Synthesis of functional nanocrystallites through reactive thermal plasma processing

A method of synthesizing functional nanostructured powders through reactive thermal plasma processing has been developed. The synthesis of nanosized titanium oxide powders was performed by the oxidation of solid and liquid precursors. Quench gases, either injected from the shoulder of the reactor or...

Full description

Bibliographic Details
Main Author: Takamasa Ishigaki and Ji-Guang Li
Format: Article
Language:English
Published: Taylor & Francis Group 2007-01-01
Series:Science and Technology of Advanced Materials
Online Access:http://www.iop.org/EJ/abstract/1468-6996/8/7-8/A11
_version_ 1818179373542408192
author Takamasa Ishigaki and Ji-Guang Li
author_facet Takamasa Ishigaki and Ji-Guang Li
author_sort Takamasa Ishigaki and Ji-Guang Li
collection DOAJ
description A method of synthesizing functional nanostructured powders through reactive thermal plasma processing has been developed. The synthesis of nanosized titanium oxide powders was performed by the oxidation of solid and liquid precursors. Quench gases, either injected from the shoulder of the reactor or injected counter to the plasma plume from the bottom of the reactor, were used to vary the quench rate, and therefore the particle size, of the resultant powders. The experimental results are well supported by numerical analysis on the effects of the quench gas on the flow pattern and temperature field of the thermal plasma as well as on the trajectory and temperature history of the particles. The plasma-synthesized TiO2 nanoparticles showed phase preferences different from those synthesized by conventional wet-chemical processes. Nanosized particles of high crystallinity and nonequilibrium chemical composition were formed in one step via reactive thermal plasma processing.
first_indexed 2024-12-11T21:02:51Z
format Article
id doaj.art-35e8eb778fe2495a81eebb2fc5fc98b5
institution Directory Open Access Journal
issn 1468-6996
1878-5514
language English
last_indexed 2024-12-11T21:02:51Z
publishDate 2007-01-01
publisher Taylor & Francis Group
record_format Article
series Science and Technology of Advanced Materials
spelling doaj.art-35e8eb778fe2495a81eebb2fc5fc98b52022-12-22T00:50:56ZengTaylor & Francis GroupScience and Technology of Advanced Materials1468-69961878-55142007-01-0187-8617Synthesis of functional nanocrystallites through reactive thermal plasma processingTakamasa Ishigaki and Ji-Guang LiA method of synthesizing functional nanostructured powders through reactive thermal plasma processing has been developed. The synthesis of nanosized titanium oxide powders was performed by the oxidation of solid and liquid precursors. Quench gases, either injected from the shoulder of the reactor or injected counter to the plasma plume from the bottom of the reactor, were used to vary the quench rate, and therefore the particle size, of the resultant powders. The experimental results are well supported by numerical analysis on the effects of the quench gas on the flow pattern and temperature field of the thermal plasma as well as on the trajectory and temperature history of the particles. The plasma-synthesized TiO2 nanoparticles showed phase preferences different from those synthesized by conventional wet-chemical processes. Nanosized particles of high crystallinity and nonequilibrium chemical composition were formed in one step via reactive thermal plasma processing.http://www.iop.org/EJ/abstract/1468-6996/8/7-8/A11
spellingShingle Takamasa Ishigaki and Ji-Guang Li
Synthesis of functional nanocrystallites through reactive thermal plasma processing
Science and Technology of Advanced Materials
title Synthesis of functional nanocrystallites through reactive thermal plasma processing
title_full Synthesis of functional nanocrystallites through reactive thermal plasma processing
title_fullStr Synthesis of functional nanocrystallites through reactive thermal plasma processing
title_full_unstemmed Synthesis of functional nanocrystallites through reactive thermal plasma processing
title_short Synthesis of functional nanocrystallites through reactive thermal plasma processing
title_sort synthesis of functional nanocrystallites through reactive thermal plasma processing
url http://www.iop.org/EJ/abstract/1468-6996/8/7-8/A11
work_keys_str_mv AT takamasaishigakiandjiguangli synthesisoffunctionalnanocrystallitesthroughreactivethermalplasmaprocessing