Microstructure Evolution in a GOES Thin Strip

This paper focuses on the evolution of the microstructure in a grain-oriented electrical steel (GOES) thin strip after casting. After solidification, the microstructure consisted of delta-ferrite. A small fraction of austenite was formed during the cooling of the thin strip in the two-phase region (...

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Main Authors: Anastasia Volodarskaja, Kryštof Hradečný, Renáta Palupčíková, Petra Váňová, Vlastimil Vodárek
Format: Article
Language:English
Published: MDPI AG 2022-12-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/13/1/51
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author Anastasia Volodarskaja
Kryštof Hradečný
Renáta Palupčíková
Petra Váňová
Vlastimil Vodárek
author_facet Anastasia Volodarskaja
Kryštof Hradečný
Renáta Palupčíková
Petra Váňová
Vlastimil Vodárek
author_sort Anastasia Volodarskaja
collection DOAJ
description This paper focuses on the evolution of the microstructure in a grain-oriented electrical steel (GOES) thin strip after casting. After solidification, the microstructure consisted of delta-ferrite. A small fraction of austenite was formed during the cooling of the thin strip in the two-phase region (gamma+delta). Fine Cr<sub>2</sub>CuS<sub>4</sub> particles precipitated in the ferrite and along the delta/gamma interfaces. Laths of primary Widmanstätten austenite (WA) nucleated directly on the high-angle delta-ferrite grain boundaries. The formation of WA laths in both adjacent ferritic grains resulted in a zig-zag shape of delta-ferrite grain boundaries due to their local rotation during austenite nucleation. Based on the EBSD results, a mechanism of the formation of the zig-zag grain boundaries has been proposed. Besides the Widmanstätten morphology, austenite also formed as films along the delta-ferrite grain boundaries. Sulfide precipitation along the delta/gamma interfaces made it possible to prove that austenite decomposition upon a drop in temperature was initiated by the formation of epitaxial ferrite. Further cooling brought the decay of austenite to either pearlite or a mixture of plate martensite and some retained austenite.
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spelling doaj.art-36c624bd18764e97a82c1b2b3593b6332023-11-30T23:30:02ZengMDPI AGMetals2075-47012022-12-011315110.3390/met13010051Microstructure Evolution in a GOES Thin StripAnastasia Volodarskaja0Kryštof Hradečný1Renáta Palupčíková2Petra Váňová3Vlastimil Vodárek4Faculty of Materials Science and Technology, VŠB—Technical University of Ostrava, 17. listopadu 2172/15, 708 00 Ostrava, Czech RepublicFaculty of Materials Science and Technology, VŠB—Technical University of Ostrava, 17. listopadu 2172/15, 708 00 Ostrava, Czech RepublicFaculty of Materials Science and Technology, VŠB—Technical University of Ostrava, 17. listopadu 2172/15, 708 00 Ostrava, Czech RepublicFaculty of Materials Science and Technology, VŠB—Technical University of Ostrava, 17. listopadu 2172/15, 708 00 Ostrava, Czech RepublicFaculty of Materials Science and Technology, VŠB—Technical University of Ostrava, 17. listopadu 2172/15, 708 00 Ostrava, Czech RepublicThis paper focuses on the evolution of the microstructure in a grain-oriented electrical steel (GOES) thin strip after casting. After solidification, the microstructure consisted of delta-ferrite. A small fraction of austenite was formed during the cooling of the thin strip in the two-phase region (gamma+delta). Fine Cr<sub>2</sub>CuS<sub>4</sub> particles precipitated in the ferrite and along the delta/gamma interfaces. Laths of primary Widmanstätten austenite (WA) nucleated directly on the high-angle delta-ferrite grain boundaries. The formation of WA laths in both adjacent ferritic grains resulted in a zig-zag shape of delta-ferrite grain boundaries due to their local rotation during austenite nucleation. Based on the EBSD results, a mechanism of the formation of the zig-zag grain boundaries has been proposed. Besides the Widmanstätten morphology, austenite also formed as films along the delta-ferrite grain boundaries. Sulfide precipitation along the delta/gamma interfaces made it possible to prove that austenite decomposition upon a drop in temperature was initiated by the formation of epitaxial ferrite. Further cooling brought the decay of austenite to either pearlite or a mixture of plate martensite and some retained austenite.https://www.mdpi.com/2075-4701/13/1/51GOESWidmanstätten austeniteK-S orientation relationshipepitaxial ferritezig-zag grain boundaries
spellingShingle Anastasia Volodarskaja
Kryštof Hradečný
Renáta Palupčíková
Petra Váňová
Vlastimil Vodárek
Microstructure Evolution in a GOES Thin Strip
Metals
GOES
Widmanstätten austenite
K-S orientation relationship
epitaxial ferrite
zig-zag grain boundaries
title Microstructure Evolution in a GOES Thin Strip
title_full Microstructure Evolution in a GOES Thin Strip
title_fullStr Microstructure Evolution in a GOES Thin Strip
title_full_unstemmed Microstructure Evolution in a GOES Thin Strip
title_short Microstructure Evolution in a GOES Thin Strip
title_sort microstructure evolution in a goes thin strip
topic GOES
Widmanstätten austenite
K-S orientation relationship
epitaxial ferrite
zig-zag grain boundaries
url https://www.mdpi.com/2075-4701/13/1/51
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AT renatapalupcikova microstructureevolutioninagoesthinstrip
AT petravanova microstructureevolutioninagoesthinstrip
AT vlastimilvodarek microstructureevolutioninagoesthinstrip