Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reaction
A fast and facile one-pot procedure for the preparation of symmetric 5-Aryloyl-1,9-dimethyl-5,9-dihydro-2H-pyrano[2,3-d:6,5-d']dipyrimidine-2,4,6,8(1H,3H,7H)-tetraone derivatives by two-component reaction of N-methylbarbituric acid and arylglyoxalmonohydrates catalyzed by DABCO in ethanol at 50...
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Growing Science
2017-02-01
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Series: | Current Chemistry Letters |
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Online Access: | http://www.growingscience.com/ccl/Vol6/ccl_2016_21.pdf |
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author | Mehdi Rimaz Hossein Mousavi Mojgan Behnam Leila Sarvari Behzad Khalili |
author_facet | Mehdi Rimaz Hossein Mousavi Mojgan Behnam Leila Sarvari Behzad Khalili |
author_sort | Mehdi Rimaz |
collection | DOAJ |
description | A fast and facile one-pot procedure for the preparation of symmetric 5-Aryloyl-1,9-dimethyl-5,9-dihydro-2H-pyrano[2,3-d:6,5-d']dipyrimidine-2,4,6,8(1H,3H,7H)-tetraone derivatives by two-component reaction of N-methylbarbituric acid and arylglyoxalmonohydrates catalyzed by DABCO in ethanol at 50 ºC is described. This protocol has the advantages of environmental friendless, very simple operation, high regio- and chemoselectivity and moderate to excellent yields. |
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institution | Directory Open Access Journal |
issn | 1927-7296 1927-730X |
language | English |
last_indexed | 2024-12-13T16:53:50Z |
publishDate | 2017-02-01 |
publisher | Growing Science |
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series | Current Chemistry Letters |
spelling | doaj.art-345ccef695e048259eea05c4020cc9892022-12-21T23:37:58ZengGrowing ScienceCurrent Chemistry Letters1927-72961927-730X2017-02-0162556810.5267/j.ccl.2016.12.001Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reactionMehdi RimazHossein MousaviMojgan BehnamLeila SarvariBehzad Khalili A fast and facile one-pot procedure for the preparation of symmetric 5-Aryloyl-1,9-dimethyl-5,9-dihydro-2H-pyrano[2,3-d:6,5-d']dipyrimidine-2,4,6,8(1H,3H,7H)-tetraone derivatives by two-component reaction of N-methylbarbituric acid and arylglyoxalmonohydrates catalyzed by DABCO in ethanol at 50 ºC is described. This protocol has the advantages of environmental friendless, very simple operation, high regio- and chemoselectivity and moderate to excellent yields.http://www.growingscience.com/ccl/Vol6/ccl_2016_21.pdfPyranodipyrimidinonesDABCOOne-potArylglyoxalmonohydrate |
spellingShingle | Mehdi Rimaz Hossein Mousavi Mojgan Behnam Leila Sarvari Behzad Khalili Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reaction Current Chemistry Letters Pyranodipyrimidinones DABCO One-pot Arylglyoxalmonohydrate |
title | Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reaction |
title_full | Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reaction |
title_fullStr | Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reaction |
title_full_unstemmed | Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reaction |
title_short | Fast and convenient synthesis of new symmetric pyrano[2,3-d:6,5-d']dipyrimidinones by an organocatalyzed annulation reaction |
title_sort | fast and convenient synthesis of new symmetric pyrano 2 3 d 6 5 d dipyrimidinones by an organocatalyzed annulation reaction |
topic | Pyranodipyrimidinones DABCO One-pot Arylglyoxalmonohydrate |
url | http://www.growingscience.com/ccl/Vol6/ccl_2016_21.pdf |
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