2-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrate
The title compound, C10H8N4O4·H2O, was obtained by the reaction of 5-hydroxy-2-nitrobenzaldehyde with cyanoacetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056 &...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2011-08-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536811025463 |
| _version_ | 1819294229400125440 |
|---|---|
| author | Hongbo Li Xiaocheng Ni |
| author_facet | Hongbo Li Xiaocheng Ni |
| author_sort | Hongbo Li |
| collection | DOAJ |
| description | The title compound, C10H8N4O4·H2O, was obtained by the reaction of 5-hydroxy-2-nitrobenzaldehyde with cyanoacetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056 Å. In the crystal, molecules are linked by N—H...O, O—H...N and O—H...O hydrogen bonds, generating a three-dimensional network. |
| first_indexed | 2024-12-24T04:23:00Z |
| format | Article |
| id | doaj.art-37e05a64331b48bea64878770a9879e4 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-24T04:23:00Z |
| publishDate | 2011-08-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-37e05a64331b48bea64878770a9879e42022-12-21T17:15:43ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-08-01678o2002o200210.1107/S16005368110254632-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrateHongbo LiXiaocheng NiThe title compound, C10H8N4O4·H2O, was obtained by the reaction of 5-hydroxy-2-nitrobenzaldehyde with cyanoacetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056 Å. In the crystal, molecules are linked by N—H...O, O—H...N and O—H...O hydrogen bonds, generating a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S1600536811025463 |
| spellingShingle | Hongbo Li Xiaocheng Ni 2-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrate Acta Crystallographica Section E |
| title | 2-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrate |
| title_full | 2-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrate |
| title_fullStr | 2-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrate |
| title_full_unstemmed | 2-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrate |
| title_short | 2-Cyano-N′-(5-hydroxy-2-nitrobenzylidene)acetohydrazide monohydrate |
| title_sort | 2 cyano n amp 8242 5 hydroxy 2 nitrobenzylidene acetohydrazide monohydrate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536811025463 |
| work_keys_str_mv | AT hongboli 2cyanonamp82425hydroxy2nitrobenzylideneacetohydrazidemonohydrate AT xiaochengni 2cyanonamp82425hydroxy2nitrobenzylideneacetohydrazidemonohydrate |