Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)

本文报道利用离子色谱法同时分离分析莠去津、扑草净、扑灭通除草剂的方法.采用CG-12(2 mm)分离柱,紫外检测器,用一系列的淋洗液.实验在0.20 mol • L-1 H2SO4 + 25%CH3CN条件下,得到最佳分离效果.莠去津、扑草净、扑灭通的测定均有良好的线性.它们的检测限分别为莠去津为3.13× 10-2µg • mL-1,扑草净为4.39×10-2µg • mL-1,扑灭通为1.36× 10-2 µ/mL-1,此方法可用于废水中除草剂的测定,样品的回收率在96.00%~105.32%之间....

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Main Authors: JIANGYin-tu(蒋银土), ZhuYan(朱岩), GOUYin-yin(郭莹莹), WANGMu-hua(王慕华), WANGJong(王炯), RUANXiu-xiu(阮秀秀)
Format: Article
Language:zho
Published: Zhejiang University Press 2001-09-01
Series:Zhejiang Daxue xuebao. Lixue ban
Subjects:
Online Access:https://doi.org/zjup/1008-9497.2001.28.5.533-536
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author JIANGYin-tu(蒋银土)
ZhuYan(朱岩)
GOUYin-yin(郭莹莹)
WANGMu-hua(王慕华)
WANGJong(王炯)
RUANXiu-xiu(阮秀秀)
author_facet JIANGYin-tu(蒋银土)
ZhuYan(朱岩)
GOUYin-yin(郭莹莹)
WANGMu-hua(王慕华)
WANGJong(王炯)
RUANXiu-xiu(阮秀秀)
author_sort JIANGYin-tu(蒋银土)
collection DOAJ
description 本文报道利用离子色谱法同时分离分析莠去津、扑草净、扑灭通除草剂的方法.采用CG-12(2 mm)分离柱,紫外检测器,用一系列的淋洗液.实验在0.20 mol • L-1 H2SO4 + 25%CH3CN条件下,得到最佳分离效果.莠去津、扑草净、扑灭通的测定均有良好的线性.它们的检测限分别为莠去津为3.13× 10-2µg • mL-1,扑草净为4.39×10-2µg • mL-1,扑灭通为1.36× 10-2 µ/mL-1,此方法可用于废水中除草剂的测定,样品的回收率在96.00%~105.32%之间.
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spelling doaj.art-31f994e22faf4077a794f61acab65a982024-03-29T01:58:17ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972001-09-01285533536zjup/1008-9497.2001.28.5.533-536Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)JIANGYin-tu(蒋银土)0ZhuYan(朱岩)1GOUYin-yin(郭莹莹)2WANGMu-hua(王慕华)3WANGJong(王炯)4RUANXiu-xiu(阮秀秀)5Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)Department of Chemistry, Zhejiang University, Hangzhou 310028, China(浙江大学化学系,浙江 杭州 310028)本文报道利用离子色谱法同时分离分析莠去津、扑草净、扑灭通除草剂的方法.采用CG-12(2 mm)分离柱,紫外检测器,用一系列的淋洗液.实验在0.20 mol • L-1 H2SO4 + 25%CH3CN条件下,得到最佳分离效果.莠去津、扑草净、扑灭通的测定均有良好的线性.它们的检测限分别为莠去津为3.13× 10-2µg • mL-1,扑草净为4.39×10-2µg • mL-1,扑灭通为1.36× 10-2 µ/mL-1,此方法可用于废水中除草剂的测定,样品的回收率在96.00%~105.32%之间.https://doi.org/zjup/1008-9497.2001.28.5.533-536高效离子色谱法除草剂莠去津扑草净扑灭通
spellingShingle JIANGYin-tu(蒋银土)
ZhuYan(朱岩)
GOUYin-yin(郭莹莹)
WANGMu-hua(王慕华)
WANGJong(王炯)
RUANXiu-xiu(阮秀秀)
Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)
Zhejiang Daxue xuebao. Lixue ban
高效离子色谱法
除草剂
莠去津
扑草净
扑灭通
title Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)
title_full Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)
title_fullStr Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)
title_full_unstemmed Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)
title_short Determination of triazine herbicides by ion chromatography with UV detection(离子色谱法测定三嗪类除草剂)
title_sort determination of triazine herbicides by ion chromatography with uv detection 离子色谱法测定三嗪类除草剂
topic 高效离子色谱法
除草剂
莠去津
扑草净
扑灭通
url https://doi.org/zjup/1008-9497.2001.28.5.533-536
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