi.org/zjup/1008-9497.2003.30.2.184-187食品添加剂离子色谱梯度淋洗电导检测 |
spellingShingle | ZHANGPei-min(张培敏) ZHUYan(朱岩) XUYu(徐育) Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测) Zhejiang Daxue xuebao. Lixue ban 食品添加剂 离子色谱 梯度淋洗 电导检测 |
title | Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测) |
title_full | Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测) |
title_fullStr | Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测) |
title_full_unstemmed | Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测) |
title_short | Determination of food additive with gradient eluent separation and suppressor conductance detector(食品添加剂的梯度淋洗分离和抑制电导检测) |
title_sort | determination of food additive with gradient eluent separation and suppressor conductance detector 食品添加剂的梯度淋洗分离和抑制电导检测 |
topic | 食品添加剂 离子色谱 梯度淋洗 电导检测 |
url | https://doi.org/zjup/1008-9497.2003.30.2.184-187 |
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