Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels

High-chromium ferritic stainless steels strengthened by Laves phase precipitates were developed for a high-temperature application in steam power plants. The impact of tungsten content on the precipitation of the intermetallic Laves phase during the newly developed thermomechanical process route was...

Full description

Bibliographic Details
Main Authors: Jana Pöpperlová, Xiuru Fan, Bernd Kuhn, Wolfgang Bleck, Ulrich Krupp
Format: Article
Language:English
Published: MDPI AG 2020-06-01
Series:Applied Sciences
Subjects:
Online Access:https://www.mdpi.com/2076-3417/10/13/4472
_version_ 1797563929928400896
author Jana Pöpperlová
Xiuru Fan
Bernd Kuhn
Wolfgang Bleck
Ulrich Krupp
author_facet Jana Pöpperlová
Xiuru Fan
Bernd Kuhn
Wolfgang Bleck
Ulrich Krupp
author_sort Jana Pöpperlová
collection DOAJ
description High-chromium ferritic stainless steels strengthened by Laves phase precipitates were developed for a high-temperature application in steam power plants. The impact of tungsten content on the precipitation of the intermetallic Laves phase during the newly developed thermomechanical process route was investigated. Due to rapid thermomechanically induced precipitation, a considerable reduction in processing time in comparison to the conventional solely thermal two-step processing of high chromium ferritic steels was achieved. Nevertheless, comparable mechanical properties at room temperature, i.e., the ultimate tensile strength of 712 MPa and the yield strength of 434 MPa, were obtained. The microstructure was analyzed by scanning electron microscopy (SEM) in combination with digital particle analysis, to estimate the particle size and the phase fraction of the Laves phase. The mean particle size of 52 nm and the volume fraction of 4.11% were achieved. Due to the tungsten content, an increase in the volume fraction and particle size was observed, giving rise to the higher strengthening effect.
first_indexed 2024-03-10T18:50:10Z
format Article
id doaj.art-328cc79687644c4397c89e0c4b2a5b86
institution Directory Open Access Journal
issn 2076-3417
language English
last_indexed 2024-03-10T18:50:10Z
publishDate 2020-06-01
publisher MDPI AG
record_format Article
series Applied Sciences
spelling doaj.art-328cc79687644c4397c89e0c4b2a5b862023-11-20T05:11:57ZengMDPI AGApplied Sciences2076-34172020-06-011013447210.3390/app10134472Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless SteelsJana Pöpperlová0Xiuru Fan1Bernd Kuhn2Wolfgang Bleck3Ulrich Krupp4Steel Institute RWTH Aachen University (IEHK), Intzestr. 1, 52072 Aachen, GermanyInstitute of Energy and Climate Research (IEK), Microstructure and Properties of Materials (IEK-2), Forschungszentrum Jülich GmbH, 52425 Jülich, GermanyInstitute of Energy and Climate Research (IEK), Microstructure and Properties of Materials (IEK-2), Forschungszentrum Jülich GmbH, 52425 Jülich, GermanySteel Institute RWTH Aachen University (IEHK), Intzestr. 1, 52072 Aachen, GermanySteel Institute RWTH Aachen University (IEHK), Intzestr. 1, 52072 Aachen, GermanyHigh-chromium ferritic stainless steels strengthened by Laves phase precipitates were developed for a high-temperature application in steam power plants. The impact of tungsten content on the precipitation of the intermetallic Laves phase during the newly developed thermomechanical process route was investigated. Due to rapid thermomechanically induced precipitation, a considerable reduction in processing time in comparison to the conventional solely thermal two-step processing of high chromium ferritic steels was achieved. Nevertheless, comparable mechanical properties at room temperature, i.e., the ultimate tensile strength of 712 MPa and the yield strength of 434 MPa, were obtained. The microstructure was analyzed by scanning electron microscopy (SEM) in combination with digital particle analysis, to estimate the particle size and the phase fraction of the Laves phase. The mean particle size of 52 nm and the volume fraction of 4.11% were achieved. Due to the tungsten content, an increase in the volume fraction and particle size was observed, giving rise to the higher strengthening effect.https://www.mdpi.com/2076-3417/10/13/4472high chromium ferritic steelintermetallic phaseLaves phaseprecipitationthermomechanical treatment
spellingShingle Jana Pöpperlová
Xiuru Fan
Bernd Kuhn
Wolfgang Bleck
Ulrich Krupp
Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels
Applied Sciences
high chromium ferritic steel
intermetallic phase
Laves phase
precipitation
thermomechanical treatment
title Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels
title_full Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels
title_fullStr Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels
title_full_unstemmed Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels
title_short Impact of Tungsten on Thermomechanically Induced Precipitation of Laves Phase in High Performance Ferritic (HiperFer) Stainless Steels
title_sort impact of tungsten on thermomechanically induced precipitation of laves phase in high performance ferritic hiperfer stainless steels
topic high chromium ferritic steel
intermetallic phase
Laves phase
precipitation
thermomechanical treatment
url https://www.mdpi.com/2076-3417/10/13/4472
work_keys_str_mv AT janapopperlova impactoftungstenonthermomechanicallyinducedprecipitationoflavesphaseinhighperformanceferritichiperferstainlesssteels
AT xiurufan impactoftungstenonthermomechanicallyinducedprecipitationoflavesphaseinhighperformanceferritichiperferstainlesssteels
AT berndkuhn impactoftungstenonthermomechanicallyinducedprecipitationoflavesphaseinhighperformanceferritichiperferstainlesssteels
AT wolfgangbleck impactoftungstenonthermomechanicallyinducedprecipitationoflavesphaseinhighperformanceferritichiperferstainlesssteels
AT ulrichkrupp impactoftungstenonthermomechanicallyinducedprecipitationoflavesphaseinhighperformanceferritichiperferstainlesssteels