The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)
Abstract A knob bow fibula (Bügelknopffibel) of the Leutkirch type, which typologically belongs to the second half of the 4th and early 5th century CE, was excavated in 2018 in the Roman city of Augusta Raurica, present-day Kaiseraugst (AG, Switzerland). This was analyzed for the first time for its...
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SpringerOpen
2023-03-01
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Series: | Heritage Science |
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Online Access: | https://doi.org/10.1186/s40494-023-00880-0 |
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author | Sayani Biswas Isabel Megatli-Niebel Lilian Raselli Ronald Simke Thomas Elias Cocolios Nilesh Deokar Matthias Elender Lars Gerchow Herbert Hess Rustem Khasanov Andreas Knecht Hubertus Luetkens Kazuhiko Ninomiya Angela Papa Thomas Prokscha Peter Reiter Akira Sato Nathal Severijns Toni Shiroka Michael Seidlitz Stergiani Marina Vogiatzi Chennan Wang Frederik Wauters Nigel Warr Alex Amato |
author_facet | Sayani Biswas Isabel Megatli-Niebel Lilian Raselli Ronald Simke Thomas Elias Cocolios Nilesh Deokar Matthias Elender Lars Gerchow Herbert Hess Rustem Khasanov Andreas Knecht Hubertus Luetkens Kazuhiko Ninomiya Angela Papa Thomas Prokscha Peter Reiter Akira Sato Nathal Severijns Toni Shiroka Michael Seidlitz Stergiani Marina Vogiatzi Chennan Wang Frederik Wauters Nigel Warr Alex Amato |
author_sort | Sayani Biswas |
collection | DOAJ |
description | Abstract A knob bow fibula (Bügelknopffibel) of the Leutkirch type, which typologically belongs to the second half of the 4th and early 5th century CE, was excavated in 2018 in the Roman city of Augusta Raurica, present-day Kaiseraugst (AG, Switzerland). This was analyzed for the first time for its elemental composition by using the non-destructive technique of Muon Induced X-ray Emission (MIXE) in the continuous muon beam facility at the Paul Scherrer Institute (PSI). In the present work, the detection limit is 0.4 wt% with $$\sim$$ ∼ 1.5 hours of measurement time. The fibula was measured at six different positions, at a depth of 0.3–0.4 mm inside the material. The experimental results show that the fibula is made of bronze, containing the main elements copper (Cu), zinc (Zn), tin (Sn) and lead (Pb). The compositional similarities/differences between different parts of the fibula reveal that it was manufactured as two “workpieces”. One workpiece consists of the knob (13.0±0.6 wt% Pb), bow (11.9±0.4 wt% Pb) and foot (12.5 ± 0.9 wt% Pb). These show a higher Pb content, suggesting a cast bronze. The spiral (3.2 ± 0.2 wt% Pb), which is part of the other workpiece, has a comparatively lower Pb content, suggesting a forged bronze. |
first_indexed | 2024-04-09T22:42:24Z |
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institution | Directory Open Access Journal |
issn | 2050-7445 |
language | English |
last_indexed | 2024-04-09T22:42:24Z |
publishDate | 2023-03-01 |
publisher | SpringerOpen |
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series | Heritage Science |
spelling | doaj.art-3338543a17224e12b366fc55bb028fb12023-03-22T12:02:16ZengSpringerOpenHeritage Science2050-74452023-03-0111111710.1186/s40494-023-00880-0The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)Sayani Biswas0Isabel Megatli-Niebel1Lilian Raselli2Ronald Simke3Thomas Elias Cocolios4Nilesh Deokar5Matthias Elender6Lars Gerchow7Herbert Hess8Rustem Khasanov9Andreas Knecht10Hubertus Luetkens11Kazuhiko Ninomiya12Angela Papa13Thomas Prokscha14Peter Reiter15Akira Sato16Nathal Severijns17Toni Shiroka18Michael Seidlitz19Stergiani Marina Vogiatzi20Chennan Wang21Frederik Wauters22Nigel Warr23Alex Amato24Paul Scherrer