The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products

The curing kinetics can influence the final macroscopic properties, particularly the three-point bending of the fiber-reinforced composite materials. In this research, the curing kinetics of commercially available glass fiber/epoxy resin prepregs were studied by non-isothermal differential scanning...

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Main Authors: Lvtao Zhu, Zhenxing Wang, Mahfuz Bin Rahman, Wei Shen, Chengyan Zhu
Format: Article
Language:English
Published: MDPI AG 2021-08-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/16/4673
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author Lvtao Zhu
Zhenxing Wang
Mahfuz Bin Rahman
Wei Shen
Chengyan Zhu
author_facet Lvtao Zhu
Zhenxing Wang
Mahfuz Bin Rahman
Wei Shen
Chengyan Zhu
author_sort Lvtao Zhu
collection DOAJ
description The curing kinetics can influence the final macroscopic properties, particularly the three-point bending of the fiber-reinforced composite materials. In this research, the curing kinetics of commercially available glass fiber/epoxy resin prepregs were studied by non-isothermal differential scanning calorimetry (DSC). The curing kinetic parameters were obtained by fitting and the apparent activation energy E<sub>a</sub> of the prepreg, the pre-exponent factor, and the reaction order value obtained. A phenomenological <i>n</i>th-order curing reaction kinetic model was established according to Kissinger equation and Crane equation. Furthermore, the optimal curing temperature of the prepregs was obtained by the T-β extrapolation method. A vacuum hot pressing technique was applied to prepare composite laminates. The pre-curing, curing, and post-curing temperatures were 116, 130, and 153 °C respectively. In addition, three-point bending was used to test the specimens’ fracture behavior, and the surface morphology was analyzed. The results show that the differences in the mechanical properties of the samples are relatively small, indicating that the process settings are reasonable.
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spelling doaj.art-337c788efc944ed19f70cb747ed92f032023-11-22T08:31:05ZengMDPI AGMaterials1996-19442021-08-011416467310.3390/ma14164673The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its ProductsLvtao Zhu0Zhenxing Wang1Mahfuz Bin Rahman2Wei Shen3Chengyan Zhu4College of Textile Science and Engineering (International Institute of Silk), Zhejiang Sci-Tech University, Hangzhou 310018, ChinaCollege of Textile Science and Engineering (International Institute of Silk), Zhejiang Sci-Tech University, Hangzhou 310018, ChinaCollege of Textile Science and Engineering (International Institute of Silk), Zhejiang Sci-Tech University, Hangzhou 310018, ChinaShaoxing Baojing Composite Materials Co., Ltd., Shaoxing 312000, ChinaCollege of Textile Science and Engineering (International Institute of Silk), Zhejiang Sci-Tech University, Hangzhou 310018, ChinaThe curing kinetics can influence the final macroscopic properties, particularly the three-point bending of the fiber-reinforced composite materials. In this research, the curing kinetics of commercially available glass fiber/epoxy resin prepregs were studied by non-isothermal differential scanning calorimetry (DSC). The curing kinetic parameters were obtained by fitting and the apparent activation energy E<sub>a</sub> of the prepreg, the pre-exponent factor, and the reaction order value obtained. A phenomenological <i>n</i>th-order curing reaction kinetic model was established according to Kissinger equation and Crane equation. Furthermore, the optimal curing temperature of the prepregs was obtained by the T-β extrapolation method. A vacuum hot pressing technique was applied to prepare composite laminates. The pre-curing, curing, and post-curing temperatures were 116, 130, and 153 °C respectively. In addition, three-point bending was used to test the specimens’ fracture behavior, and the surface morphology was analyzed. The results show that the differences in the mechanical properties of the samples are relatively small, indicating that the process settings are reasonable.https://www.mdpi.com/1996-1944/14/16/4673prepregglass fiber/epoxy resincuring kineticsbending properties
spellingShingle Lvtao Zhu
Zhenxing Wang
Mahfuz Bin Rahman
Wei Shen
Chengyan Zhu
The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
Materials
prepreg
glass fiber/epoxy resin
curing kinetics
bending properties
title The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_full The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_fullStr The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_full_unstemmed The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_short The Curing Kinetics of E-Glass Fiber/Epoxy Resin Prepreg and the Bending Properties of Its Products
title_sort curing kinetics of e glass fiber epoxy resin prepreg and the bending properties of its products
topic prepreg
glass fiber/epoxy resin
curing kinetics
bending properties
url https://www.mdpi.com/1996-1944/14/16/4673
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