The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)

Abstract A knob bow fibula (Bügelknopffibel) of the Leutkirch type, which typologically belongs to the second half of the 4th and early 5th century CE, was excavated in 2018 in the Roman city of Augusta Raurica, present-day Kaiseraugst (AG, Switzerland). This was analyzed for the first time for its...

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Main Authors: Sayani Biswas, Isabel Megatli-Niebel, Lilian Raselli, Ronald Simke, Thomas Elias Cocolios, Nilesh Deokar, Matthias Elender, Lars Gerchow, Herbert Hess, Rustem Khasanov, Andreas Knecht, Hubertus Luetkens, Kazuhiko Ninomiya, Angela Papa, Thomas Prokscha, Peter Reiter, Akira Sato, Nathal Severijns, Toni Shiroka, Michael Seidlitz, Stergiani Marina Vogiatzi, Chennan Wang, Frederik Wauters, Nigel Warr, Alex Amato
Format: Article
Language:English
Published: SpringerOpen 2023-03-01
Series:Heritage Science
Subjects:
Online Access:https://doi.org/10.1186/s40494-023-00880-0
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author Sayani Biswas
Isabel Megatli-Niebel
Lilian Raselli
Ronald Simke
Thomas Elias Cocolios
Nilesh Deokar
Matthias Elender
Lars Gerchow
Herbert Hess
Rustem Khasanov
Andreas Knecht
Hubertus Luetkens
Kazuhiko Ninomiya
Angela Papa
Thomas Prokscha
Peter Reiter
Akira Sato
Nathal Severijns
Toni Shiroka
Michael Seidlitz
Stergiani Marina Vogiatzi
Chennan Wang
Frederik Wauters
Nigel Warr
Alex Amato
author_facet Sayani Biswas
Isabel Megatli-Niebel
Lilian Raselli
Ronald Simke
Thomas Elias Cocolios
Nilesh Deokar
Matthias Elender
Lars Gerchow
Herbert Hess
Rustem Khasanov
Andreas Knecht
Hubertus Luetkens
Kazuhiko Ninomiya
Angela Papa
Thomas Prokscha
Peter Reiter
Akira Sato
Nathal Severijns
Toni Shiroka
Michael Seidlitz
Stergiani Marina Vogiatzi
Chennan Wang
Frederik Wauters
Nigel Warr
Alex Amato
author_sort Sayani Biswas
collection DOAJ
description Abstract A knob bow fibula (Bügelknopffibel) of the Leutkirch type, which typologically belongs to the second half of the 4th and early 5th century CE, was excavated in 2018 in the Roman city of Augusta Raurica, present-day Kaiseraugst (AG, Switzerland). This was analyzed for the first time for its elemental composition by using the non-destructive technique of Muon Induced X-ray Emission (MIXE) in the continuous muon beam facility at the Paul Scherrer Institute (PSI). In the present work, the detection limit is 0.4 wt% with $$\sim$$ ∼ 1.5 hours of measurement time. The fibula was measured at six different positions, at a depth of 0.3–0.4 mm inside the material. The experimental results show that the fibula is made of bronze, containing the main elements copper (Cu), zinc (Zn), tin (Sn) and lead (Pb). The compositional similarities/differences between different parts of the fibula reveal that it was manufactured as two “workpieces”. One workpiece consists of the knob (13.0±0.6 wt% Pb), bow (11.9±0.4 wt% Pb) and foot (12.5 ± 0.9 wt% Pb). These show a higher Pb content, suggesting a cast bronze. The spiral (3.2 ± 0.2 wt% Pb), which is part of the other workpiece, has a comparatively lower Pb content, suggesting a forged bronze.
