Elemental analysis of coffee: a comparison of ICP-MS and AAS methods

We determined the mineral nutrients and toxic elements (Ca, Cu, Fe, Mg, Zn, Cd, Cr, Mn, Ni, and Pb) in five types of coffee by atomic absorption spectrometry and inductively coupled plasma mass spectrometry. The decomposition of the samples took place in a microwave digestion system with HNO3 and H2...

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Main Authors: Monika Jarošová, David Milde, Martin Kuba
Format: Article
Language:English
Published: Czech Academy of Agricultural Sciences 2014-08-01
Series:Czech Journal of Food Sciences
Subjects:
Online Access:https://cjfs.agriculturejournals.cz/artkey/cjf-201404-0007_elemental-analysis-of-coffee-a-comparison-of-icp-ms-and-aas-methods.php
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author Monika Jarošová
David Milde
Martin Kuba
author_facet Monika Jarošová
David Milde
Martin Kuba
author_sort Monika Jarošová
collection DOAJ
description We determined the mineral nutrients and toxic elements (Ca, Cu, Fe, Mg, Zn, Cd, Cr, Mn, Ni, and Pb) in five types of coffee by atomic absorption spectrometry and inductively coupled plasma mass spectrometry. The decomposition of the samples took place in a microwave digestion system with HNO3 and H2O2 reagents. Partial validation of the method was performed by using the certified reference material (NCS ZC 73014). Univariate and multivariate statistical methods were used to compare both the coffee samples and the techniques used. No significant differences were found between two used methods. Significant differences occurred between the coffee samples but only the application of multivariate statistics helps to distinguish among samples from different locations.
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spelling doaj.art-35ec9afeb1bc457185a203c80ffee3ac2023-02-23T03:28:07ZengCzech Academy of Agricultural SciencesCzech Journal of Food Sciences1212-18001805-93172014-08-0132435435910.17221/399/2013-CJFScjf-201404-0007Elemental analysis of coffee: a comparison of ICP-MS and AAS methodsMonika Jarošová0David Milde1Martin Kuba2Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacký University in Olomouc, Czech RepublicRegional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacký University in Olomouc, Czech RepublicRegional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacký University in Olomouc, Czech RepublicWe determined the mineral nutrients and toxic elements (Ca, Cu, Fe, Mg, Zn, Cd, Cr, Mn, Ni, and Pb) in five types of coffee by atomic absorption spectrometry and inductively coupled plasma mass spectrometry. The decomposition of the samples took place in a microwave digestion system with HNO3 and H2O2 reagents. Partial validation of the method was performed by using the certified reference material (NCS ZC 73014). Univariate and multivariate statistical methods were used to compare both the coffee samples and the techniques used. No significant differences were found between two used methods. Significant differences occurred between the coffee samples but only the application of multivariate statistics helps to distinguish among samples from different locations.https://cjfs.agriculturejournals.cz/artkey/cjf-201404-0007_elemental-analysis-of-coffee-a-comparison-of-icp-ms-and-aas-methods.phpcoffea arabicaatomic absorption spectrometryinductively coupled plasma mass spectrometry metalsunivariate statisticsmultivariate statistics
spellingShingle Monika Jarošová
David Milde
Martin Kuba
Elemental analysis of coffee: a comparison of ICP-MS and AAS methods
Czech Journal of Food Sciences
coffea arabica
atomic absorption spectrometry
inductively coupled plasma mass spectrometry metals
univariate statistics
multivariate statistics
title Elemental analysis of coffee: a comparison of ICP-MS and AAS methods
title_full Elemental analysis of coffee: a comparison of ICP-MS and AAS methods
title_fullStr Elemental analysis of coffee: a comparison of ICP-MS and AAS methods
title_full_unstemmed Elemental analysis of coffee: a comparison of ICP-MS and AAS methods
title_short Elemental analysis of coffee: a comparison of ICP-MS and AAS methods
title_sort elemental analysis of coffee a comparison of icp ms and aas methods
topic coffea arabica
atomic absorption spectrometry
inductively coupled plasma mass spectrometry metals
univariate statistics
multivariate statistics
url https://cjfs.agriculturejournals.cz/artkey/cjf-201404-0007_elemental-analysis-of-coffee-a-comparison-of-icp-ms-and-aas-methods.php
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AT davidmilde elementalanalysisofcoffeeacomparisonoficpmsandaasmethods
AT martinkuba elementalanalysisofcoffeeacomparisonoficpmsandaasmethods