Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming Conditions

In this work, the hot deformation characteristics of a near-<inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> Ti-Al-2SnZr-2Mo alloy (Ti6242 alloy) with a Fine-Grained (FG) microstructure (<inl...

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Main Authors: Longqiu Song, Anzu Ii, Laurie Despax, Hatsumi Onishi, Hiroaki Matsumoto, Vincent Velay, Vanessa Vidal
Format: Article
Language:English
Published: MDPI AG 2020-11-01
Series:Metals
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Online Access:https://www.mdpi.com/2075-4701/10/12/1599
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author Longqiu Song
Anzu Ii
Laurie Despax
Hatsumi Onishi
Hiroaki Matsumoto
Vincent Velay
Vanessa Vidal
author_facet Longqiu Song
Anzu Ii
Laurie Despax
Hatsumi Onishi
Hiroaki Matsumoto
Vincent Velay
Vanessa Vidal
author_sort Longqiu Song
collection DOAJ
description In this work, the hot deformation characteristics of a near-<inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> Ti-Al-2SnZr-2Mo alloy (Ti6242 alloy) with a Fine-Grained (FG) microstructure (<inline-formula><math display="inline"><semantics><msub><mi>d</mi><mi>α</mi></msub></semantics></math></inline-formula> = 2.86 <inline-formula><math display="inline"><semantics><mi mathvariant="sans-serif">μ</mi></semantics></math></inline-formula>m) were investigated at two levels of temperature, <i>T</i> = 730 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C and <i>T</i> = 840 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C. The initial microstructure consists of equiaxed nodules of the <inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> phase as well as some <inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> lamellae sparsely distributed and separated by thin layers of the BCC <inline-formula><math display="inline"><semantics><mi>β</mi></semantics></math></inline-formula> phase. For both temperatures, three strain rates (<inline-formula><math display="inline"><semantics><mrow><msup><mn>10</mn><mrow><mo>−</mo><mn>4</mn></mrow></msup><mo>,</mo><msup><mn>10</mn><mrow><mo>−</mo><mn>3</mn></mrow></msup><mo>,</mo><msup><mn>10</mn><mrow><mo>−</mo><mn>2</mn></mrow></msup><mspace width="4pt"></mspace><msup><mi mathvariant="normal">s</mi><mrow><mo>−</mo><mn>1</mn></mrow></msup></mrow></semantics></math></inline-formula>) were analysed during loading. Moreover, the microstructural evolution (<inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> size and morphology) was also evaluated by conducting interrupted tensile tests. The different tensile testing conditions greatly influence the stress-strain response of the material as well as the microstructure evolution. Indeed, various phenomena can take place such as elongation of the grain structure, globularization, dynamic recrystallization and grain growth of the equiaxed areas depending on the temperature, the strain rate and the strain level. The FG Ti6242 alloy exhibits interesting superplastic ductility at <i>T</i> = 840 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C. At this temperature either a very gradual flow softening (at higher strain rate) or flow hardening (at lower strain rate) can be observed and are related respectively to one or more of the following mechanisms: lamellae globularization, DRX and grain growth. At the intermediate strain rate, both mechanisms, strain hardening and softening, coexist. At <i>T</i> = 730 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C, the onset of the <inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> lamellae globularization was only promoted at low strain rate. A mechanical behavior model was developed in the temperature range of 730–840 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C, which was able to take into account all the observed phenomena: viscosity, softened behavior and strain hardening. Constitutive equations were calibrated from the stress-strain responses and microstructural observations, and the computed results were in good agreement with the experiments.
