Field emission from crystalline niobium

Appreciable suppression of field emission (FE) from metallic surfaces has been achieved by the use of improved surface cleaning techniques. In order to understand the effects of surface preparation on field emission, systematic measurements were performed on five single crystal and three large grain...

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Main Authors: Arti Dangwal Pandey, Günter Müller, Detlef Reschke, Xenia Singer
Format: Article
Language:English
Published: American Physical Society 2009-02-01
Series:Physical Review Special Topics. Accelerators and Beams
Online Access:http://doi.org/10.1103/PhysRevSTAB.12.023501
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author Arti Dangwal Pandey
Günter Müller
Detlef Reschke
Xenia Singer
author_facet Arti Dangwal Pandey
Günter Müller
Detlef Reschke
Xenia Singer
author_sort Arti Dangwal Pandey
collection DOAJ
description Appreciable suppression of field emission (FE) from metallic surfaces has been achieved by the use of improved surface cleaning techniques. In order to understand the effects of surface preparation on field emission, systematic measurements were performed on five single crystal and three large grain samples of high purity (RRR>300) niobium by means of atomic force microscope, x-ray diffraction, scanning electron microscope (SEM), and dc field emission scanning microscope. The samples were treated with buffered chemical polishing (BCP), half of those for 30  μm and others for 100  μm removal of surface layer, followed by a final high pressure water rinsing. These samples provided the emission at minimum surface fields of 150  MV/m and those with longer BCP treatment showed the onset of field emission at slightly higher fields. A low temperature (∼150°C) heat treatment in a high vacuum (10^{-6}  mbar) chamber for 14 hours, on a selected large grain Nb sample, gives the evidence for the grain boundary assisted FE at very high fields of 250 and 300  MV/m. Intrinsic field emission measurements on the present Nb surfaces revealed anisotropic values of work function for different orientations. Finally, an interesting correlation between sizes of all investigated emitters derived from SEM images with respect to their respective onset fields has been found, which might facilitate the quality control of superconducting radio-frequency cavities for linear accelerators.
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spelling doaj.art-37359b055822493d9c2c690a14edda5d2022-12-22T00:03:46ZengAmerican Physical SocietyPhysical Review Special Topics. Accelerators and Beams1098-44022009-02-0112202350110.1103/PhysRevSTAB.12.023501Field emission from crystalline niobiumArti Dangwal PandeyGünter MüllerDetlef ReschkeXenia SingerAppreciable suppression of field emission (FE) from metallic surfaces has been achieved by the use of improved surface cleaning techniques. In order to understand the effects of surface preparation on field emission, systematic measurements were performed on five single crystal and three large grain samples of high purity (RRR>300) niobium by means of atomic force microscope, x-ray diffraction, scanning electron microscope (SEM), and dc field emission scanning microscope. The samples were treated with buffered chemical polishing (BCP), half of those for 30  μm and others for 100  μm removal of surface layer, followed by a final high pressure water rinsing. These samples provided the emission at minimum surface fields of 150  MV/m and those with longer BCP treatment showed the onset of field emission at slightly higher fields. A low temperature (∼150°C) heat treatment in a high vacuum (10^{-6}  mbar) chamber for 14 hours, on a selected large grain Nb sample, gives the evidence for the grain boundary assisted FE at very high fields of 250 and 300  MV/m. Intrinsic field emission measurements on the present Nb surfaces revealed anisotropic values of work function for different orientations. Finally, an interesting correlation between sizes of all investigated emitters derived from SEM images with respect to their respective onset fields has been found, which might facilitate the quality control of superconducting radio-frequency cavities for linear accelerators.http://doi.org/10.1103/PhysRevSTAB.12.023501
spellingShingle Arti Dangwal Pandey
Günter Müller
Detlef Reschke
Xenia Singer
Field emission from crystalline niobium
Physical Review Special Topics. Accelerators and Beams
title Field emission from crystalline niobium
title_full Field emission from crystalline niobium
title_fullStr Field emission from crystalline niobium
title_full_unstemmed Field emission from crystalline niobium
title_short Field emission from crystalline niobium
title_sort field emission from crystalline niobium
url http://doi.org/10.1103/PhysRevSTAB.12.023501
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