Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi Krim

Cream demulsification is one of the purification method for separating the glycerol residue contained as emulsion with MDAG’s product. This method could be used to break emulsion system by adding electrolyte solution. This research aims to compare the performance of calcium chloride and calcium nitr...

Full description

Bibliographic Details
Main Authors: Satiti Kawuri Putri, Purwiyatno Hariyadi, Mursalin Mursalin, Nuri Andarwulan
Format: Article
Language:English
Published: Universitas Gadjah Mada 2020-03-01
Series:Agritech
Subjects:
Online Access:https://jurnal.ugm.ac.id/agritech/article/view/48779
_version_ 1818878215820673024
author Satiti Kawuri Putri
Purwiyatno Hariyadi
Mursalin Mursalin
Nuri Andarwulan
author_facet Satiti Kawuri Putri
Purwiyatno Hariyadi
Mursalin Mursalin
Nuri Andarwulan
author_sort Satiti Kawuri Putri
collection DOAJ
description Cream demulsification is one of the purification method for separating the glycerol residue contained as emulsion with MDAG’s product. This method could be used to break emulsion system by adding electrolyte solution. This research aims to compare the performance of calcium chloride and calcium nitrate as electrolyte solution that is used in the process of cream demulsification. MDAG used was Fully Hydrogenated Palm Kernel Oil (FHPKO) from glycerolysis process. Based on student t-test, there was no significant difference (p>0,05) detected between the products of cream demulsification method using calcium nitrate and calcium chloride as electrolyte solution. It was discovered that calcium nitrate reduced residual glycerol from 11,69±0.88% to 0,57±0,07%; with characteristics of MDAG’s products were free fatty acid (ALB) of 8,51±0,94%, monoacylglycerol (MAG) of 31,53±3,27%, diacylglycerol (DAG) of 19,46±0,52%, triacylglycerol (TAG) of 39,93±4,66% and yield of 81,00±3,61%.respectively. In other hand, calcium chloride reduced residual glycerol from 11,69±0,88% to 0,64±0,06%; with characteristics of MDAG’s products were ALB of 8,91±0,71%, MAG of 9,79±1,97%, DAG of 19,16±0,53%, TAG of 41,49±3,24% and yield of 80,00±4,00%, respectively. Therefore, calcium nitrate can be to replace calcium chloride as electrolyte solution in cream demulsification method, especially in reducing the glycerol residue.
first_indexed 2024-12-19T14:10:39Z
format Article
id doaj.art-30d7c2452a8b45a7a1319ed4df7922af
institution Directory Open Access Journal
issn 0216-0455
2527-3825
language English
last_indexed 2024-12-19T14:10:39Z
publishDate 2020-03-01
publisher Universitas Gadjah Mada
record_format Article
series Agritech
spelling doaj.art-30d7c2452a8b45a7a1319ed4df7922af2022-12-21T20:18:08ZengUniversitas Gadjah MadaAgritech0216-04552527-38252020-03-01401394710.22146/agritech.4877925684Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi KrimSatiti Kawuri Putri0Purwiyatno Hariyadi1Mursalin Mursalin2Nuri Andarwulan3Departemen Ilmu dan Teknologi Pangan, Fakultas Teknologi Pertanian, Institut Pertanian Bogor, Jl. Lingkar Akademik Kampus IPB, Dramaga Bogor 16680Southeast Asian Food and Agricultural Science and Technology (SEAFAST) Center, Institut Pertanian Bogor, Dramaga Bogor 16680Fakultas Teknologi Pertanian, Universitas Jambi, Jl. Tribrata, Desa Pondok Meja Km. 11, Mestong Jambi 36364Southeast Asian Food and Agricultural Science and Technology (SEAFAST) Center, Institut Pertanian Bogor, Dramaga Bogor 16680Cream demulsification is one of the purification method for separating the glycerol residue contained as emulsion with MDAG’s product. This method could be used to break emulsion system by adding electrolyte solution. This research aims to compare the performance of calcium chloride and calcium nitrate as electrolyte solution that is used in the process of cream demulsification. MDAG used was Fully Hydrogenated Palm Kernel Oil (FHPKO) from glycerolysis process. Based on student t-test, there was no significant difference (p>0,05) detected between the products of cream demulsification method using calcium nitrate and calcium chloride as electrolyte solution. It was discovered that calcium nitrate reduced residual glycerol from 11,69±0.88% to 0,57±0,07%; with characteristics of MDAG’s products were free fatty acid (ALB) of 8,51±0,94%, monoacylglycerol (MAG) of 31,53±3,27%, diacylglycerol (DAG) of 19,46±0,52%, triacylglycerol (TAG) of 39,93±4,66% and yield of 81,00±3,61%.respectively. In other hand, calcium chloride reduced residual glycerol from 11,69±0,88% to 0,64±0,06%; with characteristics of MDAG’s products were ALB of 8,91±0,71%, MAG of 9,79±1,97%, DAG of 19,16±0,53%, TAG of 41,49±3,24% and yield of 80,00±4,00%, respectively. Therefore, calcium nitrate can be to replace calcium chloride as electrolyte solution in cream demulsification method, especially in reducing the glycerol residue.https://jurnal.ugm.ac.id/agritech/article/view/48779cream demulsificationmono-diacylglycerolpurification
spellingShingle Satiti Kawuri Putri
Purwiyatno Hariyadi
Mursalin Mursalin
Nuri Andarwulan
Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi Krim
Agritech
cream demulsification
mono-diacylglycerol
purification
title Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi Krim
title_full Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi Krim
title_fullStr Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi Krim
title_full_unstemmed Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi Krim
title_short Pemurnian Produk Mono-Diasilgliserol (MDAG) Hasil Gliserolisis Kimia dengan Metode Demulsifikasi Krim
title_sort pemurnian produk mono diasilgliserol mdag hasil gliserolisis kimia dengan metode demulsifikasi krim
topic cream demulsification
mono-diacylglycerol
purification
url https://jurnal.ugm.ac.id/agritech/article/view/48779
work_keys_str_mv AT satitikawuriputri pemurnianprodukmonodiasilgliserolmdaghasilgliserolisiskimiadenganmetodedemulsifikasikrim
AT purwiyatnohariyadi pemurnianprodukmonodiasilgliserolmdaghasilgliserolisiskimiadenganmetodedemulsifikasikrim
AT mursalinmursalin pemurnianprodukmonodiasilgliserolmdaghasilgliserolisiskimiadenganmetodedemulsifikasikrim
AT nuriandarwulan pemurnianprodukmonodiasilgliserolmdaghasilgliserolisiskimiadenganmetodedemulsifikasikrim