Validation of the stamping method for CaSO4:RE + Teflon® pellets production

The IPEN method for the CaSO4:RE + Teflon® production, developed and patented at the Dosimetric Materials Laboratory – LMD/IPEN in the earlier 1980’s, [1] is highly time-demanding, so that the use of the stamping method, already widely industrially applied, would enhance the CaSO4:RE + Teflon® pelle...

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Main Authors: Maira Goes Nunes, Leticia Lucente Campos
Format: Article
Language:English
Published: Brazilian Radiation Protection Society (Sociedade Brasileira de Proteção Radiológica, SBPR) 2015-05-01
Series:Brazilian Journal of Radiation Sciences
Subjects:
Online Access:https://bjrs.org.br/revista/index.php/REVISTA/article/view/170
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author Maira Goes Nunes
Leticia Lucente Campos
author_facet Maira Goes Nunes
Leticia Lucente Campos
author_sort Maira Goes Nunes
collection DOAJ
description The IPEN method for the CaSO4:RE + Teflon® production, developed and patented at the Dosimetric Materials Laboratory – LMD/IPEN in the earlier 1980’s, [1] is highly time-demanding, so that the use of the stamping method, already widely industrially applied, would enhance the CaSO4:RE + Teflon® pellets production. Thus, validating the stamping method, by comparing the dosimetric properties of a batch of pellets produced by each method, became a must. The stamped batch presents the same mean non-irradiated signals either after sintering or annealing while IPEN batch mean non-irradiated signals vary in 23%. The mean TL signal after irradiation was about 50 nC, but the standard deviation varies from 20% to 33% for IPEN batch and keeps in 10% for the stamped batch. 24 h after the irradiation, the TL signal decreased to about 35 nC, with no differences in IPEN batch standard deviation and a decrease to 5% in stamped batch standard deviation, for the five performed essays. Calibration curves present a linear behavior over the entire studied dose range and the same coefficients for both methods, however, the uncertainties in the coefficients determined to the calibration curve obtained with stamped pellets are significantly smaller, leading to a more precise dose determination. This results show that the stamping method produces more homogeneous batches, with pellets that maintain the dosimetric characteristics of the detectors produced by IPEN method, in such a way that the stamping method can substitute with advantages the IPEN method in the CaSO4:RE + Teflon® dosimetric pellets production.
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spelling doaj.art-362804fab66f425ba039683c5fc13c232022-12-22T02:27:04ZengBrazilian Radiation Protection Society (Sociedade Brasileira de Proteção Radiológica, SBPR)Brazilian Journal of Radiation Sciences2319-06122015-05-0131A10.15392/bjrs.v3i1A.170Validation of the stamping method for CaSO4:RE + Teflon® pellets productionMaira Goes Nunes0Leticia Lucente Campos1Instituto de Pesquisas Energéticas e NuclearesInstituto de Pesquisas Energéticas e NuclearesThe IPEN method for the CaSO4:RE + Teflon® production, developed and patented at the Dosimetric Materials Laboratory – LMD/IPEN in the earlier 1980’s, [1] is highly time-demanding, so that the use of the stamping method, already widely industrially applied, would enhance the CaSO4:RE + Teflon® pellets production. Thus, validating the stamping method, by comparing the dosimetric properties of a batch of pellets produced by each method, became a must. The stamped batch presents the same mean non-irradiated signals either after sintering or annealing while IPEN batch mean non-irradiated signals vary in 23%. The mean TL signal after irradiation was about 50 nC, but the standard deviation varies from 20% to 33% for IPEN batch and keeps in 10% for the stamped batch. 24 h after the irradiation, the TL signal decreased to about 35 nC, with no differences in IPEN batch standard deviation and a decrease to 5% in stamped batch standard deviation, for the five performed essays. Calibration curves present a linear behavior over the entire studied dose range and the same coefficients for both methods, however, the uncertainties in the coefficients determined to the calibration curve obtained with stamped pellets are significantly smaller, leading to a more precise dose determination. This results show that the stamping method produces more homogeneous batches, with pellets that maintain the dosimetric characteristics of the detectors produced by IPEN method, in such a way that the stamping method can substitute with advantages the IPEN method in the CaSO4:RE + Teflon® dosimetric pellets production. https://bjrs.org.br/revista/index.php/REVISTA/article/view/170Thermoluminescent DosimeterThermoluminescent DosimetryRadiometry.
spellingShingle Maira Goes Nunes
Leticia Lucente Campos
Validation of the stamping method for CaSO4:RE + Teflon® pellets production
Brazilian Journal of Radiation Sciences
Thermoluminescent Dosimeter
Thermoluminescent Dosimetry
Radiometry.
title Validation of the stamping method for CaSO4:RE + Teflon® pellets production
title_full Validation of the stamping method for CaSO4:RE + Teflon® pellets production
title_fullStr Validation of the stamping method for CaSO4:RE + Teflon® pellets production
title_full_unstemmed Validation of the stamping method for CaSO4:RE + Teflon® pellets production
title_short Validation of the stamping method for CaSO4:RE + Teflon® pellets production
title_sort validation of the stamping method for caso4 re teflon r pellets production
topic Thermoluminescent Dosimeter
Thermoluminescent Dosimetry
Radiometry.
url https://bjrs.org.br/revista/index.php/REVISTA/article/view/170
work_keys_str_mv AT mairagoesnunes validationofthestampingmethodforcaso4reteflonpelletsproduction
AT leticialucentecampos validationofthestampingmethodforcaso4reteflonpelletsproduction