Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling Treatment

Effects of ball milling (BM) on the structure and physicochemical properties of three types of citrus fibers were investigated. With the extension of the grinding time, the particle size of citrus fibers significantly decreased. Fourier transform infrared spectroscopy (FTIR) showed that the three ci...

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Main Authors: Zhanmei Jiang, Minghan Zhang, Yuxuan Huang, Chenglong Ma, Sinan Mu, Hongyu Li, Xianqi Liu, Yue Ma, Yue Liu, Juncai Hou
Format: Article
Language:English
Published: MDPI AG 2022-09-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/11/17/2665
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author Zhanmei Jiang
Minghan Zhang
Yuxuan Huang
Chenglong Ma
Sinan Mu
Hongyu Li
Xianqi Liu
Yue Ma
Yue Liu
Juncai Hou
author_facet Zhanmei Jiang
Minghan Zhang
Yuxuan Huang
Chenglong Ma
Sinan Mu
Hongyu Li
Xianqi Liu
Yue Ma
Yue Liu
Juncai Hou
author_sort Zhanmei Jiang
collection DOAJ
description Effects of ball milling (BM) on the structure and physicochemical properties of three types of citrus fibers were investigated. With the extension of the grinding time, the particle size of citrus fibers significantly decreased. Fourier transform infrared spectroscopy (FTIR) showed that the three citrus fibers had similar chemical groups, and more -OH and phenolic acid groups were exposed after BM, and pectin and lignin were not degraded. Scanning electron microscope (SEM) results showed that the appearance of particles changed from spherical to fragmented, irregular shapes. The water holding capacity (WHC), oil holding capacity (OHC), and water swelling capacity (WSC) of citrus fibers LM, JK, and FS reached the maximum value after BM of 2 h (increasing by 18.5%), 4 h (increasing by 46.1%), and 10 h (increasing by 38.3%), respectively. After 10 h BM, citrus fibers FS and JK had the highest adsorption capacity of cholesterol and sodium cholate, increasing by 48.3% and 48.6%, respectively. This indicates that BM transforms the spatial structure of citrus fibers and improves their physicochemical properties.
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spelling doaj.art-3467b01477094f6f9f59036852c725332023-11-23T13:09:08ZengMDPI AGFoods2304-81582022-09-011117266510.3390/foods11172665Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling TreatmentZhanmei Jiang0Minghan Zhang1Yuxuan Huang2Chenglong Ma3Sinan Mu4Hongyu Li5Xianqi Liu6Yue Ma7Yue Liu8Juncai Hou9Key Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaKey Laboratory of Dairy Science, Ministry of Education, College of Food Science, Northeast Agricultural University, Harbin 150030, ChinaEffects of ball milling (BM) on the structure and physicochemical properties of three types of citrus fibers were investigated. With the extension of the grinding time, the particle size of citrus fibers significantly decreased. Fourier transform infrared spectroscopy (FTIR) showed that the three citrus fibers had similar chemical groups, and more -OH and phenolic acid groups were exposed after BM, and pectin and lignin were not degraded. Scanning electron microscope (SEM) results showed that the appearance of particles changed from spherical to fragmented, irregular shapes. The water holding capacity (WHC), oil holding capacity (OHC), and water swelling capacity (WSC) of citrus fibers LM, JK, and FS reached the maximum value after BM of 2 h (increasing by 18.5%), 4 h (increasing by 46.1%), and 10 h (increasing by 38.3%), respectively. After 10 h BM, citrus fibers FS and JK had the highest adsorption capacity of cholesterol and sodium cholate, increasing by 48.3% and 48.6%, respectively. This indicates that BM transforms the spatial structure of citrus fibers and improves their physicochemical properties.https://www.mdpi.com/2304-8158/11/17/2665citrus fiberball millingfunctional propertiesphysicochemical properties
spellingShingle Zhanmei Jiang
Minghan Zhang
Yuxuan Huang
Chenglong Ma
Sinan Mu
Hongyu Li
Xianqi Liu
Yue Ma
Yue Liu
Juncai Hou
Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling Treatment
Foods
citrus fiber
ball milling
functional properties
physicochemical properties
title Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling Treatment
title_full Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling Treatment
title_fullStr Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling Treatment
title_full_unstemmed Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling Treatment
title_short Comparison and Characterization of the Structure and Physicochemical Properties of Three Citrus Fibers: Effect of Ball Milling Treatment
title_sort comparison and characterization of the structure and physicochemical properties of three citrus fibers effect of ball milling treatment
topic citrus fiber
ball milling
functional properties
physicochemical properties
url https://www.mdpi.com/2304-8158/11/17/2665
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