Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity Sensing

This work presents a feedback closed-loop platform to be used for viscosity or viscoelasticity sensing of Newtonian or non-Newtonian fluids. The system consists of a photothermally excited microcantilever working in a digital Phase-Locked Loop, in which the phase between the excitation signal to the...

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Main Authors: João Mouro, Paolo Paoletti, Marco Sartore, Massimo Vassalli, Bruno Tiribilli
Format: Article
Language:English
Published: MDPI AG 2022-11-01
Series:Sensors
Subjects:
Online Access:https://www.mdpi.com/1424-8220/22/21/8421
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author João Mouro
Paolo Paoletti
Marco Sartore
Massimo Vassalli
Bruno Tiribilli
author_facet João Mouro
Paolo Paoletti
Marco Sartore
Massimo Vassalli
Bruno Tiribilli
author_sort João Mouro
collection DOAJ
description This work presents a feedback closed-loop platform to be used for viscosity or viscoelasticity sensing of Newtonian or non-Newtonian fluids. The system consists of a photothermally excited microcantilever working in a digital Phase-Locked Loop, in which the phase between the excitation signal to the cantilever and the reference demodulating signals is chosen and imposed in the loop. General analytical models to describe the frequency and amplitude of oscillation of the cantilever immersed in viscous and viscoelastic fluids are derived and validated against experiments. In particular, the sensitivity of the sensor to variations of viscosity of Newtonian fluids, or to variations of elastic/viscous modulus of non-Newtonian fluids, are studied. Interestingly, it is demonstrated the possibility of controlling the sensitivity of the system to variations of these parameters by choosing the appropriate imposed phase in the loop. A working point with maximum sensitivity can be used for real-time detection of small changes of rheological parameters with low-noise and fast-transient response. Conversely, a working point with zero sensitivity to variations of rheological parameters can be potentially used to decouple the effect of simultaneous external factors acting on the resonator.
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spelling doaj.art-3724672709ad44a788177bc99af56c792023-11-24T06:47:51ZengMDPI AGSensors1424-82202022-11-012221842110.3390/s22218421Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity SensingJoão Mouro0Paolo Paoletti1Marco Sartore2Massimo Vassalli3Bruno Tiribilli4Institute for Complex Systems, National Research Council (ISC-CNR), 50019 Florence, ItalySchool of Engineering, University of Liverpool, Liverpool L69 3GH, UKElbatech Srl, 57030 Marciana, ItalySchool of Engineering, University of Glasgow, Glasgow G12 8LT, UKInstitute for Complex Systems, National Research Council (ISC-CNR), 50019 Florence, ItalyThis work presents a feedback closed-loop platform to be used for viscosity or viscoelasticity sensing of Newtonian or non-Newtonian fluids. The system consists of a photothermally excited microcantilever working in a digital Phase-Locked Loop, in which the phase between the excitation signal to the cantilever and the reference demodulating signals is chosen and imposed in the loop. General analytical models to describe the frequency and amplitude of oscillation of the cantilever immersed in viscous and viscoelastic fluids are derived and validated against experiments. In particular, the sensitivity of the sensor to variations of viscosity of Newtonian fluids, or to variations of elastic/viscous modulus of non-Newtonian fluids, are studied. Interestingly, it is demonstrated the possibility of controlling the sensitivity of the system to variations of these parameters by choosing the appropriate imposed phase in the loop. A working point with maximum sensitivity can be used for real-time detection of small changes of rheological parameters with low-noise and fast-transient response. Conversely, a working point with zero sensitivity to variations of rheological parameters can be potentially used to decouple the effect of simultaneous external factors acting on the resonator.https://www.mdpi.com/1424-8220/22/21/8421Phase-Locked Loopmicrocantileversensingviscosityviscoelasticityelastic modulus
spellingShingle João Mouro
Paolo Paoletti
Marco Sartore
Massimo Vassalli
Bruno Tiribilli
Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity Sensing
Sensors
Phase-Locked Loop
microcantilever
sensing
viscosity
viscoelasticity
elastic modulus
title Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity Sensing
title_full Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity Sensing
title_fullStr Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity Sensing
title_full_unstemmed Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity Sensing
title_short Photothermal Self-Excitation of a Phase-Controlled Microcantilever for Viscosity or Viscoelasticity Sensing
title_sort photothermal self excitation of a phase controlled microcantilever for viscosity or viscoelasticity sensing
topic Phase-Locked Loop
microcantilever
sensing
viscosity
viscoelasticity
elastic modulus
url https://www.mdpi.com/1424-8220/22/21/8421
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