The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys

This study is aimed at exploring the effects of multi-stage homogenization and trace amounts of Zr and Sc on the microstructures, mechanical properties, and recrystallization of Al–4.5Zn–1.5Mg alloys. The mechanical properties of the AA7005 aluminum alloys after the T6 heat treatment were evaluated...

Full description

Bibliographic Details
Main Authors: Yang-Chun Chiu, Tse-An Pan, Mien-Chung Chen, Jun-Wei Zhang, Hui-Yun Bor, Sheng-Long Lee
Format: Article
Language:English
Published: MDPI AG 2021-01-01
Series:Applied Sciences
Subjects:
Online Access:https://www.mdpi.com/2076-3417/11/2/470
_version_ 1797542239110430720
author Yang-Chun Chiu
Tse-An Pan
Mien-Chung Chen
Jun-Wei Zhang
Hui-Yun Bor
Sheng-Long Lee
author_facet Yang-Chun Chiu
Tse-An Pan
Mien-Chung Chen
Jun-Wei Zhang
Hui-Yun Bor
Sheng-Long Lee
author_sort Yang-Chun Chiu
collection DOAJ
description This study is aimed at exploring the effects of multi-stage homogenization and trace amounts of Zr and Sc on the microstructures, mechanical properties, and recrystallization of Al–4.5Zn–1.5Mg alloys. The mechanical properties of the AA7005 aluminum alloys after the T6 heat treatment were evaluated through a hardness test and tensile test. The microstructures were analyzed by an optical microscope (OM), a differential scanning calorimeter (DSC), a transmission electron microscope (TEM), a scanning electron microscope (SEM), and electron backscattered diffraction (EBSD). The results show that the grain refinement effect of the as-cast, homogenized, and recrystallized Al–4.5Zn–1.5Mg alloy containing 0.05Sc (wt%) after the T6 heat treatment was more significant than that of the alloy containing 0.1Zr (wt%). In addition, compared with the aforementioned one-stage homogenization heat treatment, the two-stage homogenization made the dispersed grain phase (Al<sub>3</sub>Zr/Al<sub>3</sub>Sc) smaller. As a result, the T6 mechanical strength of the alloy after the two-stage homogenization heat treatment was better than that of the contrastive alloy after the one-stage homogenization heat treatment. However, the two different homogenization heat treatments caused a greater divergence between the sizes of the dispersed grain phases of the Al–4.5Zn–1.5Mg alloys containing Zr than between the sizes of the dispersed grain phases of the alloys containing Sc. Therefore, after the two-stage homogenization heat treatment, the alloy with 0.1Zr (wt%) promoted the mechanical properties better than the alloy with 0.05Sc (wt%).
first_indexed 2024-03-10T13:26:53Z
format Article
id doaj.art-36e8721970984ee3bde0d2787ecc8711
institution Directory Open Access Journal
issn 2076-3417
language English
last_indexed 2024-03-10T13:26:53Z
publishDate 2021-01-01
publisher MDPI AG
record_format Article
series Applied Sciences
spelling doaj.art-36e8721970984ee3bde0d2787ecc87112023-11-21T08:43:13ZengMDPI AGApplied Sciences2076-34172021-01-0111247010.3390/app11020470The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc AlloysYang-Chun Chiu0Tse-An Pan1Mien-Chung Chen2Jun-Wei Zhang3Hui-Yun Bor4Sheng-Long Lee5Institute of Materials Science and Engineering, National Central University, Jhongli 32001, TaiwanInstitute of Materials Science and Engineering, National Central University, Jhongli 32001, TaiwanInstitute of Materials Science and Engineering, National Central University, Jhongli 32001, TaiwanInstitute of Materials Science and Engineering, National Central University, Jhongli 32001, TaiwanInstitute of Materials Science and Engineering, National Central University, Jhongli 32001, TaiwanInstitute of Materials Science and Engineering, National Central University, Jhongli 32001, TaiwanThis study is aimed at exploring the effects of multi-stage homogenization and trace amounts of Zr and Sc on the microstructures, mechanical properties, and recrystallization of Al–4.5Zn–1.5Mg alloys. The mechanical properties of the AA7005 aluminum alloys after the T6 heat treatment were evaluated through a hardness test and tensile test. The microstructures were analyzed by an optical microscope (OM), a differential scanning calorimeter (DSC), a transmission electron microscope (TEM), a scanning electron microscope (SEM), and electron backscattered diffraction (EBSD). The results show that the grain refinement effect of the as-cast, homogenized, and recrystallized Al–4.5Zn–1.5Mg alloy containing 0.05Sc (wt%) after the T6 heat treatment was more significant than that of the alloy containing 0.1Zr (wt%). In addition, compared with the aforementioned one-stage homogenization heat treatment, the two-stage homogenization made the dispersed grain phase (Al<sub>3</sub>Zr/Al<sub>3</sub>Sc) smaller. As a result, the T6 mechanical strength of the alloy after the two-stage homogenization heat treatment was better than that of the contrastive alloy after the one-stage homogenization heat treatment. However, the two different homogenization heat treatments caused a greater divergence between the sizes of the dispersed grain phases of the Al–4.5Zn–1.5Mg alloys containing Zr than between the sizes of the dispersed grain phases of the alloys containing Sc. Therefore, after the two-stage homogenization heat treatment, the alloy with 0.1Zr (wt%) promoted the mechanical properties better than the alloy with 0.05Sc (wt%).https://www.mdpi.com/2076-3417/11/2/470Al–Zn–Mg alloyzirconiumscandiummulti-stage homogenizationsrecrystallized microstructures
spellingShingle Yang-Chun Chiu
Tse-An Pan
Mien-Chung Chen
Jun-Wei Zhang
Hui-Yun Bor
Sheng-Long Lee
The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys
Applied Sciences
Al–Zn–Mg alloy
zirconium
scandium
multi-stage homogenizations
recrystallized microstructures
title The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys
title_full The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys
title_fullStr The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys
title_full_unstemmed The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys
title_short The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys
title_sort effects of multi stage homogenizations on the microstructures and mechanical properties of al zn mg zr sc alloys
topic Al–Zn–Mg alloy
zirconium
scandium
multi-stage homogenizations
recrystallized microstructures
url https://www.mdpi.com/2076-3417/11/2/470
work_keys_str_mv AT yangchunchiu theeffectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT tseanpan theeffectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT mienchungchen theeffectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT junweizhang theeffectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT huiyunbor theeffectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT shenglonglee theeffectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT yangchunchiu effectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT tseanpan effectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT mienchungchen effectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT junweizhang effectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT huiyunbor effectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys
AT shenglonglee effectsofmultistagehomogenizationsonthemicrostructuresandmechanicalpropertiesofalznmgzrscalloys