Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness

The widely adopted temperature for solid solution heat treatment (ST) for the conventionally fabricated Inconel 718 is 1100 °C for a hold time of 1 h or less. This ST scheme is, however, not enough to dissolve Laves and annihilate dislocations completely in samples fabricated with Laser metal powder...

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Main Authors: Wakshum M. Tucho, Vidar Hansen
Format: Article
Language:English
Published: MDPI AG 2021-02-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/11/2/266
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author Wakshum M. Tucho
Vidar Hansen
author_facet Wakshum M. Tucho
Vidar Hansen
author_sort Wakshum M. Tucho
collection DOAJ
description The widely adopted temperature for solid solution heat treatment (ST) for the conventionally fabricated Inconel 718 is 1100 °C for a hold time of 1 h or less. This ST scheme is, however, not enough to dissolve Laves and annihilate dislocations completely in samples fabricated with Laser metal powder bed fusion (L-PBF) additive manufacturing (AM)-Inconel 718. Despite this, the highest hardness obtained after aging for ST temperatures (970–1250 °C) is at 1100 °C/1 as we have ascertained in our previous studies. The unreleased residual stresses in the retained lattice defects potentially affect other properties of the material. Hence, this work aims to investigate if a longer hold time of ST at 1100 °C will lead to complete recrystallization while maintaining the hardness after aging or not. For this study, L-PBF-Inconel 718 samples were ST at 1100 °C at various hold times (1, 3, 6, 9, 16, or 24 h) and aged to study the effects on microstructure and hardness. In addition, a sample was directly aged to study the effects of bypassing ST. The samples (ST and aged) gain hardness by 43–49%. The high density of annealing twins evolved during 3 h of ST and only slightly varies for longer ST.
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spelling doaj.art-3497fd2aad594caab5e81e02e656d9ba2023-12-03T12:21:52ZengMDPI AGMetals2075-47012021-02-0111226610.3390/met11020266Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and HardnessWakshum M. Tucho0Vidar Hansen1Department of Mechanical and Structural Engineering and Materials Science, Faculty of Science and Technology, University of Stavanger, 4036 Stavanger, NorwayDepartment of Mechanical and Structural Engineering and Materials Science, Faculty of Science and Technology, University of Stavanger, 4036 Stavanger, NorwayThe widely adopted temperature for solid solution heat treatment (ST) for the conventionally fabricated Inconel 718 is 1100 °C for a hold time of 1 h or less. This ST scheme is, however, not enough to dissolve Laves and annihilate dislocations completely in samples fabricated with Laser metal powder bed fusion (L-PBF) additive manufacturing (AM)-Inconel 718. Despite this, the highest hardness obtained after aging for ST temperatures (970–1250 °C) is at 1100 °C/1 as we have ascertained in our previous studies. The unreleased residual stresses in the retained lattice defects potentially affect other properties of the material. Hence, this work aims to investigate if a longer hold time of ST at 1100 °C will lead to complete recrystallization while maintaining the hardness after aging or not. For this study, L-PBF-Inconel 718 samples were ST at 1100 °C at various hold times (1, 3, 6, 9, 16, or 24 h) and aged to study the effects on microstructure and hardness. In addition, a sample was directly aged to study the effects of bypassing ST. The samples (ST and aged) gain hardness by 43–49%. The high density of annealing twins evolved during 3 h of ST and only slightly varies for longer ST.https://www.mdpi.com/2075-4701/11/2/266laser metal powder bed fusion (L-PBF)Inconel 718microstructurehardnessheat treatmentrecrystallization
spellingShingle Wakshum M. Tucho
Vidar Hansen
Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness
Metals
laser metal powder bed fusion (L-PBF)
Inconel 718
microstructure
hardness
heat treatment
recrystallization
title Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness
title_full Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness
title_fullStr Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness
title_full_unstemmed Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness
title_short Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness
title_sort studies of post fabrication heat treatment of l pbf inconel 718 effects of hold time on microstructure annealing twins and hardness
topic laser metal powder bed fusion (L-PBF)
Inconel 718
microstructure
hardness
heat treatment
recrystallization
url https://www.mdpi.com/2075-4701/11/2/266
work_keys_str_mv AT wakshummtucho studiesofpostfabricationheattreatmentoflpbfinconel718effectsofholdtimeonmicrostructureannealingtwinsandhardness
AT vidarhansen studiesofpostfabricationheattreatmentoflpbfinconel718effectsofholdtimeonmicrostructureannealingtwinsandhardness