Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatments

A novel maraging steel with vanadium supplement called Specialis® has been developed for additive manufacturing by powder bed fusion using a laser beam. This study characterized this material after processing and post-processing. An intensive process optimization was carried out by means of a single...

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Main Authors: Niki Nouri, Qing Li, James Damon, Fabian Mühl, Gregor Graf, Stefan Dietrich, Volker Schulze
Format: Article
Language:English
Published: Elsevier 2022-05-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785422002988
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author Niki Nouri
Qing Li
James Damon
Fabian Mühl
Gregor Graf
Stefan Dietrich
Volker Schulze
author_facet Niki Nouri
Qing Li
James Damon
Fabian Mühl
Gregor Graf
Stefan Dietrich
Volker Schulze
author_sort Niki Nouri
collection DOAJ
description A novel maraging steel with vanadium supplement called Specialis® has been developed for additive manufacturing by powder bed fusion using a laser beam. This study characterized this material after processing and post-processing. An intensive process optimization was carried out by means of a single track melt pool analysis to investigate optimal parameter sets for manufacturing of dense parts. Furthermore, the development of post heat treatment strategies and their influence on mechanical and microstructural characteristics of the material was evaluated. Two main concepts of direct aging treatment (AT) and solution treatment followed by aging treatment (ST+AT) were tested by dilatometry, to analyse the material behaviour with different initial microstructures: as-built and recrystallized. Both heat treatments resulted in a considerable improvement of hardness after only 2 h of aging, increasing to approximately 700 HV and 760 HV respectively, which exceeded the peak hardness of commonly known maraging steel 18Ni300 (660 HV after 6 h). These results were confirmed by tensile tests, where a tensile strength of more than 2300 MPa was achieved. Alongside the precipitation hardening known for maraging steels, the increased hardness was a result of grain refinement due to the addition of vanadium.
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spelling doaj.art-341efa5b13144058937b8d009da3b6492022-12-21T21:10:37ZengElsevierJournal of Materials Research and Technology2238-78542022-05-0118931942Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatmentsNiki Nouri0Qing Li1James Damon2Fabian Mühl3Gregor Graf4Stefan Dietrich5Volker Schulze6Institute for Applied Materials – Materials Science and Engineering (IAM-WK), Karlsruhe Institute of Technology, Karlsruhe, Germany; Corresponding author.Institute for Applied Materials – Materials Science and Engineering (IAM-WK), Karlsruhe Institute of Technology, Karlsruhe, Germany; Rosswag GmbH, August-Roßwag-Straße 1, 76327, Pfinztal, GermanyInstitute for Applied Materials – Materials Science and Engineering (IAM-WK), Karlsruhe Institute of Technology, Karlsruhe, GermanyInstitute for Applied Materials – Materials Science and Engineering (IAM-WK), Karlsruhe Institute of Technology, Karlsruhe, GermanyRosswag GmbH, August-Roßwag-Straße 1, 76327, Pfinztal, GermanyInstitute for Applied Materials – Materials Science and Engineering (IAM-WK), Karlsruhe Institute of Technology, Karlsruhe, GermanyInstitute for Applied Materials – Materials Science and Engineering (IAM-WK), Karlsruhe Institute of Technology, Karlsruhe, GermanyA novel maraging steel with vanadium supplement called Specialis® has been developed for additive manufacturing by powder bed fusion using a laser beam. This study characterized this material after processing and post-processing. An intensive process optimization was carried out by means of a single track melt pool analysis to investigate optimal parameter sets for manufacturing of dense parts. Furthermore, the development of post heat treatment strategies and their influence on mechanical and microstructural characteristics of the material was evaluated. Two main concepts of direct aging treatment (AT) and solution treatment followed by aging treatment (ST+AT) were tested by dilatometry, to analyse the material behaviour with different initial microstructures: as-built and recrystallized. Both heat treatments resulted in a considerable improvement of hardness after only 2 h of aging, increasing to approximately 700 HV and 760 HV respectively, which exceeded the peak hardness of commonly known maraging steel 18Ni300 (660 HV after 6 h). These results were confirmed by tensile tests, where a tensile strength of more than 2300 MPa was achieved. Alongside the precipitation hardening known for maraging steels, the increased hardness was a result of grain refinement due to the addition of vanadium.http://www.sciencedirect.com/science/article/pii/S2238785422002988Laser-based powder bed fusionProcess developmentMaterial characterizationPost heat treatmentNovel maraging steel
spellingShingle Niki Nouri
Qing Li
James Damon
Fabian Mühl
Gregor Graf
Stefan Dietrich
Volker Schulze
Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatments
Journal of Materials Research and Technology
Laser-based powder bed fusion
Process development
Material characterization
Post heat treatment
Novel maraging steel
title Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatments
title_full Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatments
title_fullStr Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatments
title_full_unstemmed Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatments
title_short Characterization of a novel maraging steel for laser-based powder bed fusion: optimization of process parameters and post heat treatments
title_sort characterization of a novel maraging steel for laser based powder bed fusion optimization of process parameters and post heat treatments
topic Laser-based powder bed fusion
Process development
Material characterization
Post heat treatment
Novel maraging steel
url http://www.sciencedirect.com/science/article/pii/S2238785422002988
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AT jamesdamon characterizationofanovelmaragingsteelforlaserbasedpowderbedfusionoptimizationofprocessparametersandpostheattreatments
AT fabianmuhl characterizationofanovelmaragingsteelforlaserbasedpowderbedfusionoptimizationofprocessparametersandpostheattreatments
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AT stefandietrich characterizationofanovelmaragingsteelforlaserbasedpowderbedfusionoptimizationofprocessparametersandpostheattreatments
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