Synthesis of N –sulfamethoxazolederivative imide on polymeric chain
The present work involved synthesis of several new N-Sulfamethoxazol derivatives imide on Polymeric chain by two steps. The first stip involved preparation of N- (sub.orunsub benzoyl and sub unsub acetyl) amidyl sub sulfamethoxazole (1-5) by condensation of sulfamethoxazole drug with many substitute...
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| Format: | Article |
| Language: | Arabic |
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College of Science for Women, University of Baghdad
2014-12-01
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| Series: | Baghdad Science Journal |
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| Online Access: | http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2052 |
| _version_ | 1818777838608711680 |
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| author | Baghdad Science Journal |
| author_facet | Baghdad Science Journal |
| author_sort | Baghdad Science Journal |
| collection | DOAJ |
| description | The present work involved synthesis of several new N-Sulfamethoxazol derivatives imide on Polymeric chain by two steps. The first stip involved preparation of N- (sub.orunsub benzoyl and sub unsub acetyl) amidyl sub sulfamethoxazole (1-5) by condensation of sulfamethoxazole drug with many substituted acid chloride, then the second step include, preparation new five N-(acrly-N–sub or unsub benzoyl) imidyl substituted sulfamethoxazol(6-10) by reaction of poly acryloyl chloride with the prepared compound (1-5) in first stepin asuitable solvent in the presenceamount triethylamine (Et3N) with heating. The structure confirmations of all polymers wereconfirmed using FT-IR,1H-NMR,13C-NMR and UV spectroscopy. Other physical properties including softeningpoint's, melting point, and solubility of the polymers were also measured. |
| first_indexed | 2024-12-18T11:35:11Z |
| format | Article |
| id | doaj.art-32dca02886134ea084820cb8cb02006f |
| institution | Directory Open Access Journal |
| issn | 2078-8665 2411-7986 |
| language | Arabic |
| last_indexed | 2024-12-18T11:35:11Z |
| publishDate | 2014-12-01 |
| publisher | College of Science for Women, University of Baghdad |
| record_format | Article |
| series | Baghdad Science Journal |
| spelling | doaj.art-32dca02886134ea084820cb8cb02006f2022-12-21T21:09:32ZaraCollege of Science for Women, University of BaghdadBaghdad Science Journal2078-86652411-79862014-12-0111410.21123/bsj.11.4.1567-1576Synthesis of N –sulfamethoxazolederivative imide on polymeric chainBaghdad Science JournalThe present work involved synthesis of several new N-Sulfamethoxazol derivatives imide on Polymeric chain by two steps. The first stip involved preparation of N- (sub.orunsub benzoyl and sub unsub acetyl) amidyl sub sulfamethoxazole (1-5) by condensation of sulfamethoxazole drug with many substituted acid chloride, then the second step include, preparation new five N-(acrly-N–sub or unsub benzoyl) imidyl substituted sulfamethoxazol(6-10) by reaction of poly acryloyl chloride with the prepared compound (1-5) in first stepin asuitable solvent in the presenceamount triethylamine (Et3N) with heating. The structure confirmations of all polymers wereconfirmed using FT-IR,1H-NMR,13C-NMR and UV spectroscopy. Other physical properties including softeningpoint's, melting point, and solubility of the polymers were also measured.http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2052Sulfamethoxzole drug, poly acryloyl chloride, polyamides derivatives. |
| spellingShingle | Baghdad Science Journal Synthesis of N –sulfamethoxazolederivative imide on polymeric chain Baghdad Science Journal Sulfamethoxzole drug, poly acryloyl chloride, polyamides derivatives. |
| title | Synthesis of N –sulfamethoxazolederivative imide on polymeric chain |
| title_full | Synthesis of N –sulfamethoxazolederivative imide on polymeric chain |
| title_fullStr | Synthesis of N –sulfamethoxazolederivative imide on polymeric chain |
| title_full_unstemmed | Synthesis of N –sulfamethoxazolederivative imide on polymeric chain |
| title_short | Synthesis of N –sulfamethoxazolederivative imide on polymeric chain |
| title_sort | synthesis of n sulfamethoxazolederivative imide on polymeric chain |
| topic | Sulfamethoxzole drug, poly acryloyl chloride, polyamides derivatives. |
| url | http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2052 |
| work_keys_str_mv | AT baghdadsciencejournal synthesisofnsulfamethoxazolederivativeimideonpolymericchain |