Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steel

Plain strain deformation trials were carried out on samples of pipeline steels at 1473 K, 1673 K and 1723 K, respectively. The deformation of inclusions in the solid steel at different temperatures and in the semi-solid steel was studied. The composition of inclusions changed from 60.62%Al2O3–16.10%...

Full description

Bibliographic Details
Main Authors: Yi Wang, Lifeng Zhang, Ying Ren, Zushu Li, Carl Slater, Kaiyu Peng, Fenggang Liu, Yanyu Zhao
Format: Article
Language:English
Published: Elsevier 2021-03-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785421001071
_version_ 1818574025012543488
author Yi Wang
Lifeng Zhang
Ying Ren
Zushu Li
Carl Slater
Kaiyu Peng
Fenggang Liu
Yanyu Zhao
author_facet Yi Wang
Lifeng Zhang
Ying Ren
Zushu Li
Carl Slater
Kaiyu Peng
Fenggang Liu
Yanyu Zhao
author_sort Yi Wang
collection DOAJ
description Plain strain deformation trials were carried out on samples of pipeline steels at 1473 K, 1673 K and 1723 K, respectively. The deformation of inclusions in the solid steel at different temperatures and in the semi-solid steel was studied. The composition of inclusions changed from 60.62%Al2O3–16.10%CaO–10.27%MgO–13.01%CaS before deformation to 60.59%Al2O3–13.03%CaO–12.74%MgO–13.63%CaS, 59.69%Al2O3–7.04%CaO–11.51%MgO–21.76%CaS, and 68.26%Al2O3–22.56%CaO–6.68%MgO–2.5%CaS with corresponding deforming temperatures of 1473 K, 1673 K and 1723 K. While the average aspect ratio of inclusions increased from 1.28 to 2.23, 1.32, and 1.35, respectively. Thermodynamic calculations performed by FactSage 7.0 verified the composition transformation from CaO to CaS during the solidification and cooling process of the steel. A kinetic model was used to calculate the dynamic transformation of the inclusion composition at compression temperatures. The inclusion transformation ratio from CaO to CaS increased from 38.28% at 1473 K to 50.50% at 1673 K. For the deformation in the solid steel at the temperature below 1673 K, the thickness of the hard phase CaS increased with the soaking temperature, while the hardness of the steel matrix decreased. The larger hardness difference between inclusions and the steel matrix led to a higher aspect ratio of inclusions after deformation. For the deformation in the semi-solid steel, the small difference of hardness between the soft inclusion phase and the soft steel matrix resulted in a low aspect ratio of inclusions in the semi-solid steel after deformation.
first_indexed 2024-12-15T00:20:55Z
format Article
id doaj.art-345c7eec7f794ee3b45d74bdebec9de5
institution Directory Open Access Journal
issn 2238-7854
language English
last_indexed 2024-12-15T00:20:55Z
publishDate 2021-03-01
publisher Elsevier
record_format Article
series Journal of Materials Research and Technology
spelling doaj.art-345c7eec7f794ee3b45d74bdebec9de52022-12-21T22:42:18ZengElsevierJournal of Materials Research and Technology2238-78542021-03-011112201231Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steelYi Wang0Lifeng Zhang1Ying Ren2Zushu Li3Carl Slater4Kaiyu Peng5Fenggang Liu6Yanyu Zhao7School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing (USTB), Beijing, 100083, ChinaState Key Laboratory of Metastable Materials Science and Technology, School of Mechanical Engineering, Yanshan University, Qinhuangdao City, Hebei Province, 066004, China; Corresponding author.School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing (USTB), Beijing, 100083, China; Corresponding author.Advanced Steel Research Centre, WMG, University of Warwick, Coventry, CV4 7AL, UK; Corresponding author.Advanced Steel Research Centre, WMG, University of Warwick, Coventry, CV4 7AL, UKSchool of Metallurgical and Ecological Engineering, University of Science and Technology Beijing (USTB), Beijing, 100083, ChinaSchool of Metallurgical and Ecological Engineering, University of Science and Technology Beijing (USTB), Beijing, 100083, ChinaSchool of Metallurgical and Ecological Engineering, University of Science and Technology Beijing (USTB), Beijing, 100083, ChinaPlain strain deformation trials were carried out on samples of pipeline steels at 1473 K, 1673 K and 1723 K, respectively. The deformation of inclusions in the solid steel at different temperatures and in the semi-solid steel was studied. The composition of inclusions changed from 60.62%Al2O3–16.10%CaO–10.27%MgO–13.01%CaS before deformation to 60.59%Al2O3–13.03%CaO–12.74%MgO–13.63%CaS, 59.69%Al2O3–7.04%CaO–11.51%MgO–21.76%CaS, and 68.26%Al2O3–22.56%CaO–6.68%MgO–2.5%CaS with corresponding deforming temperatures of 1473 K, 1673 K and 1723 K. While the average aspect ratio of inclusions increased from 1.28 to 2.23, 1.32, and 1.35, respectively. Thermodynamic calculations performed by FactSage 7.0 verified the composition transformation from CaO to CaS during the solidification and cooling process of the steel. A kinetic model was used to calculate the dynamic transformation of the inclusion composition at compression temperatures. The inclusion transformation ratio from CaO to CaS increased from 38.28% at 1473 K to 50.50% at 1673 K. For the deformation in the solid steel at the temperature below 1673 K, the thickness of the hard phase CaS increased with the soaking temperature, while the hardness of the steel matrix decreased. The larger hardness difference between inclusions and the steel matrix led to a higher aspect ratio of inclusions after deformation. For the deformation in the semi-solid steel, the small difference of hardness between the soft inclusion phase and the soft steel matrix resulted in a low aspect ratio of inclusions in the semi-solid steel after deformation.http://www.sciencedirect.com/science/article/pii/S2238785421001071Inclusion deformationInclusion transformationSemi-solid rollingPipeline steelThermodynamicsKinetics
spellingShingle Yi Wang
Lifeng Zhang
Ying Ren
Zushu Li
Carl Slater
Kaiyu Peng
Fenggang Liu
Yanyu Zhao
Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steel
Journal of Materials Research and Technology
Inclusion deformation
Inclusion transformation
Semi-solid rolling
Pipeline steel
Thermodynamics
Kinetics
title Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steel
title_full Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steel
title_fullStr Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steel
title_full_unstemmed Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steel
title_short Effect of compression temperature on deformation of CaO–CaS–Al2O3–MgO inclusions in pipeline steel
title_sort effect of compression temperature on deformation of cao cas al2o3 mgo inclusions in pipeline steel
topic Inclusion deformation
Inclusion transformation
Semi-solid rolling
Pipeline steel
Thermodynamics
Kinetics
url http://www.sciencedirect.com/science/article/pii/S2238785421001071
work_keys_str_mv AT yiwang effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel
AT lifengzhang effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel
AT yingren effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel
AT zushuli effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel
AT carlslater effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel
AT kaiyupeng effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel
AT fenggangliu effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel
AT yanyuzhao effectofcompressiontemperatureondeformationofcaocasal2o3mgoinclusionsinpipelinesteel