Synthesis,Characterization and Properties of Ag/InP Composites

InP microcrystal was successfully synthesized <i>via</i> a facile hydrothermal route, and then Ag nanoparticles were loaded on the surface of InP microcrystal using UV lamp to reduce silver versions. The as-prepared composites were characterized by X-ray diffraction (XRD) and field-emiss...

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Main Authors: LIU Shu-ling, HAN Xiao-li, TONG Jian-bo
Format: Article
Language:zho
Published: Journal of Materials Engineering 2017-10-01
Series:Cailiao gongcheng
Subjects:
Online Access:http://jme.biam.ac.cn/CN/Y2017/V45/I10/18
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author LIU Shu-ling
HAN Xiao-li
TONG Jian-bo
author_facet LIU Shu-ling
HAN Xiao-li
TONG Jian-bo
author_sort LIU Shu-ling
collection DOAJ
description InP microcrystal was successfully synthesized <i>via</i> a facile hydrothermal route, and then Ag nanoparticles were loaded on the surface of InP microcrystal using UV lamp to reduce silver versions. The as-prepared composites were characterized by X-ray diffraction (XRD) and field-emission scanning electron microscopy (FE-SEM). The results show that Ag/InP composite is composed of lots of spherical microcrystals with a size of 500nm and Ag nanoparticles with a diameter of 20 nm loaded uniformly on the surface of cubic phase InP microspheres,the surface is rough. Using Congo red as model organic pollutant, the photo-catalytic performance of Ag/InP microspheres is further detected by fluorescence and UV-vis spectra. It is found that the as-prepared composite exhibits a superior photo-catalytic degradation activity as compared to InP, which might be the effective separation of electrons and holes after Ag nanoparticles loaded on the surface of InP microspheres.In addition,the photo-catalytic performance of Ag/InP microspheres with different Ag loads was studied,and the results show that when the loading is 73.3%,the photocatalytic activity of the product is the best,and the degradation rate is 64%.
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spelling doaj.art-356213c9cf374aa28b6ef363edc5f09d2023-01-03T01:57:56ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43811001-43812017-10-014510182210.11868/j.issn.1001-4381.2016.001198201710001198Synthesis,Characterization and Properties of Ag/InP CompositesLIU Shu-ling0HAN Xiao-li1TONG Jian-bo2Key Laboratory of Auxiliary Chemistry and Technology for Chemical Industry(Ministry of Education), Shaanxi University of Science and Technology, Xi'an 710021, ChinaKey Laboratory of Auxiliary Chemistry and Technology for Chemical Industry(Ministry of Education), Shaanxi University of Science and Technology, Xi'an 710021, ChinaKey Laboratory of Auxiliary Chemistry and Technology for Chemical Industry(Ministry of Education), Shaanxi University of Science and Technology, Xi'an 710021, ChinaInP microcrystal was successfully synthesized <i>via</i> a facile hydrothermal route, and then Ag nanoparticles were loaded on the surface of InP microcrystal using UV lamp to reduce silver versions. The as-prepared composites were characterized by X-ray diffraction (XRD) and field-emission scanning electron microscopy (FE-SEM). The results show that Ag/InP composite is composed of lots of spherical microcrystals with a size of 500nm and Ag nanoparticles with a diameter of 20 nm loaded uniformly on the surface of cubic phase InP microspheres,the surface is rough. Using Congo red as model organic pollutant, the photo-catalytic performance of Ag/InP microspheres is further detected by fluorescence and UV-vis spectra. It is found that the as-prepared composite exhibits a superior photo-catalytic degradation activity as compared to InP, which might be the effective separation of electrons and holes after Ag nanoparticles loaded on the surface of InP microspheres.In addition,the photo-catalytic performance of Ag/InP microspheres with different Ag loads was studied,and the results show that when the loading is 73.3%,the photocatalytic activity of the product is the best,and the degradation rate is 64%.http://jme.biam.ac.cn/CN/Y2017/V45/I10/18Ag/InPfluorescene spectroscopyphoto-catalytic performancecomposite
spellingShingle LIU Shu-ling
HAN Xiao-li
TONG Jian-bo
Synthesis,Characterization and Properties of Ag/InP Composites
Cailiao gongcheng
Ag/InP
fluorescene spectroscopy
photo-catalytic performance
composite
title Synthesis,Characterization and Properties of Ag/InP Composites
title_full Synthesis,Characterization and Properties of Ag/InP Composites
title_fullStr Synthesis,Characterization and Properties of Ag/InP Composites
title_full_unstemmed Synthesis,Characterization and Properties of Ag/InP Composites
title_short Synthesis,Characterization and Properties of Ag/InP Composites
title_sort synthesis characterization and properties of ag inp composites
topic Ag/InP
fluorescene spectroscopy
photo-catalytic performance
composite
url http://jme.biam.ac.cn/CN/Y2017/V45/I10/18
work_keys_str_mv AT liushuling synthesischaracterizationandpropertiesofaginpcomposites
AT hanxiaoli synthesischaracterizationandpropertiesofaginpcomposites
AT tongjianbo synthesischaracterizationandpropertiesofaginpcomposites