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spelling doaj.art-3338543a17224e12b366fc55bb028fb12023-03-22T12:02:16ZengSpringerOpenHeritage Science2050-74452023-03-0111111710.1186/s40494-023-00880-0The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)Sayani Biswas0Isabel Megatli-Niebel1Lilian Raselli2Ronald Simke3Thomas Elias Cocolios4Nilesh Deokar5Matthias Elender6Lars Gerchow7Herbert Hess8Rustem Khasanov9Andreas Knecht10Hubertus Luetkens11Kazuhiko Ninomiya12Angela Papa13Thomas Prokscha14Peter Reiter15Akira Sato16Nathal Severijns17Toni Shiroka18Michael Seidlitz19Stergiani Marina Vogiatzi20Chennan Wang21Frederik Wauters22Nigel Warr23Alex Amato24Paul Scherrer Institute PSIArchäologisches Institut, Universität zu Köln, Albertus-Magnus-PlatzAugusta RauricaAugusta RauricaKU Leuven, Instituut voor Kern-en StralingfysicaPRISMA+ Cluster of Excellence and Institute of Nuclear Physics, Johannes Gutenberg Universität MainzPaul Scherrer Institute PSIPaul Scherrer Institute PSIInstitut für Kernphysik, Universität zu KölnPaul Scherrer Institute PSIPaul Scherrer Institute PSIPaul Scherrer Institute PSIGraduate School of Science, Osaka UniversityPaul Scherrer Institute PSIPaul Scherrer Institute PSIInstitut für Kernphysik, Universität zu KölnGraduate School of Science, Osaka UniversityKU Leuven, Instituut voor Kern-en StralingfysicaPaul Scherrer Institute PSIInstitut für Kernphysik, Universität zu KölnPaul Scherrer Institute PSIPaul Scherrer Institute PSIPRISMA+ Cluster of Excellence and Institute of Nuclear Physics, Johannes Gutenberg Universität MainzInstitut für Kernphysik, Universität zu KölnPaul Scherrer Institute PSIAbstract A knob bow fibula (Bügelknopffibel) of the Leutkirch type, which typologically belongs to the second half of the 4th and early 5th century CE, was excavated in 2018 in the Roman city of Augusta Raurica, present-day Kaiseraugst (AG, Switzerland). This was analyzed for the first time for its elemental composition by using the non-destructive technique of Muon Induced X-ray Emission (MIXE) in the continuous muon beam facility at the Paul Scherrer Institute (PSI). In the present work, the detection limit is 0.4 wt% with $$\sim$$ ∼ 1.5 hours of measurement time. The fibula was measured at six different positions, at a depth of 0.3–0.4 mm inside the material. The experimental results show that the fibula is made of bronze, containing the main elements copper (Cu), zinc (Zn), tin (Sn) and lead (Pb). The compositional similarities/differences between different parts of the fibula reveal that it was manufactured as two “workpieces”. One workpiece consists of the knob (13.0±0.6 wt% Pb), bow (11.9±0.4 wt% Pb) and foot (12.5 ± 0.9 wt% Pb). These show a higher Pb content, suggesting a cast bronze. The spiral (3.2 ± 0.2 wt% Pb), which is part of the other workpiece, has a comparatively lower Pb content, suggesting a forged bronze.https://doi.org/10.1186/s40494-023-00880-0Knob bow fibula (Leutkirch type)Copper alloyMuon Induced X-ray Emission (MIXE)Non-destructive elemental analysisDepth-resolved
spellingShingle Sayani Biswas
Isabel Megatli-Niebel
Lilian Raselli
Ronald Simke
Thomas Elias Cocolios
Nilesh Deokar
Matthias Elender
Lars Gerchow
Herbert Hess
Rustem Khasanov
Andreas Knecht
Hubertus Luetkens
Kazuhiko Ninomiya
Angela Papa
Thomas Prokscha
Peter Reiter
Akira Sato
Nathal Severijns
Toni Shiroka
Michael Seidlitz
Stergiani Marina Vogiatzi
Chennan Wang
Frederik Wauters
Nigel Warr
Alex Amato
The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)
Heritage Science
Knob bow fibula (Leutkirch type)
Copper alloy
Muon Induced X-ray Emission (MIXE)
Non-destructive elemental analysis
Depth-resolved
title The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)
title_full The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)
title_fullStr The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)
title_full_unstemmed The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)
title_short The non-destructive investigation of a late antique knob bow fibula (Bügelknopffibel) from Kaiseraugst/CH using Muon Induced X-ray Emission (MIXE)
title_sort non destructive investigation of a late antique knob bow fibula bugelknopffibel from kaiseraugst ch using muon induced x ray emission mixe
topic Knob bow fibula (Leutkirch type)
Copper alloy
Muon Induced X-ray Emission (MIXE)
Non-destructive elemental analysis
Depth-resolved
url https://doi.org/10.1186/s40494-023-00880-0
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