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spelling doaj.art-3051f87ca3e24951bdf343f8a4b6914b2023-11-20T22:50:54ZengMDPI AGMetals2075-47012020-11-011012159910.3390/met10121599Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming ConditionsLongqiu Song0Anzu Ii1Laurie Despax2Hatsumi Onishi3Hiroaki Matsumoto4Vincent Velay5Vanessa Vidal6Institut Clément Ader (ICA), Université de Toulouse, CNRS, IMT Mines Albi, UPS, INSA, ISAE-SUPAERO, Campus Jarlard, 81013 Albi CT CEDEX 09, FranceInstitut Clément Ader (ICA), Université de Toulouse, CNRS, IMT Mines Albi, UPS, INSA, ISAE-SUPAERO, Campus Jarlard, 81013 Albi CT CEDEX 09, FranceInstitut Clément Ader (ICA), Université de Toulouse, CNRS, IMT Mines Albi, UPS, INSA, ISAE-SUPAERO, Campus Jarlard, 81013 Albi CT CEDEX 09, FranceInstitut Clément Ader (ICA), Université de Toulouse, CNRS, IMT Mines Albi, UPS, INSA, ISAE-SUPAERO, Campus Jarlard, 81013 Albi CT CEDEX 09, FranceDepartment of Advanced Materials Science, Faculty of Engineering, Kagawa University, 2217-20 Hayashi-cho, Takamatsu, Kagawa 761-0396, JapanInstitut Clément Ader (ICA), Université de Toulouse, CNRS, IMT Mines Albi, UPS, INSA, ISAE-SUPAERO, Campus Jarlard, 81013 Albi CT CEDEX 09, FranceInstitut Clément Ader (ICA), Université de Toulouse, CNRS, IMT Mines Albi, UPS, INSA, ISAE-SUPAERO, Campus Jarlard, 81013 Albi CT CEDEX 09, FranceIn this work, the hot deformation characteristics of a near-<inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> Ti-Al-2SnZr-2Mo alloy (Ti6242 alloy) with a Fine-Grained (FG) microstructure (<inline-formula><math display="inline"><semantics><msub><mi>d</mi><mi>α</mi></msub></semantics></math></inline-formula> = 2.86 <inline-formula><math display="inline"><semantics><mi mathvariant="sans-serif">μ</mi></semantics></math></inline-formula>m) were investigated at two levels of temperature, <i>T</i> = 730 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C and <i>T</i> = 840 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C. The initial microstructure consists of equiaxed nodules of the <inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> phase as well as some <inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> lamellae sparsely distributed and separated by thin layers of the BCC <inline-formula><math display="inline"><semantics><mi>β</mi></semantics></math></inline-formula> phase. For both temperatures, three strain rates (<inline-formula><math display="inline"><semantics><mrow><msup><mn>10</mn><mrow><mo>−</mo><mn>4</mn></mrow></msup><mo>,</mo><msup><mn>10</mn><mrow><mo>−</mo><mn>3</mn></mrow></msup><mo>,</mo><msup><mn>10</mn><mrow><mo>−</mo><mn>2</mn></mrow></msup><mspace width="4pt"></mspace><msup><mi mathvariant="normal">s</mi><mrow><mo>−</mo><mn>1</mn></mrow></msup></mrow></semantics></math></inline-formula>) were analysed during loading. Moreover, the microstructural evolution (<inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> size and morphology) was also evaluated by conducting interrupted tensile tests. The different tensile testing conditions greatly influence the stress-strain response of the material as well as the microstructure evolution. Indeed, various phenomena can take place such as elongation of the grain structure, globularization, dynamic recrystallization and grain growth of the equiaxed areas depending on the temperature, the strain rate and the strain level. The FG Ti6242 alloy exhibits interesting superplastic ductility at <i>T</i> = 840 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C. At this temperature either a very gradual flow softening (at higher strain rate) or flow hardening (at lower strain rate) can be observed and are related respectively to one or more of the following mechanisms: lamellae globularization, DRX and grain growth. At the intermediate strain rate, both mechanisms, strain hardening and softening, coexist. At <i>T</i> = 730 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C, the onset of the <inline-formula><math display="inline"><semantics><mi>α</mi></semantics></math></inline-formula> lamellae globularization was only promoted at low strain rate. A mechanical behavior model was developed in the temperature range of 730–840 <inline-formula><math display="inline"><semantics><msup><mrow></mrow><mo>∘</mo></msup></semantics></math></inline-formula>C, which was able to take into account all the observed phenomena: viscosity, softened behavior and strain hardening. Constitutive equations were calibrated from the stress-strain responses and microstructural observations, and the computed results were in good agreement with the experiments.https://www.mdpi.com/2075-4701/10/12/1599Ti-6Al-2Sn-4Zr-2Mo titanium alloyhot forming conditionsmicrostructural observationssoftening mechanismsunified viscoplastic constitutive equations
spellingShingle Longqiu Song
Anzu Ii
Laurie Despax
Hatsumi Onishi
Hiroaki Matsumoto
Vincent Velay
Vanessa Vidal
Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming Conditions
Metals
Ti-6Al-2Sn-4Zr-2Mo titanium alloy
hot forming conditions
microstructural observations
softening mechanisms
unified viscoplastic constitutive equations
title Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming Conditions
title_full Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming Conditions
title_fullStr Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming Conditions
title_full_unstemmed Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming Conditions
title_short Experimental Analysis and Behaviour Modelling of the Deformation Mechanisms of a Ti-6242S Alloy under Hot and Superplastic Forming Conditions
title_sort experimental analysis and behaviour modelling of the deformation mechanisms of a ti 6242s alloy under hot and superplastic forming conditions
topic Ti-6Al-2Sn-4Zr-2Mo titanium alloy
hot forming conditions
microstructural observations
softening mechanisms
unified viscoplastic constitutive equations
url https://www.mdpi.com/2075-4701/10/12/1599
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