Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrots

Many unit operations in the food industry are diffusional driven. These processes are usually very slow and difficult to handle for specific groups of raw materials. Vacuum impregnation (VI) is one example. Impregnating low-porous or densely-structured materials is problematic and often requires low...

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Main Authors: Elżbieta Radziejewska-Kubzdela, Justyna Szadzińska, Róża Biegańska-Marecik, Tomasz Spiżewski, Dominik Mierzwa
Format: Article
Language:English
Published: Elsevier 2023-10-01
Series:Ultrasonics Sonochemistry
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S1350417723003048
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author Elżbieta Radziejewska-Kubzdela
Justyna Szadzińska
Róża Biegańska-Marecik
Tomasz Spiżewski
Dominik Mierzwa
author_facet Elżbieta Radziejewska-Kubzdela
Justyna Szadzińska
Róża Biegańska-Marecik
Tomasz Spiżewski
Dominik Mierzwa
author_sort Elżbieta Radziejewska-Kubzdela
collection DOAJ
description Many unit operations in the food industry are diffusional driven. These processes are usually very slow and difficult to handle for specific groups of raw materials. Vacuum impregnation (VI) is one example. Impregnating low-porous or densely-structured materials is problematic and often requires low pressure, which can negatively affect product quality and be expensive in energy consumption. This research aimed to evaluate ultrasound (US) as a factor in intensifying mass transfer and enhancing its effectiveness in the VI process. Experiments on impregnation enhanced with ultrasound applied at different stages of the process were carried out. Carrot, a difficult-to-process raw material, was impregnated with ascorbic acid as a mass transfer marker. The process’s effectiveness and selected quality parameters were then analyzed. Ultrasound was found to have a positive influence on mass transfer during VI. The effects of ultrasound enhancement were different for particular processes, and depended on the stage of the application and duration of US exposure. The greatest increase in the tissue’s ascorbic acid content (60% compared to the non-ultrasound-assisted process) was observed when ultrasound was applied continuously throughout the process. Applying ultrasound only during the relaxation (at atmospheric pressure) or aeration periods resulted in a similar effect – c.a. 20% increase in the marker’s content. The smallest increase (10%) was observed when ultrasound was applied only during the vacuum period. Applying US did not result in any unfavorable color change. In most cases, pH decreased, which is favorable for the semi-product’s stability. The carotenoid and phenolic compounds’ content did not decrease. The results unequivocally indicate that ultrasound has great potential for use as a mass transfer accelerator in the VI process for low porosity materials. The effectiveness of the US is influenced not only by pressure but also by exposure duration. The synergistic effect observed using ultrasound-enhanced impregnation throughout the process confirmed this hypothesis.
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spelling doaj.art-33fd5dc4e57a4d6b8c464403513cdc8c2023-09-11T04:16:42ZengElsevierUltrasonics Sonochemistry1350-41772023-10-0199106592Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrotsElżbieta Radziejewska-Kubzdela0Justyna Szadzińska1Róża Biegańska-Marecik2Tomasz Spiżewski3Dominik Mierzwa4Department of Food Technology of Plant Origin, Poznań University of Life Sciences, ul. Wojska Polskiego 31, 60-624 Poznań, PolandDivision of Process Engineering, Institute of Chemical Technology and Engineering, Poznan University of Technology, ul. Berdychowo 4, 60-965 Poznań, PolandDepartment of Food Technology of Plant Origin, Poznań University of Life Sciences, ul. Wojska Polskiego 31, 60-624 Poznań, PolandDepartment of Vegetable Crops, Poznań University of Life Sciences, ul. Dąbrowskiego 159, 60-594 Poznań, PolandDivision of Process Engineering, Institute of Chemical Technology and Engineering, Poznan University of Technology, ul. Berdychowo 4, 60-965 Poznań, Poland; Corresponding author.Many unit operations in the food industry are diffusional driven. These processes are usually very slow and difficult to handle for specific groups of raw materials. Vacuum impregnation (VI) is one example. Impregnating low-porous or densely-structured materials is problematic and often requires low pressure, which can negatively affect product quality and be expensive in energy consumption. This research aimed to evaluate ultrasound (US) as a factor in intensifying mass transfer and enhancing its effectiveness in the VI process. Experiments on impregnation enhanced with ultrasound applied at different stages of the process were carried out. Carrot, a difficult-to-process raw material, was impregnated with ascorbic acid as a mass transfer marker. The process’s effectiveness and selected quality parameters were then analyzed. Ultrasound was found to have a positive influence on mass transfer during VI. The effects of ultrasound enhancement were different for particular processes, and depended on the stage of the application and duration of US exposure. The greatest increase in the tissue’s ascorbic acid content (60% compared to the non-ultrasound-assisted process) was observed when ultrasound was applied continuously throughout the process. Applying ultrasound only during the relaxation (at atmospheric pressure) or aeration periods resulted in a similar effect – c.a. 20% increase in the marker’s content. The smallest increase (10%) was observed when ultrasound was applied only during the vacuum period. Applying US did not result in any unfavorable color change. In most cases, pH decreased, which is favorable for the semi-product’s stability. The carotenoid and phenolic compounds’ content did not decrease. The results unequivocally indicate that ultrasound has great potential for use as a mass transfer accelerator in the VI process for low porosity materials. The effectiveness of the US is influenced not only by pressure but also by exposure duration. The synergistic effect observed using ultrasound-enhanced impregnation throughout the process confirmed this hypothesis.http://www.sciencedirect.com/science/article/pii/S1350417723003048Ascorbic acidDaucus carotaPolyphenolCarotenoidAntioxidant activityStructure change
spellingShingle Elżbieta Radziejewska-Kubzdela
Justyna Szadzińska
Róża Biegańska-Marecik
Tomasz Spiżewski
Dominik Mierzwa
Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrots
Ultrasonics Sonochemistry
Ascorbic acid
Daucus carota
Polyphenol
Carotenoid
Antioxidant activity
Structure change
title Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrots
title_full Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrots
title_fullStr Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrots
title_full_unstemmed Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrots
title_short Effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products: A case study of carrots
title_sort effect of ultrasound on mass transfer during vacuum impregnation and selected quality parameters of products a case study of carrots
topic Ascorbic acid
Daucus carota
Polyphenol
Carotenoid
Antioxidant activity
Structure change
url http://www.sciencedirect.com/science/article/pii/S1350417723003048
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