Institute PSIArchäologisches Institut, Universität zu Köln, Albertus-Magnus-PlatzAugusta RauricaAugusta RauricaKU Leuven, Instituut voor Kern-en StralingfysicaPRISMA+ Cluster of Excellence and Institute of Nuclear Physics, Johannes Gutenberg Universität MainzPaul Scherrer Institute PSIPaul Scherrer Institute PSIInstitut für Kernphysik, Universität zu KölnPaul Scherrer Institute PSIPaul Scherrer Institute PSIPaul Scherrer Institute PSIGraduate School of Science, Osaka UniversityPaul Scherrer Institute PSIPaul Scherrer Institute PSIInstitut für Kernphysik, Universität zu KölnGraduate School of Science, Osaka UniversityKU Leuven, Instituut voor Kern-en StralingfysicaPaul Scherrer Institute PSIInstitut für Kernphysik, Universität zu KölnPaul Scherrer Institute PSIPaul Scherrer Institute PSIPRISMA+ Cluster of Excellence and Institute of Nuclear Physics, Johannes Gutenberg Universität MainzInstitut für Kernphysik, Universität zu KölnPaul Scherrer Institute PSIAbstract A knob bow fibula (Bügelknopffibel) of the Leutkirch type, which typologically belongs to the second half of the 4th and early 5th century CE, was excavated in 2018 in the Roman city of Augusta Raurica, present-day Kaiseraugst (AG, Switzerland). This was analyzed for the first time for its elemental composition by using the non-destructive technique of Muon Induced X-ray Emission (MIXE) in the continuous muon beam facility at the Paul Scherrer Institute (PSI). In the present work, the detection limit is 0.4 wt% with $$\sim$$ ∼ 1.5 hours of measurement time. The fibula was measured at six different positions, at a depth of 0.3–0.4 mm inside the material. The experimental results show that the fibula is made of bronze, containing the main elements copper (Cu), zinc (Zn), tin (Sn) and lead (Pb). The compositional similarities/differences between different parts of the fibula reveal that it was manufactured as two “workpieces”. One workpiece consists of the knob (13.0±0.6 wt% Pb), bow (11.9±0.4 wt% Pb) and foot (12.5 ± 0.9 wt% Pb). These show a higher Pb content, suggesting a cast bronze. The spiral (3.2 ± 0.2 wt% Pb), which is part of the other workpiece, has a comparatively lower Pb content, suggesting a forged bronze.https://doi.org/10.1186/s40494-023-00880-0Knob bow fibula (Leutkirch type)Copper alloyMuon Induced X-ray Emission (MIXE)Non-destructive elemental analysisDepth-resolved |
spellingShingle | Sayani Biswas Isabel Megatli-Niebel Lilian Raselli Ronald Simke Thomas Elias Cocolios Nilesh Deokar Matthias Elender Lars Gerchow Herbert Hess Rustem Khasanov Andreas Knecht Hubertus Luetkens Kazuhiko Ninomiya Angela Papa Thomas Prokscha Peter Reiter Akira Sato Nathal Severijns Toni Shiroka Michael Seidlitz Stergiani Marina Vogiatzi Chennan Wang Frederik Wauters Nigel Warr Alex Amato The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE) Heritage Science Knob bow fibula (Leutkirch type) Copper alloy Muon Induced X-ray Emission (MIXE) Non-destructive elemental analysis Depth-resolved |
title | The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE) |
title_full | The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE) |
title_fullStr | The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE) |
title_full_unstemmed | The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE) |
title_short | The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE) |
title_sort | non destructive investigation of a late antique knob bow fibula bugelknopffibel from kaiseraugst ch using muon induced x ray emission mixe |
topic | Knob bow fibula (Leutkirch type) Copper alloy Muon Induced X-ray Emission (MIXE) Non-destructive elemental analysis Depth-resolved |
url | https://doi.org/10.1186/s40494-023-00880-0 |
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