Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics

Butter may be adulterated with cheaper animal fats, such as chicken fat (CF). Thus, the detection and quantification of butter adulteration with CF was monitored using Fourier transform infrared (FTIR) spectroscopy, combined with chemometric of partial least square (PLS) at the frequency regions of...

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Main Authors: A. F. Nurrulhidayah, A. Rohman, I. Amin, M. Shuhaimi, A. Khatib
Format: Article
Language:English
Published: Consejo Superior de Investigaciones Científicas 2013-09-01
Series:Grasas y Aceites
Subjects:
Online Access:http://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/1440
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author A. F. Nurrulhidayah
A. Rohman
I. Amin
M. Shuhaimi
A. Khatib
author_facet A. F. Nurrulhidayah
A. Rohman
I. Amin
M. Shuhaimi
A. Khatib
author_sort A. F. Nurrulhidayah
collection DOAJ
description Butter may be adulterated with cheaper animal fats, such as chicken fat (CF). Thus, the detection and quantification of butter adulteration with CF was monitored using Fourier transform infrared (FTIR) spectroscopy, combined with chemometric of partial least square (PLS) at the frequency regions of 1200-1000cm–1. FTIR measurements were made on pure butter and that adulterated with varying concentrations of CF (0-100% w/w in butter). PLS calibration exhibits a good relationship between actual and FTIR predicted values of CF with a coefficient of determination (R2) of 0.981. The root means standard error of calibration (RMSEC) and during cross validation (RMSECV) obtained using six principal components (PCs) are 2.08 and 4.33% v/v, respectively.
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spelling doaj.art-34fa4eb458d04fc2bab7ed4dd39e94062022-12-21T18:50:46ZengConsejo Superior de Investigaciones CientíficasGrasas y Aceites0017-34951988-42142013-09-0164434935510.3989/gya.0728121408Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometricsA. F. Nurrulhidayah0A. Rohman1I. Amin2M. Shuhaimi3A. Khatib4Laboratory of Halal Science Research, Halal Products Research Institute, Universiti Putra MalaysiaResearch Center of Halal Products and Faculty of Pharmacy, Gadjah Mada UniversityLaboratory of Halal Science Research, Halal Products Research Institute, Universiti Putra Malaysia - Department of Nutrition and Dietetics, Faculty of Medicine and Health Sciences, Universiti Putra MalaysiaLaboratory of Halal Science Research, Halal Products Research Institute, Universiti Putra MalaysiaLaboratory of Natural Product, Institute of Bioscience, Universiti Putra Malaysia - Faculty of Food Science and Technology, Universiti Putra MalaysiaButter may be adulterated with cheaper animal fats, such as chicken fat (CF). Thus, the detection and quantification of butter adulteration with CF was monitored using Fourier transform infrared (FTIR) spectroscopy, combined with chemometric of partial least square (PLS) at the frequency regions of 1200-1000cm–1. FTIR measurements were made on pure butter and that adulterated with varying concentrations of CF (0-100% w/w in butter). PLS calibration exhibits a good relationship between actual and FTIR predicted values of CF with a coefficient of determination (R2) of 0.981. The root means standard error of calibration (RMSEC) and during cross validation (RMSECV) obtained using six principal components (PCs) are 2.08 and 4.33% v/v, respectively.http://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/1440animal fatbutterchemometricsftir spectroscopymultivariate calibration
spellingShingle A. F. Nurrulhidayah
A. Rohman
I. Amin
M. Shuhaimi
A. Khatib
Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
Grasas y Aceites
animal fat
butter
chemometrics
ftir spectroscopy
multivariate calibration
title Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
title_full Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
title_fullStr Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
title_full_unstemmed Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
title_short Analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
title_sort analysis of chicken fat as adulterant in butter using fourier transform infrared spectroscopy and chemometrics
topic animal fat
butter
chemometrics
ftir spectroscopy
multivariate calibration
url http://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/1440
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AT iamin analysisofchickenfatasadulterantinbutterusingfouriertransforminfraredspectroscopyandchemometrics
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