Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy Nanocomposites

Common dispersion methods such as ultrasonic sonication, planetary centrifugal mixing and magnetic dispersion have been used extensively to achieve moderate exfoliation of nanoparticles in polymer matrix. In this study, the effect of adding three roll milling to these three dispersion methods for na...

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Main Authors: Mahesh V. Hosur, Victor A. Agubra, Peter S. Owuor
Format: Article
Language:English
Published: MDPI AG 2013-08-01
Series:Nanomaterials
Subjects:
Online Access:http://www.mdpi.com/2079-4991/3/3/550
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author Mahesh V. Hosur
Victor A. Agubra
Peter S. Owuor
author_facet Mahesh V. Hosur
Victor A. Agubra
Peter S. Owuor
author_sort Mahesh V. Hosur
collection DOAJ
description Common dispersion methods such as ultrasonic sonication, planetary centrifugal mixing and magnetic dispersion have been used extensively to achieve moderate exfoliation of nanoparticles in polymer matrix. In this study, the effect of adding three roll milling to these three dispersion methods for nanoclay dispersion into epoxy matrix was investigated. A combination of each of these mixing methods with three roll milling showed varying results relative to the unmodified polymer laminate. A significant exfoliation of the nanoparticles in the polymer structure was obtained by dispersing the nanoclay combining three roll milling to magnetic and planetary centrifugal mixing methods. This exfoliation promoted a stronger interfacial bond between the matrix and the fiber, which increased the final properties of the E-glass/epoxy nanocomposite. However, a combination of ultrasound sonication and three roll milling on the other hand, resulted in poor clay exfoliation; the sonication process degraded the polymer network, which adversely affected the nanocomposite final properties relative to the unmodified E-glass/epoxy polymer.
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spelling doaj.art-347797e101524ef69b17fb8ada8e72422022-12-22T01:41:32ZengMDPI AGNanomaterials2079-49912013-08-013355056310.3390/nano3030550Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy NanocompositesMahesh V. HosurVictor A. AgubraPeter S. OwuorCommon dispersion methods such as ultrasonic sonication, planetary centrifugal mixing and magnetic dispersion have been used extensively to achieve moderate exfoliation of nanoparticles in polymer matrix. In this study, the effect of adding three roll milling to these three dispersion methods for nanoclay dispersion into epoxy matrix was investigated. A combination of each of these mixing methods with three roll milling showed varying results relative to the unmodified polymer laminate. A significant exfoliation of the nanoparticles in the polymer structure was obtained by dispersing the nanoclay combining three roll milling to magnetic and planetary centrifugal mixing methods. This exfoliation promoted a stronger interfacial bond between the matrix and the fiber, which increased the final properties of the E-glass/epoxy nanocomposite. However, a combination of ultrasound sonication and three roll milling on the other hand, resulted in poor clay exfoliation; the sonication process degraded the polymer network, which adversely affected the nanocomposite final properties relative to the unmodified E-glass/epoxy polymer.http://www.mdpi.com/2079-4991/3/3/550nanoclaysnanocompositesmechanical propertiesdispersion methods
spellingShingle Mahesh V. Hosur
Victor A. Agubra
Peter S. Owuor
Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy Nanocomposites
Nanomaterials
nanoclays
nanocomposites
mechanical properties
dispersion methods
title Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy Nanocomposites
title_full Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy Nanocomposites
title_fullStr Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy Nanocomposites
title_full_unstemmed Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy Nanocomposites
title_short Influence of Nanoclay Dispersion Methods on the Mechanical Behavior of E-Glass/Epoxy Nanocomposites
title_sort influence of nanoclay dispersion methods on the mechanical behavior of e glass epoxy nanocomposites
topic nanoclays
nanocomposites
mechanical properties
dispersion methods
url http://www.mdpi.com/2079-4991/3/3/550
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