Synthesis, characterization and formation mechanisms of nanocrystalline akermanite powder

Pure nanocrystalline akermanite was successfully synthesized by mechanical activation and heat treatment of talc, calcium carbonate, and silicate. Powders were characterized by thermogravimetric analysis (TGA), x-ray diffractometry (XRD), scanning electron microscopy (SEM), and transmission electron...

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Bibliographic Details
Main Authors: Fariborz Tavangarian, Caleb A. Zolko, Keivan Davami
Format: Article
Language:English
Published: Elsevier 2021-03-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785421000211
Description
Summary:Pure nanocrystalline akermanite was successfully synthesized by mechanical activation and heat treatment of talc, calcium carbonate, and silicate. Powders were characterized by thermogravimetric analysis (TGA), x-ray diffractometry (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The formation mechanism was studied in depth. These results showed that akermanite was produced by the formation and consumption of transitionary compounds such as enstatite, wollastonite, larnite, and merwinite. Pure akermanite was synthesized with a crystalline size of 34 nm after ball milling for 20 h and subsequent heat treatment at 900 °C for 1 h.
ISSN:2238-7854