Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloy

Due to the effective precipitation strengthening effect of the β′ phase, Mg-Gd alloys exhibit excellent room temperature mechanical behaviors. However, when served at high temperatures, the metastable β′ phase will transform to other phases, resulting in severe performance degradation. In this study...

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Main Authors: Shuxia Ouyang, Guangyu Yang, He Qin, Chunhui Wang, Shifeng Luo, Wanqi Jie
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2022-12-01
Series:Journal of Magnesium and Alloys
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2213956721001602
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author Shuxia Ouyang
Guangyu Yang
He Qin
Chunhui Wang
Shifeng Luo
Wanqi Jie
author_facet Shuxia Ouyang
Guangyu Yang
He Qin
Chunhui Wang
Shifeng Luo
Wanqi Jie
author_sort Shuxia Ouyang
collection DOAJ
description Due to the effective precipitation strengthening effect of the β′ phase, Mg-Gd alloys exhibit excellent room temperature mechanical behaviors. However, when served at high temperatures, the metastable β′ phase will transform to other phases, resulting in severe performance degradation. In this study, we investigated the effect of precipitation state achieved by different heat treatments on high temperature tensile and creep behaviors of the Mg-15Gd alloy by comparing the properties of the as-cast, solid-solutioned (T4) and peak-aged (T6) alloys. The results showed that the tensile mechanical properties of the T6 alloy were always highest from room temperature to 300 °C, in spite of an abnormal strength increase with temperature existed in the T4 alloy. For tensile creep properties, the T6 alloy exhibited the lowest steady creep rate below 235 °C while the T4 alloy possessed the best properties above 260 °C. Microstructure characterization revealed that the transition was caused by the stress-promoted precipitation of β′ phase in the T4 alloy and rapid phase transformation in the T6 alloy at high temperatures. At 260 °C, the calculated stress exponent n was 3.1 and 2.8 for the T4 and T6 alloys, respectively, suggesting the creep deformation mechanism was dislocation slip, which was further confirmed by the microstructure after creeping. Our findings can provide new insights into the heat treatment process of Mg-Gd alloys served at high temperatures.
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spelling doaj.art-35d9b05fd8864dce9b056869c61826be2024-04-27T02:44:46ZengKeAi Communications Co., Ltd.Journal of Magnesium and Alloys2213-95672022-12-01101234593469Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloyShuxia Ouyang0Guangyu Yang1He Qin2Chunhui Wang3Shifeng Luo4Wanqi Jie5State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, ChinaCorresponding author.; State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, ChinaDue to the effective precipitation strengthening effect of the β′ phase, Mg-Gd alloys exhibit excellent room temperature mechanical behaviors. However, when served at high temperatures, the metastable β′ phase will transform to other phases, resulting in severe performance degradation. In this study, we investigated the effect of precipitation state achieved by different heat treatments on high temperature tensile and creep behaviors of the Mg-15Gd alloy by comparing the properties of the as-cast, solid-solutioned (T4) and peak-aged (T6) alloys. The results showed that the tensile mechanical properties of the T6 alloy were always highest from room temperature to 300 °C, in spite of an abnormal strength increase with temperature existed in the T4 alloy. For tensile creep properties, the T6 alloy exhibited the lowest steady creep rate below 235 °C while the T4 alloy possessed the best properties above 260 °C. Microstructure characterization revealed that the transition was caused by the stress-promoted precipitation of β′ phase in the T4 alloy and rapid phase transformation in the T6 alloy at high temperatures. At 260 °C, the calculated stress exponent n was 3.1 and 2.8 for the T4 and T6 alloys, respectively, suggesting the creep deformation mechanism was dislocation slip, which was further confirmed by the microstructure after creeping. Our findings can provide new insights into the heat treatment process of Mg-Gd alloys served at high temperatures.http://www.sciencedirect.com/science/article/pii/S2213956721001602Mg-Gd alloysPrecipitation stateHigh temperature tensile propertiesTensile creep behaviorsStress-promoted precipitation
spellingShingle Shuxia Ouyang
Guangyu Yang
He Qin
Chunhui Wang
Shifeng Luo
Wanqi Jie
Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloy
Journal of Magnesium and Alloys
Mg-Gd alloys
Precipitation state
High temperature tensile properties
Tensile creep behaviors
Stress-promoted precipitation
title Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloy
title_full Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloy
title_fullStr Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloy
title_full_unstemmed Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloy
title_short Effect of the precipitation state on high temperature tensile and creep behaviors of Mg-15Gd alloy
title_sort effect of the precipitation state on high temperature tensile and creep behaviors of mg 15gd alloy
topic Mg-Gd alloys
Precipitation state
High temperature tensile properties
Tensile creep behaviors
Stress-promoted precipitation
url http://www.sciencedirect.com/science/article/pii/S2213956721001602
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AT heqin effectoftheprecipitationstateonhightemperaturetensileandcreepbehaviorsofmg15gdalloy
AT chunhuiwang effectoftheprecipitationstateonhightemperaturetensileandcreepbehaviorsofmg15gdalloy
AT shifengluo effectoftheprecipitationstateonhightemperaturetensileandcreepbehaviorsofmg15gdalloy
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