Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate
The title compound, C22H26N2O3, was synthesized by esterification of trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylic acid in the presence of H2SO4 in methanol. The dihedral angle between the benzene and pyridine rings is 84.46 (17)°. The piperidin...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2008-10-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536808029048 |
| _version_ | 1818085106212929536 |
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| author | Orhan Büyükgüngör Milen G. Bogdanov Meglena I. Kandinska Mehmet Akkurt Sema Öztürk Yıldırım |
| author_facet | Orhan Büyükgüngör Milen G. Bogdanov Meglena I. Kandinska Mehmet Akkurt Sema Öztürk Yıldırım |
| author_sort | Orhan Büyükgüngör |
| collection | DOAJ |
| description | The title compound, C22H26N2O3, was synthesized by esterification of trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylic acid in the presence of H2SO4 in methanol. The dihedral angle between the benzene and pyridine rings is 84.46 (17)°. The piperidine ring adopts a screw-boat conformation. In the crystal, inversion dimers linked by two C—H...O bonds occur. |
| first_indexed | 2024-12-10T20:04:30Z |
| format | Article |
| id | doaj.art-313e4355d8464e9298801beaf92ca607 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-10T20:04:30Z |
| publishDate | 2008-10-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-313e4355d8464e9298801beaf92ca6072022-12-22T01:35:25ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-10-016410o1932o193210.1107/S1600536808029048Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylateOrhan BüyükgüngörMilen G. BogdanovMeglena I. KandinskaMehmet AkkurtSema Öztürk YıldırımThe title compound, C22H26N2O3, was synthesized by esterification of trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylic acid in the presence of H2SO4 in methanol. The dihedral angle between the benzene and pyridine rings is 84.46 (17)°. The piperidine ring adopts a screw-boat conformation. In the crystal, inversion dimers linked by two C—H...O bonds occur.http://scripts.iucr.org/cgi-bin/paper?S1600536808029048 |
| spellingShingle | Orhan Büyükgüngör Milen G. Bogdanov Meglena I. Kandinska Mehmet Akkurt Sema Öztürk Yıldırım Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate Acta Crystallographica Section E |
| title | Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate |
| title_full | Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate |
| title_fullStr | Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate |
| title_full_unstemmed | Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate |
| title_short | Methyl trans-rac-2-hexyl-1-oxo-3-(2-pyridyl)-1,2,3,4-tetrahydroisoquinoline-4-carboxylate |
| title_sort | methyl trans rac 2 hexyl 1 oxo 3 2 pyridyl 1 2 3 4 tetrahydroisoquinoline 4 carboxylate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536808029048 |
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