Intergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics
As a complex multiphase heterogeneous system in solid state, multifunctional active microalloyed alumo-silicate ceramics has an inhomogeneous structure with intergranular space, which is reflected in a number of structurally sensitive properties. A very complex intergranular space and numerous inter...
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| Format: | Article |
| Language: | English |
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International Institute for the Science of Sintering, Beograd
2023-01-01
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| Series: | Science of Sintering |
| Subjects: | |
| Online Access: | https://doiserbia.nb.rs/img/doi/0350-820X/2023/0350-820X2300001P.pdf |
| _version_ | 1797748882595119104 |
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| author | Purenović Jelena M. Purenović Milovan M. |
| author_facet | Purenović Jelena M. Purenović Milovan M. |
| author_sort | Purenović Jelena M. |
| collection | DOAJ |
| description | As a complex multiphase heterogeneous system in solid state, multifunctional active microalloyed alumo-silicate ceramics has an inhomogeneous structure with intergranular space, which is reflected in a number of structurally sensitive properties. A very complex intergranular space and numerous interactions between individual phases and grains create new boundaries and an even more complex space with much smaller micrograins, which are formed by grain fragmentation by dislocations displacement. In addition to reducing macro and meso porosity, densification of intergranular space increases the number of micro pores. Intergranular surface area and volume are considered as dislocation space. Quantitative metallography method was applied to determine grain size distribution using software for automatic analysis. Specific surface tests and pore distribution were performed on special samples of multifunctional ceramics. Standard methods for determining specific surface area of samples in vacuum were used. Obtained results, which were relevant in terms of theoretical and practical implications, confirmed that multifunctional active microalloyed ceramics had a developed surface with significant number of meso and micro pores. Due to constancy of grain fragmentation process, there were significant changes in micromorphology and all multifunctional properties, as well as movement of dislocations, which made a significant contribution to contemporary research in this field. |
| first_indexed | 2024-03-12T16:12:15Z |
| format | Article |
| id | doaj.art-312714c866dd49f2b52a416e748df8fb |
| institution | Directory Open Access Journal |
| issn | 0350-820X 1820-7413 |
| language | English |
| last_indexed | 2024-03-12T16:12:15Z |
| publishDate | 2023-01-01 |
| publisher | International Institute for the Science of Sintering, Beograd |
| record_format | Article |
| series | Science of Sintering |
| spelling | doaj.art-312714c866dd49f2b52a416e748df8fb2023-08-09T12:42:32ZengInternational Institute for the Science of Sintering, BeogradScience of Sintering0350-820X1820-74132023-01-0155212714410.2298/SOS220630001P0350-820X2300001PIntergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramicsPurenović Jelena M.0https://orcid.org/0000-0002-7181-7400Purenović Milovan M.1Faculty of Technical Sciences Čačak, University of Kragujevac, SerbiaFaculty of Sciences and Mathematics, University of Niš, Serbia + Serbian Academy of inventors and scientists, SerbiaAs a complex multiphase heterogeneous system in solid state, multifunctional active microalloyed alumo-silicate ceramics has an inhomogeneous structure with intergranular space, which is reflected in a number of structurally sensitive properties. A very complex intergranular space and numerous interactions between individual phases and grains create new boundaries and an even more complex space with much smaller micrograins, which are formed by grain fragmentation by dislocations displacement. In addition to reducing macro and meso porosity, densification of intergranular space increases the number of micro pores. Intergranular surface area and volume are considered as dislocation space. Quantitative metallography method was applied to determine grain size distribution using software for automatic analysis. Specific surface tests and pore distribution were performed on special samples of multifunctional ceramics. Standard methods for determining specific surface area of samples in vacuum were used. Obtained results, which were relevant in terms of theoretical and practical implications, confirmed that multifunctional active microalloyed ceramics had a developed surface with significant number of meso and micro pores. Due to constancy of grain fragmentation process, there were significant changes in micromorphology and all multifunctional properties, as well as movement of dislocations, which made a significant contribution to contemporary research in this field.https://doiserbia.nb.rs/img/doi/0350-820X/2023/0350-820X2300001P.pdfmultifunctional ceramicsgrain distributionmacromeso and micro porositydislocationsfragmentation |
| spellingShingle | Purenović Jelena M. Purenović Milovan M. Intergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics Science of Sintering multifunctional ceramics grain distribution macro meso and micro porosity dislocations fragmentation |
| title | Intergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics |
| title_full | Intergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics |
| title_fullStr | Intergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics |
| title_full_unstemmed | Intergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics |
| title_short | Intergranular space, specific surface area, grain size distribution and distribution of macro, meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics |
| title_sort | intergranular space specific surface area grain size distribution and distribution of macro meso and micropores of multiphase microstructure in active microalloyed multifunctional ceramics |
| topic | multifunctional ceramics grain distribution macro meso and micro porosity dislocations fragmentation |
| url | https://doiserbia.nb.rs/img/doi/0350-820X/2023/0350-820X2300001P.pdf |
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